Alaska Logo
Department of Commerce, Community, and Economic Development
Alaska Oil and Gas Conservation
Commission
Loading...
HomeMy WebLinkAboutGMC Data Report No. 109Vitrinite reflectance data and analysis of the 900 - 13,816 foot interval of the Colorado Oil Malaspina Unit No. 1-A well Received 9 February 1989 Total of 25 pages in report Geologic Materials Center Data Report 109 VITRINITE REFLECTANCE ANALYSIS OF THE INTERVAL 900 - 13,816 FT MALASPINA # lA WELL, ALASKA IntroducliO,rl .! This report describes the vitrinite reflectance analysis of 15 cuttings samples from the Malaspina # lA oil exploration well. Fifty vitrinite reflectance measurements for each sample are taken wherever possible utilizing a Zeiss 01K photometer attachment mounted on a Zeiss Pho- toscope 1. Each measurement is qualified as to poor (P), good (G) or excellent (E). Depending upon such factors as; particle size, pitting, scratching or the proximity to pyritic particles. The measurements of particles interpreted to be reworked vitrinite are labeled with an "R" while the measurements of particles interpreted to be caved material are' labeled. With .a "C". A .table and a plot of all measurements displayed as a histogram for each sample are g!ven in-APpendix A. A vitrinite reflectance log is included which displays each histogram at the level of the sample. The material considered as caved is cross-hatched in blue while the material considered to be reworked is cross-hatched in red. The good and excellent samples are coloured in solid green while the poor measurements are coloured in cross-hatched green. Fudher colour copies of this log are available through the Bujak Davies Group. The laboratory procedures for the mounting and polishing of the vitrinite samples follows the methodology described by Davies and Avery (1984) in a 'triple mount stub with standard 600 grit,.3 micron and .05 micron polishing procedure on Buehler Automet polishing equipment. This methodology results in a polished mount of unoxidized kerogen. The levels of vitrinite reflectance are compared to the Thermal Alteration Index (TAI) of Bujak, Barss & Williams (1977a,b)in Table 1 and are subdivided into various levels of thermal maturation for the generation of liquid and gaseous hydrocarbons. This generation model will vary from basin to basin depending upon the geohistory and kerogen compositions. . GMC Data Report 109 Page 1/25 Bujak Davies Group Malaspina #1 ..... 2 VITR!NITE REFLECTANCE SUMMARY Maturity Zones Based on Ro 900-5,760ft 6,600-12,750ft 13,350-13,823fl Immature Onset of Maturation Marginally Mature Immature Zone: 900-5.760ft The two uppermost samples in'this zone, at 900 and 1,920ft, are entirely reworked. At 3090ft there appears to be.several populations of vitrinite on the histogram. The population chosen as in situ has an Ro=0.48%. At 4,200ft and 5,490ff the vitrinite is again almost entirely reworked. One reading from in situ vitrinite in the 5,490ft sample, may suggest that the sample is still in the immature zone (Ro=0.47%); this should not be heavily relied upon. Onset of Maturation Zone: 6.600-.12.760fi The sample at the top of this zone at 6,600fl contains very little vitrinite. It is again almost entirely reworked. From only two in situ readings, the Ro=0.565%. This may indicate that the sample is in the zone of onset. The 2,880ft sample (Ro=C].534%) -is in aggreement with the overlying sample. Other samples deeper in this zone have slightly depressed Ro's and only fair histogram distributions, due to the presence of cavings and reworked material. The 10,560ft, 11,880ft and 12,510ft samples (Ro's=0.501,0.530% and 0.540%, respectively) all have relatively good histogram distributions and can be considered reliable. Marginally Mature Zone: 13,350-1,3.823 Both samples in this zone have gaod histogram distributions, even though they contain a fair amount of pyrite and little vitrinite: From fifty readings, taken on both samples, the Ro's=0.736 and 0.798% indicate that these samples are well within the oil window. GMC Data Report 109 Page 2/25 Bujak Davies Group Malaspina #1 ..... 3 REFERENCES BUJAK, J.P., BARSS, M.S. & WILLIAMS, G.L. 1977 Offshore eastern Canada Part !. Offshore east Canada's organic type and colour and hydrocarbon potential. Oil and Gas Journal, vol.75, pp. 198-2132. BUJAK, J.P., BARSS, M.S. & WILLIAMS, G.L. 1977 Offshore eastern Canada Pad II. Offshore east Canada's organic type and colour and hydrocarbon potential. Oil and Gas Journal vol.75, pp.96-100. DAVIES, E.H. & AVERY, M.P. 1984 A system for vitrinite reflectance analysis on dispersed organic matter for offshore eaStern Canada. In: .Current Research, Part A, Geological SurveY of Canada, Paper 84-114, Pp.367-372. GMC Data Report 109 Page 3/25 Bujak Davies Group Malaspina #1 ..... 4 TABLE 1: TAI & Ro% TA[ Spo re Approx. Amorphous col our Ro equiv, kerogen Herbaceous-woody kero~en 1 Green/Yellow Immature 1+ Yellow 0.35% Immature 2- Yellow/orange 0.45% Immature 2-to2 Orange 0.50% Onset of maturity 2 Orange/brown 0.60% Marginally mature 2to2+ Brown/orange 0.70% Marginally mature 2+ Light brown 0.9% Peak maturity 2+to3- L~Brown/brown 1.0% Highl.y mature 3- Brown 1.1% Highly mature 3-to3 Med. brown 1.2% Highly mature 3 Brown/df.brown 1.5% Overmature 3+ Dark brown 2.0% Overmature 4- B1 ack 2.5% Overmature 4 Black/corroded 4.0% Overmature Ilnmature Immature Immature Immature Immature Onset of maturity -Onset of .maturity Peak maturity Peak maturity Peak maturity Peak maturity Highly mature Highly mature Overmature Table 1: Comparison of Vitrinite Reflectance (Ro%) and the Thermal Alteration Index scale (TAI) of Bujak, Barss & Williams (1977a,b). GMC Data Report 109 Page 4/25 Bujak Davies Group Malaspina #1 APPENDIX A VITRINITE REFLECTANCE MEASUREMENTS AND HISTROGRAMS GMC Data Report 109 Page 5/25 Client: M.M.S. Well: MALASPINAilA Area: ALASKA Scientist: DUMCIUS Date: JULY 1988 Samples are: F VITRINITE DATA: Sample Depth : 900.0 0.700 R 0.830 R 0.830 R 0.850 R 0.860 R 0.860 0.880 R 0.890 R 0.900 R 0.900 R 0.910 R 0.910 0.910 R 0.910 R 0.920 R 0.930 R 0.930 R 0.940 0.960 R 0.960 R 0.960 R 0.980 R 0.990 R 1.000 1.040 R 1.040 R 1.050 R 1.050 R 1.060 R 1.060 1.110 R 1.130 R 1.140 R 1.140 R 1.170 R 1.170 1.260 R 1.260- R 1.320 R 1.360 R 1.370 R 1.430 1.980 R Actual Mean = 1.055 Actual Standard Deviation = 0.240 0.87O 0.910 0.950 1.030 1.060 1.180 1.900 m Con~nent : Mostly fine light grey amorphous inorganic material; little vitrinite present. Sample Depth : 1920.0 0.650 R 0.680 R 0.690 R 0.710 R 0.720 R 0.730 0.880 R 0.890 R 0.900 R 0.920 R 0.930 R 0.950 0.960 R 0.990 R 1.000 R 1.000 R 1.010 R 1.040 -1.140 R 1.150 R 1.210 R 1.250 R 1.260 R 1.290 1.300 R 1.330 R 1.330 R 1.330 R 1.330 R 1.380 1.440 R 1.450 R 1.470 R 1.490 R 1.550 R 1.570 1.660 R 1.790 R 1.790 R 1.810 R 2.030 R 2.120 2.240 R Actual Mean = 1.253 Actual Standard Deviation - 0.404 Comment : Mostly fine light grey amorphous inorganic material; little vitrinite present. · . . Sample Depth : 3090.0 0.290 C 0.390 0.400 0.430 0.430 0.450 0.460 0.480 0.520 0.540 0.550 0.560 0.610 R 0.650 R 0.710 R 0.710 R 0.740 R 0.780 0.800 R 0.820 R 0.950 R 0.990 R 1.070 R 1.100 1.180 R 1.200 R 1.290 R 1.360 R 1.370 R 1.380 1.450 R 1.450 R 1.490 R 1.560 R 1.610 R 1.650 Actual Mean - 0.920 Actual Standard Deviation ~ 0.434 Edited Mean - 0.480 Edited Standard Deviation - 0.062 Comment : Mostly fine light grey amorphous inorganic material; little vttrtntte present. 0.840 0.950 1.070 1.290 1.400 1.590 2.140 O. 460 0.570 0.790 1.100 1.420 1.860 GMC Data Report 109 Page 6/25 Sample Depth : 4200.0 0.600 R 0.640 R 0.680 R 0.680 R 0.680 R 0.680 R 0.700 0.720 R 0.770 R 0.770 R 0.780 R 0.780 R 0.790 R 0.790 0.800 R 0.840 R 0.850 R 0.860 R 0.880 R 0.900 R 0.900 0.910 R 0.910 R 0.920 R 0.950 R 0.950 R 0.960 R 0.960 0.970 R 0.980 R 0.990 R 1.000 R 1.020 R 1.020 R 1.020 1.030 R 1.060 R 1.150 R 1.160 R 1.160 R 1.280 R 1.290 1.300 R 1.320 R 1.360 R 1.380 R 1.500 R 1.510 R 1.560 1.610 R Actual Mean = 0.986 Actual Standard Oevlation = 0.257 Cor~nent : Mostly fine light grey amorphous inorganic material; little vltrintte present. Sample Depth : 5490.0 0.470 0.740 R 0.750 R 0.810 R 0.830 R 0.940 R 1.030 1.100 R 1.200 R 1.240 R 1.240 R 1.340 R 1.380 R 1.390 1.420 R Actual Mean - 1.059 Actual Standard Deviation = 0.291 Edited Mean ~ 0.470 Edited Standard Deviation = 0.000 Con~nent : Almost entirely fine light grey amorphous inorganic material; very little vitrinite present. Sample Depth : 6600.0 0.530 0.600 0.950 R 0.990 0.670 r 0.670 R 0.720 r 0.720 R 0.740 Actual Mean - 0.732 Actual Standard Deviation ~ 0.150 Edited Mean = 0.565 Edited Standard Deviation = 0.049 Comnent : Almost enttrely fine light grey amorphous inorganic material; very ltttle vttrlnite present. Sample Depth : 8280.0 0.260 C 0.260 C 0.270 C 0.310 C 0.320 C 0.330 C 0.330' 0.340 C 0.370 C 0.390 C 0.390 C 0.390 C 0.410 C 0.410 0.420 C 0.430 C 0.430 C 0.430 C 0.440 0.450 0.480 0.480 P 0.480 0.490 0.490 0.490 0.500 0.510 0.510 0.510 0.520 * 0.530 0.540 0.540 0.550 0.550 0.560 P 0.570 0.570 0.580 0.590 0.590 0.600 0.600 0.600 0.620 0.700 R 0.760 R 0.770 0.790 R Actual Mean - 0.489 Edited Mean - 0.534 Actu'al Standard Deviation - 0.126 Edited Standard Deviation ~ 0.050 Comment :Ltttle vttrlntte present. GMC Data Report 109 Page 7/25 San~ole Depth : 9090.0 O. 290 C O. 320 C O. 330 C O. 340 C O. 350 0.350 C 0.350 C 0.350 C 0.360 C 0.360 O. 380 C O. 380 C O. 380 C O. 390 C O. 390 0.410 C 0.410 C 0.410 C 0.420 C 0.420 0.430 C 0.440 0.450 0.450 0.450 O. 480 O. 490 O. 490 O. 490 O. 500 O. 560 O. 580 O. 590 O. 600 O. 660 1. 290 R Actual Mean = 0,457 Actual Standard Deviation = 0.155 Edited Mean : 0.505 Edited Standard Deviation = 0.054 Cor~nent : Mostly small, occasionally large vitrinite particles present° 0.350 O. 360 0.400 0.420 0.450 0.540 0.660 0.350 0.360 0.410 0.430 0.480 0.550 0.740 Sample Depth : 9810.0 0.400 C 0.430 C 0.450 0.460 0.480 0.510 E 0.520 0.520 0.560 0.600 0.670 R 0.680 R 0.690 R 0.710 R 0.710 0.720 R 0.720 R 0.730 R 0.760 R 0.770 0.790 R 0.810 R 0.830 R 0.830 R 0.830 0.850 R 0.880 R 0.880 R 0.890 R 0.900 1.010 R 1.020 R 1.040 R 1.050 R 1.059 1.400 R Actual Mean = 0.766 Actual Standard Deviation = 0.215 Edited Mean -- 0,530 Edited Standard Deviation : 0.062 Conrnent : Mostly small particles present. 0.500 0.630 0.710 0.770 0.830 0.910 1.130 0.500 0,630 0.710 0,790 0.840 0.930 1.240 Sample Depth : 10560.0 0.390 C - 0.410 C 0.420 C 0.430 0.440 0.440 0.450 0.450 , 0.460' 0,460 0.470 0.480 0.500 0.500 0.500 0.500 0.510 0.520 0.520 0.520 0.560 0.560 0.570 0.580 0.670 R 0.670 R 0.710 R 0.730 0.880 R C 0.430 C 0.460 0.480 0.500 0.530 0.610 R 0.770 R Actual Mean = 0.538 Actual Standard Deviation = 0.116 Edited Mean = 0.501 Edited Standard Deviation = 0.044 · Conment : Occasionally large, mostly small vttrlntte particles present. O. 430 O. 460 0.480 0.510 0.540 0.650 0.780 0.440 0.460 0.490 0.510 0.560 0.650 0.870 GMC Data Report 109 Page 8/25 Sample Depth : 11160.0 0.370 C 0.380 C 0.390 £ 0.410 C 0.440 0.440 0.450 0.470 0.510 0.520 0.520 0.520 0.560 0.560 0.590 0.590 0.710 R 0.730 R 0.800 R 0.810 R 0.410 0.480 0.530 0.590 0.820 0.430 0.500 0.530 0.600 0.840 0.440 0.510 0.550 0.620 0.850 Actual Mean = 0.556 Actual Standard Deviation = 0.139 Edited Mean = 0.524 Edited Standard Deviation = 0.055 Comnent : Little vttrtntte present. Sample Depth : 11880.0 O. 320 C O. 380 C O. 440 P O. 440 O. 510 O. 520 0.540 0.540 O. 680 O. 720 R 0.810 R 0.810 R 0.950 R 1.040 R 0.400 C 0.400 C 0.480 0.490 0.520 0.520 0.570 0.580 0.720 R -0~740 'R 0.830 R 0.840 R 1.120 R 0.420 0.490 0.530 0.580 0.760 0.840 0.420 0.500 0.530 0.580 0.780 0.880 0.430 0.500 0.530 0.590 0.800. 0.880 Actual Mean = 0.621 Actual Standard Deviation = 0.190 Edited Mean = 0.530 Edited Standard Deviation : 0.053 Conment : Little vttrintte present. Sample Depth : 12510.0 0.400 C 0.410 C 0.440 0.440 0.490 0.490 0.490 0.500 0.520 0.520 0.520 0,530 0.550 0.550 0.560 0.570 0.590 0.600 0.600 0.620 0.640 0.750 R 0.810 R 0.810 0.870 R 0.890 R 0.900 R 0.930 1.210 R 0.460 0.500 0.540 0.570 0.620 R 0.83O R 0.980 0.470 0.500 0.540 0.580 0.620 0.840 1.190 O. 480 0.510 0.55O 0.580 0.630 0.840 1.210 Actual Mean - 0.645 Actual Standard Deviation - 0.206 Edtted Mean - 0.540 Edited Standard Deviation - 0.056 Comment : Little vttrtntte present. GMC Data Report 109 Page 9/25 Sample Depth : 13350.0 0.420 C 0.600 0.620 0.620 0.630 P 0.630 0.640 0.650 0.660 0.660 0.660 0.660 0.680 0.680 0.690 0.700 0.700 0.710 0.720 0.720 0.720 0.720 0.730 0.730 0.740 P 0.750 0.750 0.760 0.760 0.760 0.770 0.780 0.780 P 0.790 0.790 0.800 0.820 0.830 0.830 P 0.830 0.830 0.840 0.880 Actual Mean = 0.725 Actual Standard Deviation = 0.084 Edited Mean = 0.731 Edited Standard Deviation : 0.072 Comment : Common pyrite; abundant degraded amorphous material; little vitrinite present. 0.630 0.660 0.720 0.740 0.760 0.810 0.870 Sample Depth : 13816.0 0.580 C 0.600 0.640 0.660 0.690 0.700 0.710 0.720 0.720 0.720 0.730 0.730 0.730 0.740 0.750 0.760 0.770 0.770 0.770 0.790 0.790 0.790 0.790 0.790 0.820 0.820 0.830 0.830 0.840 0.840 0.880 0.890 0.920 0.930 0.940 0.940 0.960 .000 R R 1. 59 i.260 n Actual Mean = 0.831 Actual Standard Deviation = 0.151 Edited Mean = 0.798 Edited Standard Deviation : 0.097 Comment : Common pyrite; abundant degraded amorphous material; little vitrtnite present. 0.710 0.730 0.770 0.790 0.860 0.950 1.210 GMC Data Report 109 Page 10/25 BUJAK DAVIES GROUP' VITRINITE SAMPLE ' 900f MALASPINA#~A Population Meon In Si~u Caved Reworked Tots! Tota! meaeuremen~e thte eemple : 50 Stmndmrd Devtmtton 0.24 0.24 .3 .4 .5 .6 .8 1 I I I r , I I .3 .4 .5 .6 .0 t Ceved Zn $ttu t.5 ! Reworked BUJAK DAVIES GROUP · VlTRINITE MALASPINA#1A SAMPLE · '1920f Population Mean In S~tu Caved Reworked Total Standapd Deviation ~ . 25 0.40 ~ . 25 0.40 Total memeupemante thio ammple : DO .3 .4 .5 .6 .8 t 1.5 2 3 4 , .I ., I . I I I. I I I , · ..... .3 .4 .5 .6 .8 :~ t.5 2 3 4 Csved In Sttu Re~orkecl GMC Data Report 109 Page 12/25 , . MALASpINA# ~A BUJAK DAVIES GROUP ' VITRINITE SAMPLE ' 3090f Po~u]ation Mean In Situ 0.48 0.06 Caved 0.29 -- Reworked 1.t5 0.35 Total 0.92 0.43 Tote] meaeuremente thie eemple : 42 .3 .4 .5 .6 .8 I 1.5 2 3 4 I I I I I I I I ' I . .3 .4 .§ .6 .8 t t.§ 2 3 4 Caved In 8itu Rewor, l<ed e~r n.,. o~.,,, ina Page 13/25 BUdAK DAVIES GROUP ' VITRINITE HALASPINA#~A SAMPLE ' 4200f Population Memn In Sttu - Ceved -- Reworked o.gg Total O.gg Torsi meeeuPsments this Stenderd Devtstion 0.26 .3 o4 .5 .6 .8 ! 1.5 2 3 4 _ i I I I ! .1 I I ',. , ' ' '! ~' '~ ~ I I ~ .3 .4 o~ .E .8 I ~.5 2 3 4 Caved :In Sttu Rev,~ooi<ed , ,, ,, AMC. O~t~ Rmnnrt lOc] Paqe 14/25 BUJAK DAVIES GROUP° VITRINITE MALASPINA#1A SAMPLE · 5490f PopuIot~on Mean Standard Dev&ation In Sttu 0.47 -- Caved -- -- Reworked 2.t0 0.28 Total 1.08 0.2g Caved .3 .4 .5 .6 I I I ' .4 .5 .IS In 8itu t.5 2 3 4 I I I · ~.5 2 Rawor-I<ed GMC Data ReBort 109 Paqe 15/25 BUJAK DAVIES GROUP · VITRINITE SAMPLE ' 6600f MALASPINA#~A Populmtion Memn Stendapd Deviation In Situ 0.56 0.05 Caved - -- Rewopked 0.78 0.13 Total 0.73 0.~§ Total meaau'pemente thia emmple : 9 .3 .4 .5 .6 .8 t .5 2 3 4 I I I I i I I i '' ~ ' !4 ! ~ ~ " t ~ i "' .3 . .~ .ii .8 - I ~,.§ 2 3 4 Caved In 8ttu Rewop~ed GMC Data Report 109 Page 16/25 MALASPINA#~A BUJAK DAVIES GROUP ' VITRINITE SAMPLE ' 8280f PopuIet~on Mean Standard Oev~etion In Sttu 0.53 0.05 Caved 0.36 0.08 Reworked 0.78 0.04 Tote! O.4~ O.~3 Tote1 m~m~urement~ thi~ aampl~ : ~O .3 .4 .§ .6 .8 t t.5 2 3 4 , , I I I I I I I I . . ' i I l:· I I ' ii .3 .4 .~ ., .e , ,.~ z 3 4 Caved :rn 8ttu Rewo~,l<ed , ~Mr n~t',,1 ~,nnv,'l' lflq Paae ]7/25 BUJAK DAVIES GROUP · VITRINITE SAMPLE · 9090f HALASPINA#~A Standard Deviation In Situ 0.51 0.05 Caved 0.38 0.04 Reworked 0.84 0.30 Total 0.46 0.C5 Total memaupemente this sample .3 .4 .5 .6 .8 ! .5 2 3 4 I I I I I I I ~ ~ ~ ~ ~ 'i ~ i ' .3 .4 .5 .6 .8 t 1.§ 2 3 4 ', r Caved ..' In Sttu Rewopl<ed ., GMC Data Report 109 Page 18/25 BUJAK DAVIES GROUP · VITRINITE MALASPINA#~A SAMPLE · 98]0f Population MeSh Stsndepd Deviation In Situ 0.53 0.06 Caved 0.42 0.02 Reworked 0.86 0.t7 Total 0.77 0.21 .3 .4 .5 .6 .8 t ~.5 2 3 4 ., . I I I I I I I .! · ! .3 .4 .5 .6 .8 I S.5 :)3 4 : - , Caved In Situ RewoPked , , GMC Data Report 109 Page 19/25 BUJAK DAVIES GROUP ' VITRINITE HALASPINA#~A SAMPLE ' :tO560f Popu~mtSon Henn Stmndmrd D~v&mt~on In Situ 0.50 O.O4 Cmvmd 0.42 0.02 Reworked 0.74 O.Og Total 0.54 0.~2 TotmZ meaaurementa th/~ aampZe : 50 .3 .4 .5 .6 .8 ! ,5 2 3 4 I I I I I ., I ! . 1 I I i I i I I .3 .4 .~ .6 .8 t t.5 2 3 4 Ceved In S~tu Reworked . GMC Data Report 109 Page 20/25 BUJAK DAVIES GROUP ' VITRINITE MALASPINA#~A SAMPLE ' ~.~.60f ~tmndm~d Oevimt&on In Situ 0.52 0.08 Ceved 0.40 0.02 Reworked 0.79 0.05 Totel 0.58 0.t4 .3 .4 .5 .6 .8 ! 1.5 2 3 4 I I I ! I I ! I , 3 .4 .5 .6 .6 .]. f..5 2 - . 4 . Caved 'rn Sttu Rewor"~ed · r GMC Data Report 109 Page 21/25 BUJAK DAVIES GROUP ' VITRINITE MALASPINA#JA SAMPLE ' 11880f Population Nean StandePd Devtet&on · n Sttu 0.53 0.05 Caved 0.40 0.04 Rewopked 0.84 0.11 Tote! 0.82 0.19 Total meaeupementa thia aamp3e : 45 .3 .4 .5 .6 .8 ! t,5 2 3 4 ., I.. I I ... I I ., . I I I · · 3 .4 .~ .8 .8 I t.5 2 3 4 Cmved ]:n Sttu GMC Data Report 109 Page 22/25 BUJAK DAVIES GROUP ' VITRINITE MALASPINA#~A SAMPLE ' ~2510f PoDuZ~on Mean Zn Sttu 0.54 0.08 Caved 0.40 0.00 Reworked 0.93 0.i8 Torsi 0.84 0.21 Totei meaeuremente thte eampie : 50 .3 .4 .5 .6 I I I .8 t 2 3 4 I I I Caved .4 .5 .6 o8 1 In 8itu i Re~or, l<ed GMC Data Report 109 Page 23/25 BUJAK DAVZES GROUP ' VTTRINTTE SAMPLE ' :13350f NALASPINA#~A Population Mean Zn S&tu 0.73 0.07 Caved 0.42 -- RewopKad - -- Total 0.72 0.08 Total meaeupamente t~te oampZe : 50 .3 ,4 .§ .6 I I Caved .8 ,, .8 I In Sttu t.5 1.5 2 RewoPl<ad GMC Data Report 109 Page 24/25 BUJAK DAVIES GROUP ' VITRINITE SAMPLE ' 13B~6f MALASPINA#1A Population Mean Standard Deviation In Situ 0.80 O. 10 Caved 0.58 -- Reworked 1.17 0.06 Total 0.83 0.15 Total meaaurements this aample : 50 .3 .4 .fl .§ .8 I .5 2 3 4 I I I I I Il · I ! I l_ .3 .4 . .6 .6 t t.~ 2 3 4 Caved In Sttu Reworked .. GMC Data Renort 109 Paae 25/25