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GMC Data Report No. 150
Carbon isotope and hydrocarbon characteristic determinations with gas chromatographs mass spectroscopy data of samples from the following four wel 1 s: Atlantic Richfield Itkillik River Unit No. I (of core, 7902' - 7911'); Arco Alaska Inc. KRU West Sak No. 26 (of core, 6873' - 6885'); Atlantic Richfield Toolik Fed No. 2 (of dry cuttings, 7830' - 7860'); and Atlantic Richfield Nora Fed No. 1 (of dry cuttings, 12,460' - 12,580'). Received 18 January 1990 Total of 29 pages in report State of Alaska Geologic Materials Center Data Report No. 150 WELL ITKILLIK R-1 WEST SAK-26 TOOLIK FED-2 NORA FED-1 EXTRACT ISOTOPE DATA DEPTH(') CODE 7902-7911 WF 3640 6873-6885 WF 3641 7830-7860 WF 3642 12400-12580 WF 3643 C ISOTOPE COMPN -27.28 -29.70 -30.23 -27.66 GMC Data Report No. 150 Page 1/29 PETROt_EUIt GEOCHEmlSTRY *~* SAMPLE NAME INSTRUMENT !NJECT TIME METHOD USED SEOUENCE RESULT F!LE REPORT T !f'lE : BEAUFORT!AN L,.IF?,64{~ : HPLC F I D -- : Fr t Oct 22. 1989 12: 32:26 Dm : /METHO0/HPLC F!D0.MTH : /DATA/LEJOP/SEOUENCE/HP1090 AUTOW.SEL-I : /RESULT/WF3640_SAP.RES : 2:18 PM FRI. , 1 DEC. , 1989 Satucates Apomat ics 1 Aromatics 2 Polars RESPONSE AREA TIME FACTOR 40110. 5.29 .1225E-0D 1550. 9.42 .5470E-04 338?. 14.36 .5470E-04 t0356. 19.92 .4160E-04 Saturates Aroma t i cs Po lars AMOUNT (mg) ~ RESIDUE .51 42.2 .27 22.2 .4~ Saturates Aromatics Potars Asohaltenes OIL 41.9 22.1 35.4 ./ GMC Data Report No. 150 Page 2/29 ~D -5 r-~ Z O · O N ~Z .77 .62 ~%tes 5.25 .46 SAMPLE: BEAUFORTIAN NF3640 ANALYZED: Fri Oct 27, 1989 12: 37:26 pm METHO0: HPLC FIO0 RESULT: /RESULT/HF3640 SAP.RES PETROLEUM GEOCHEMISTRY SATURATE GC SAMPLE NAME INSTRUMENT INJECT TIME METHOD USED RESULT FILE REPORT TIME B&-8 STUDY WF3640 HP_5890_2 Man Nov 6, 1989 12:13:03 pm /METHOD/SAT5890C.MTH /RESULT/WF3640 SAT.RES -- 5:01 PM MOlq.~ 6 NOU.~ 1989 CPI UALUE : 1.12 PRISTANE / PHYTANE : PRISTANE / El? : PHYTANE / C18 : 2.29 C15×C25 : 1.55 .51 Ci?/Pr : 1.96 .25 C18×Ph : 3.95 AREA ~AREA NALK TIME NORM N-CiO N-Cll N-Ci2 N-C13 N-C14 N-C15 N-C16 N-C17 N-C18 N-C19 N-C20 N-C21 N-C22 N-C23 N-C24 N-C25 N-C26 N-C27 N-C28 N-C29 N-C30 N-C31 N-C32 N-C33 N-C34 N-C35 N-C36 211. .0 5.26 .00 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 1229. .0 12.07 .00 66825. 2 · 2 14.05 . 27 245258 . 8.3 15 · 93 1 · 00 272646. 9.2 17.69 1. 11 288822. 9.7 19 · 35 1.18 211981. 7.1 20.92 .86 19 0552 · 6.4 22 · 41 . 78 174915. 5.9 23 · 84 . 71 191341 · 6 . 4 25 · 21 . 28 197582. 6.6 26.53 .80 210558. 2. 1 27.29 .86 162952. 5.5 28.99 .66 158947. 5.3 30 . 15 . 65 112382. 3.8 31.26 .46 120254. 4. 1 32.34 .49 81388. 2.2 33.32 .33 80634. 2.7 34.38 .33 51820. 1.7 35.35 .21 42940. 1.4 36.29 .17 28359. 1. 0 37.19 . 12 35473. 1.2 38.12 . 14 17062. .6 39.15 .07 17121. .6 40.30 .07 9054. .3 41.63 .04 AREA %AREA ISPR TIME Far'nesane Ac~clic C16 Acyclic C18 Pr istane Phytane 5854. 2.0 13.63 15346. 5.2 15.37 72338. 24.5 18.54 147720. 50.1 19.50 53674. 18.2 21 · 09 GMC Data Report No. !50 Page 4/29 31.54 25. i9. 6.67 .46 i~.50 . 10.3! aa. ia 25,93 29,75 33,56 37.37 minutes SAI~PLE: B~,B STUDY WF3640 ANALYZED: Non Nov 6, 1989 i2: 13:03 pm RESULT: /RESULT/WF3640 SAT.RES NETHOD: SAT5890C 41,i8 45,00 C. ~,IID~:iC DATA: kF3648_SAT t~l SCANS 1 TO 4580 ! ~,,'31 xSS liS: 28:00 CALI: HF3640_SAT ~3 SR~'!PLE: HF3640_SAT COI,~OS.: HP THIN FILM, RES=NORM ,.~.,~-: ,4 1,4988 LHBP-L: N 0, 4.8 ~!UAN: A ~'., 1.8 J 8 SASE: LI 28, 3 080 2000 3800 4888 ~: 40 :-'i:::: 20 50:00 F_,E;: 40 78:48. TilqE HiOMASS CHROMATOGRAMS DATA: WF3640_SAT #1 SCANS 1588 TO 4500 18/31/89 i6:28:88 CALl: HF3648_SAT #3 SAMPLE: NF3648_SAT COHOS.: HP THIN FILM, RES=NORM RA~;E: G 1,4988 LABEL: N 8, 4.8 QUAN: A 8.. 1.8 J 8 SASE: U 28, 3 5(~:~ 2888 2588 38¢~8 :,: 0 i.-.1 ..-,.): .... i_~1.057 z 0, 462. ';" i ?. , ~ .................. I "'~' ' ' .:,.,uu 4888 4588 """ 58:2E~' ~:40 75:88 TIME i'l];Oi.~SS CHROi'I~TOC, R~i"IS DATA: 14F3640_SAT ~1 SCANS 30~ TO 450E~ :~E~/'Si/',-",9 1~:2~:00 C~LT: NFS~40_SAT ~ S~.~F'LE: HF3940_SAT C:',}!.?~S,: HP THIN FILI~, RES=NORFI RAHs]E: G 1,4~80 LABEL: N 0, 4.0 QUAN: A 0.. 1.0 O ~9 E:ASE: U 2.8, 3 ~:?.S. Z 0 I i ' I __ n,.,'..,. SC:AIqS -"~'- TO 3588 ['ilD~'iAi.~-. CHROMATOGRAMS ~, M: NF3~.40_SAT ~1 10,"3.1,'8~ 1G:28:88 CALl: NF3~48-SAT ~3 SA.['~F'LE: lqF3~48_SAT .'ZC::'~D'S.: HP THIN FILM, RES=i~ORM o.'.,.-.~ G 1 4988 LABEL: N 8, 4 8 QUAN: A 8 i 8 J 8 BASE: U 28, 3 I I I 4~2. I [, o~ 217. PETROLEUM GEOCHEMISTRY SATURRTE GC SAMPLE NAME INSTRUMENT INJECT TIME METHOD USED RESULT FILE REPORT TIME : B&B STUDY WF3641 : HP_5890_2 : Mort Now 6, 1989 1:08:35 : /METHOD/SAT5890C.MTH : /RESULT/WF3641_SAT.RES : 5:26 PM MON. ~ 6 NOU.~ pm 1989 CPI UALUE : 1.24 PRISTANE / PHYTANE : PRISTANE / C12 : PHYTANE / C18 : 1.16 C15/C25 : .10 .45 £12/Pr : 2.24 .36 C18/Ph : 2.29 AREA %AREA NALK TIME NORM C15 N-CI0 N-Clt N-C12 N-C13 N-C14 N-C15 N-C16 N-C17 N-Ci8 N-C19 N-C20 N-C21 N-C22 N- C23 N-C24 N-C25 N-C26 N-C2? N-C28 N-C29 N-C30 N-C31 N-C32 N-C33 N-C34 N-C35 N-C36 130. .2 5.76 .41 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 315. .6 15.90 t.00 800. 1.5 17.65 2.54 2758 . 5.3 19 · 31 8.75 2966. 5.7 20.88 9.41 3527. 6.8 22.38 11.19 3928. 7.5 23.81 12.46 3651. 7.0 25.18 11.58 3624. 6.9 26 . 49 11.49 4146 . 7.9 27.74 13.15 3062. 5.9 28.95 9.71 3291 . 6.3 30 · 11 10.44 2380. 4.6 31.23 7.55 2362. 4.5 32.31 7.51 1861. 3.6 33.35 5.90 2054. 3.9 34.36 6.51 1214. 2.3 35.33 3.85 3106. 5.9 36.50 9.85 861. 1.6 37.19 2.73 1523 . 2.9 38 . 12 4.83 465. · 9 39 . 14 1 · 42 2516. 4.8 40.48 7.98 1673. 3.2 41.63 5.31 AREA NAREA ISPR TIME Farnesane Acyclic C16 Acyclic C18 Primtane Ph~tane O. O.O 0.00 O. 0.0 0.00 346. 13.1 18.52 1232. 46.7 19 · 47 ~062. 40.2 21.08 GMC Data Report No. 150 Page 10/29 P.3t . 2. t9, 2. t. i8.3 ! 22.12 25.93' 2_9.75 33.56 37.37 41. ~8 45. O0 t4.50, m ~.nu'r..e s SANPLE: B6B STUDY WF3641 ANALYZEO: Non Nov 6o 1989 l: 08:35 pm RESULT: /RESULT/WF3641 SAT.RES NETHOD: SAT58906 MIDRIC DATA: WF3641A_SAT #1 SCANS 1 TO 4580 12.,"04/'89 14:6.o:00 CALl: WF~,b41A_SAT #3 CC~HDS.: HP THIN FILM ,RES=NORM ,,.,~,~u=-'"'~ ....: C 1,4988 LABEL: N 8, 4 .... 8 QUAN: A 8, 1 ~ J 8 UH_~. U 2~, 3 '>000 :_::000 4000 '£(:.gH · :,.:,, '..,~:: 5F~: ~:~'.~ _f':,~ ... 48 T .~ r,lE ,.[.1,..1,:. n, 0 0 o nM'ASS CHROMATOGRAMS 2..,'a4/'89 14: 28:.88 SAI'IF'LE: ~,IF3~4IA_SAT DE-NORM COI.!DS,: HP THIN FILM , RES=NORM R[~t.~CE: G 1,4988 LABEL: N 8, DATA: NF3641A_SAT #1 CALl: NF3G41A_SAT #3 4.8 QUAN: A 8, 1.8 J 0 SCANS 1588 TO 4588 BASE: U 28, 3 I l .~ O. 60',) .... ,u.-'~ 4888 45~38 SC:A!.~ ..,,.,: '.',F~ ~,~,: 4A 75' '88 T',, fie MI[.!'IASS CHROMATO~RAMS DATA: WF3641A_SAT #1 SCANS 3000 TO 4500 12/04,"8_q 14:23:00 CALl: WF3641A_SAT #3 SAMPLE: WF3641A_SAT OE-NORM COt~qS.: HP THIN FILM ,RES--NORM RA~]E: G 1,4_~80 LABEL: N 0, 4.8 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 1984 3208 ::;4 ak4 3600 3800 4000 42~'-~0 440E~ = ~' ~: ............... ~ ~,: ~ '1 12768. MIOMASS CHROMATOGRAMS DATA: WF3G41A_SAT #1 SCANS 2588 TO 3588 12/04/89 14:23:80 CALl: ~F3641A_SAT #3 S~I.1PLE: WF3G41A_SAT DE-NORM C:ONOS.: HP THIN FILM ,RES=NORM RANGE: G 1,4980 LABEL: N 8, 4.8 QUAN: A 8, 1.8 J 0 BASE: U 28, 3 386. 217. 065 ± 0. 508 .._ GMC Data Report No. 150 Page 16/29 PETROLEUM GEOCHEMISTRY SATURATE GC SAMPLE NAME INSTRUMENT INJECT TIME METHOD USED RESULT FILE REPORT TIME : B&B STUDY WF3642 : HP 5890 2 Mon Now 6, 1989 2:04:06 /METHOD×SAT5890£.MTH /RESULT/WF3642_SAT.RES : 5:28 PM MON.. 6 NOU.~ pm 1989 CPI UALUE : 1.05 PRISTANE / PHYTANE : PRISTANE / C12 : PHYTANE / C18 : 1.42 C15/C25 : .88 .54 C17/Pr : 1.84 .54 C18/Ph : 1.85 AREA bAREA NALK TIME NORM N-Ci0 N-Cll N-C12 N-C13 N-Ct4 N-Ci5 N-C16 N-Ci7 N-C18 N-C19 N-C20 N-C21 N-C22 N-C23 N-C24 N-C25 N-C26 N-C22 N-C28 N-C29 N-C30 N-C31 N-C32 N-C33 N-C34 N-C35 N-C36 O. 0.0 0.00 0.00 102 . . 3 7.69 . 10 110. .3 9.98 .11 O. 0.0 0.00 O.OO 161. .4 14.05 . 16 982 . 2.5 15 · 90 1.00 4173. 10.6 17.65 4.25 6320. 16.1 19.31 6.44 4482. 11.4 20.88 4.56 3739 · 9 · 5 22.38 3'. 81 2974. 7.6 23.81 3.03 2709 . 6 · 9 25.18 2.76 2386 . 6.1 26.49 2 · 43 1779 . 4.5 27.74 1.81 1244. 3.2 28.95 1.27 1112. 2.8 30.11 1. 13 872. 2.2 31.23 .89 698. 1.8 32.31 .71 558. 1.4 33.35 .57 854. 2.2 34.36 .87 356. .9 35.33 .36 539. 1.4 36.28 .55 1006 · 2 · 6 32. 19 1 · 02 737. 1.9 38.12 . 75 239. 1.9 39.15 ,25 44~. 1.1 40.43 .45 149. . 4 41.99 · 15 AREA ~AREA ISPR TIME Farnesane O. 0.0 0.00 Acyclic C16 145. 1.8 15.25 Acyclic C18 2282. 27.5 18.52 Pri~tane 3443. 41.6 19.46 Phytane 2416. 29.2 21.08 0 N 2.59 P.44 2.29 a. i4 1,99 ~ i.84 . , ~4.50 minutes RESULT: ia.31 aa.ia a5.93 29.75 SAMPLE: 8aB STUDY WF3642 ANALYZED: M0n Nov 6, 1989 /RESUL'r/WF3642 SAT. RES METHOD: 33.56 37.37 4i.i8 45.00 2: 04' 06 pm SAT5890C ~,~.C C, ATA: NF3642_SAT #1 _,~,~,,.~¢r~':~ 1 TO 4588 i iXSlXS~1~.8~:' ~' 88 CALl: NF3~42_SAT ~3 ~._,~ .... ; HP TH]H FILM., K~-~'~HEM R'.A~.I,]~: ~ 1,4SSE~ LABEL: N ~, 4.E~ QLIAH: A ~, ~.8 .J B 8ASE~ ~J 28, 3 i 1764, ~ Z 0 I 100a 16:46 I 3000 · _,0.00 I 66:48 TIME ['ilOi'!ASS CHRO~IATOGRAI'IS DATA: iqF3642_SAT #1 SCANS 1500 TO 4500 ,-~- ~ S ! I.,"(~i,."8~ 17:89:80 CALl: ~,,~,4,__AT ~3 SAMPLE: ~r~--,~ '"' ~'- · HP THIN FILM., RES=NORM ~'-"'~" p .~.qo~ LAE'.EL' H ~, 4 E~ QIIAN: A El, 1 8 J 8 BASE: U 28., 3 F.'.AHGE: ~ 1, ~_,~ ~ ..... R_~ CHROFI~TOC, RAFIS OAT~: WF3642_SAT 1~1 SCANS 2.,u¢ TO ~.¢~,~ 11/C~1/E:9 i7:89:88 CALl: NF~G~.__AT ~3 _,~:',r ~ : CO~'IDS.: HP THIN FILM, RES=NORM RA~SE: G 1,4988 LABEL: N ~, 4.~ m~UAN: A B, 1.~ J ~ BASE: U 0 Z 0 C) HiOHASS CHROMATOGRAMS LH/H. NF3642_SAT #1 SCANS 3888 TO 4588 .~ ..-, ¢. l l/'E~l,."8_~ 17:0S:00 CALl: WF~G4~.__,AT ~3 SAHF'LE: MF3642_SAT ,_.~,~. =.. HP THI~ FILM, RES=~ORM 277. I 1 ?~ £~53 4~1. 0 '5 Z '~* P6TROLEUI1 GEOCHEMISTRY SARA AHALYSIS SAMPLE NAME INSTRUMENT INJECT TIME METHOD USED SEOUENCE RESULT FILE REPORT TIME BEAUFORTIAN WF3643 HPLC FID Fri Oct 27. 19:39 2:45:11 om /METHOO/HPLC FID0.r;TH /OATA/LOOP/SE©UENCE/HP1890 AUTOW.SEO /RESULT/WF3643 SAP.RES 3:10 PM FRI.. 27 OCT.. 1989 Saturates Aromatics Aromatics Polars RESPONSE AREA TIME FACTOR 584. 5 · 29 . 1275E- 03 315 . 9 · 42 . 5470E- 04 1015. 14.:36 .5420E-04 3199. 19.92 .4160E-04 Saturates Aromatics Polars AMOUNT (mo) ~ RESIDUE · 07 26.6 · 07 26.0 · 13 42.5 Saturates Aromatics Polars Asohaltenes OIL 26.6 26.0 47.5 0.0 GMC Data Report No. 150 Page 22/29 0 .64 .8O .57 3.oo 5.ie ?.3? 9.~ ii.?5 t3.93 ~6.~2 minutes SAMPLE: BEAUFORTIAN HF3643 ANALYZED: Fri Oct 27, 1989 2: 45: it pm RESULT: /RESULT/HF3643 SAP.RES METHOD: HPLC FIDO SAMPLE NAME INSTRUMENT INOECT TIME METHOD USED RESULT FILE REPORT TIME PETROLEUM GEOCHEMISTRY SATURATE GC 8&B STUDY ~F }a4~___ ,..,,a'/~ ~ ~ F~ ~ HP_5890_2 Mort Nou 6, 1989 2:59:40 pm /METHOD/SAT5890C.MTH /RESULT/~F3643 SAT.RES 5:30 PM MON. ~ 6 NOU., 1989 CPI UALUE : 1.03 PRISTANE / PHYTANE : PRISTANE ? CI? : ' PHYTANE / C18 : 2. 11 C15/C25 : 2.75 .54 C17/Pr : 1.84 .41 C18/Ph : 2.46 AREA NAREA NALK TIME NORM N-CI0 N-Cll N-C12 N-C13 N-C14 N-C15 N-C16 N-C17 N-C18 N-C19 N-C28 N-C21 N-C22 N-C23 N-C24 N-C25 N- C26 N-C27 N-C28 N-C29 N-C30 N-C31 N-C32 N-C33 N-C34 N-C35 N-C36 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 O. 0.0 0.00 0.00 205. .5 14.05 .08 2469. 6.5 15.90 1. O0 5297. 13 · 9 17.65 2 · 15 7064. 18.5 19.31 2.86 4475. 11.7 20.88 1.81 3177. 8 · 3 22.38 1.29 2612. 6.8 23.81 1.06 2319. 6. 1 25. 18 .94 1929. 5.2 26.49 .80 1307. 3 · 4 27.75 . 53 1005. 2.6 28.95 .41 896. 2.3 30. 12 .36 673. 1.8 31.23 .27 605. 1.6 32.31 .24 559. 1.5 33.36 .23 901. 2.4 34.36 .36 423. 1.1 35.33 . 12 383 . 1 · 0 36 . 28 . 16 468. 1.2 37.19 . 19 356. .9 38.12 . 14 685 . 1.8 39.15 . 28 179. . 5 40.30 . 07 200. .5 42. O0 .08 Farne~ane Ac~clic C16 flcyclic C18 Pri~tane Phytane AREA NAREA ISPR TIME O. O.O O.O0 160. 2.1 15.37 1964. 25.3 18.53 3833. 49.3 19.4]) 1818. 23.4 21.08 GMC Data Report No. 150 Page 24/29 0 0 CD 0 N 0'~ ~ tO 2,77 2:.58 2 2.20 2.02 i.8 18.3i 22.12 25.93 29.75 33.56 37,37 41.t8 i4.50 mlntltes SAMPLE: B~B STUDY -WF-3642-L- ~/-- ANALYZED: Non Nov 6, t989 2: 59:40 pm RESULT: /RESULT/WF3643 SAT.RES. METHOD: SAT5890C 45 MIORIC DATA: WF3643_SAT #1 SCANS 1 TO 4588 li,,'13/89 14:18:88 CALl: WF3643_SAT #3 SAMPLE: WF3643_SAT CONDS.: HP THIN FILM, RES=NORM RAt.~'~E: G 1,4988 LABEL: N 8, 4.8 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 1000 2008 3000 16:40 4.,.'~-'~ · __~.,r.~ 50:00 4008 66: 40 3780. SCAN TIME 1.1IOI.IASS CHROMATOGRAMS DATA: ~F3643_SAT #1 SCANS 1588 TO 4588 11..'13/8~ 14:18:88 CALl: WF3643_SAT #$ SAMPLE: WF3643_SAT COI~OS.: HP THIN FILM, RES=NORM RAHs]E: G 1,4988 LABEL: N 8, 4.8 QUAN: A 8, 1.8 J 8 BASE: U 28, 3 958. / / 857 " ' .... ~ .....' ..... ' -'1 ~ " ~' ~ I' ~ ~" -'~ ~ 1 ~' -i, ~ ~ i" ~ "~ "~ ' I ' ~ i ~ I .~..,88 4888 ~A: 28 G(: 48 382. I I I 217.865 ~ 4588 SCAN 75:88 T I ME MIDMASS CHROMATOGRAMS DATA: WF3643_SAT #1 SCANS 2500 TO 3500 11×13/8B 14:18:00 CALl: WF3643_SAT #3 SAMPLE: WF3643_SAT CONOS.: HP THIN FILM, RES=NORM P, AHGE: G 1,4B80 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J 0 SASE: U 20, 3 374. '? 17' ±217. 065 0. 500 i"~,:' ~ ' ~ I ~~' 8.508'~ .... .,,, l ,,, : . , 2680 28C~0 3000 , 3200 3400 SCAN C 21×i3/8S 14:18:00 S~'~PLE: CO~DS.: HP THIN FIL~, ~N~E: ~ l, 4980 SCANS 8000 TO 4500 20, 3 · 3208 .34E10 - se:oe ~ee 4eee ~ ' 4200 4488 475. 177.85,3 ~: 0.580 1S1.0§? ~ 8.588 fl) 0 0 ·
