Department of Commerce, Community, and Economic Development
Alaska Oil and Gas Conservation
Commission
HOME
EVENTS
DATA
Data List
Drilling
Production
Orders
Data Miner
Document Search
REPORTS
Reports and Charts
Pool Statistics
FORMS
LINKS
Links
Test Notification
Data Requests
Regulations
Industry Guidance Bulletins
How to Apply
ABOUT US
History
Staff
HELP
Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
2018-11-15_318-511
RECEIVED STATE OF ALASKA ALASKA OIL AND GAS CONSERVATION COMMISSION APPLICATION FOR SUNDRY APPROVALS 20 AAC 25.280 NOV 15 2018 1. Type of Request: Abandon ❑ Plug Perforations ❑ Fracture Stimulate R] Repair Well ❑ r""' "00ra?1As'AvJdown ❑ Suspend ❑ Perforate ❑ Other Stimulate ❑ Pull Tubing ❑ Change Approved Program ❑ Plug for Redrill ❑ Perforate New Pool ❑ Re-enter Susp Well ❑ Alter Casing ❑ Other: ❑ 2. Operator Name: 4. Current Well Class: 5. Permit to Drill Number: ConocoPhillips Exploratory ❑ Development ❑✓ Stratigraphic Service El❑ 218-111 3. Address: 6. API Number: P. O. Box 100360, Anchorage, Alaska 99510 50-103-20777-00-00 7. If perforating: 8. Well Name and Number: What Regulation or Conservation Order governs well spacing in this pool? KRU 3S-612 Will planned perforations require a spacing exception? Yes ❑ No 1Z 9. Property Designation (Lease Number): 10. Field/Pool(s): ADL380107, ADL025528, ADL025544 Kuparuk River Field, Torok Oil Pool 11. PRESENT WELL CONDITION SUMMARY Total Depth MD (ft): Total Depth TVD (ft): Effective Depth MD: Effective Depth TVD: MPSP (psi): Plugs (MD): Junk (MD): 19,862' 5,218' 19,854' 5,218' 7,000 Casing Length Size MD TVD Burst Collapse Structural Conductor 120' 20" 120' 120' Surface 3027' 10-3/4" 3027' 2,588' Intermediate 13,866' 7-5/8" 13,866' 2,218' Production Liner 6,161 4-1/2" 19,854' 5,218' Perforation Depth MD (ft): Perforation Depth TVD (ft): Tubing Size: Tubing Grade: Tubing MD (ft): See Attached Schematic See Attached Schematic 4.5" IL80 13,699' Packers and SSSV Type: Packers and SSSV MD (ft) and TVD (ft): Baker Premier Packer 13,569' MD/5,057' TVD 12. Attachments: Proposal Summary Wellbore schematic ❑✓ 13. Well Class after proposed work: Detailed Operations Program ❑ BOP Sketch ❑ Exploratory ❑ Stratigraphic ❑ Development Service ❑ 14. Estimated Date for 15. Well Status after proposed work: Commencing Operations: 12/2/2018 OIL Q WINJ ❑ WDSPL ❑ Suspended ❑ GAS ❑ WAG ❑ GSTOR ❑ SPLUG ❑ 16. Verbal Approval: Date: Commission Representative: GINJ ❑ Op Shutdown ❑ Abandoned ❑ 17. 1 hereby certify that the foregoing is true and the procedure approved herein will not be deviated from without prior written approval. Contact Hanna Sylte, 907-265-6342 Email Hanna.Sylte@ConocoPhillips.com Printed Name Hanna Sylte Title Completions Engineer �p �A y . MI \\ Signature ° Phone 907-265-6342 Date COMMISSION USE ONLY Conditions of approval: Notify Commission so that a representative may witness Sundry Number: Plug Integrity ❑ BOP Test ❑ Mechanical Integrity Test ❑ Location Clearance ❑ Other: Post Initial Injection MIT Req'd? Yes ❑ No ❑ Spacing Exception Required? Yes ❑ No ❑ Subsequent Form Required: APPROVED BY Approved by: COMMISSIONER THE COMMISSION Date: IAJf Submit Form and Form 10-403 Revised 11/2015 Approved applicati R 1n � SAJthe date of approval. Attachments in Duplicate ine 3S-612 Grass Roots Horizontal Multi -Stage Frac'd Infector ConoeoPhiillps Final Wellbore Schematic Cameron 10K 4-%" tree, top joint is 4-%" 12.6# HYD563 New Conductor: Spud Mud 20" Conductor @ 119' 9.6 PPG 3 20 Camco DB Nipple 3.813" I 111 , 192o'Mo 13-1/2" Surface Hole 1 11_Jil 4'/::" x 1 "KBMG with SOV 3,644' MD Surface Casing: 10-3/4" 45.5# L-80 Hydril 563/TXP 3,027' MD / 2,567' TVD @ 55° Eampamael'8S Top of cement 8,270 MD / 3,830' TVD - _ - (250' TVD above the K-3) Top K-3 (Coyote) 9,458' MD / 4,097' TVD 9-7/8" Intermediate Hole Tubing: 4-'/z" 12.6# L-80 Hydril 563 8.6 PPG Keep up witi= — 4'/:"x1"KBMG w/DV m 12,080' MD - _ SLB Gauge Carrier, 13,506' MD 4.5" x 7-5/8", Baker Premier Packer +/- 13,569' MD a 4'h" Camco Dn Nippie 3.75" nogo 9 13,633' MD 7-5/8" x 4-%a" Baker Flex Lock Liner hanger ZXP liner top packer w/ RS Nipple, @ +/- 13693' MD Intermediate CasingSet-25' TVD above to Moraine: p �Top ofMoraine 5,104'ND:':'::'"'':':' '' 7-5/8" 29.7# L-80 Hydril 563 866 MD / 50 1 4' TVD @ 77° ...:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.: 4'/z" Swell Packer ...............:..........:.:.:.:.:.:.:.:. Section 1 -Affidavit 10 AAC 25.283 (a)(1) Exhibit 1 is an affidavit stating that the owners, landowners, surface owners and operators within one-half mile radius of the current or proposed wellbore trajectory have been provided notice of operations in compliance with 20 AAC 25.283(a)(1). ConocoPsphilli Alaska To: Operator and Owners (shown on Exhibit 2) Re: Notice pursuant to 20 AAC 25.283 (1) 3S-612 Well Kuparuk River Unit, Alaska ADL 380107, KRU Tract 150; ADL 380106, ADL 25528, KRU Tract 147 Dear Sirs: Paul K. Wharton Staff Landman P.O. Box 100360 — Suite ATO 1482 Anchorage, Alaska 99510-0360 Phone (907) 263-4076 Paul. K.Wharton@conocophillips.com KRU Tract 146; ADL 25544, KRU Tract 149; and ConocoPhillips Alaska, Inc. ("CPAI") as Operator and on behalf of the Kuparuk River Unit ("KRU") working interest owners, hereby notifies you that it intends to submit an Application for Sundry Approvals for stimulation by hydraulic fracturing pursuant to the provisions of 20 AAC 25.280 ("Application") for the 3S-612 Well (the "Well"). The Application will be filed with the Alaska Oil and Gas Conservation Commission ("AOGCC") on or about November 14, 2018. This Notice is being provided pursuant to 20 AAC 25.283. The Well has been drilled as a directional well as shown on the attached plat (Exhibit 1). Exhibit 1 shows the location of the Well and the lands that are within a one-half mile radius of the current proposed trajectory of the Well, including the reservoir section ("Notification Area"). Exhibit 2 is a list of the names and addresses of all owners, landowners and operators of record of all properties within the Notification Area. Upon your request CPA[ will provide a complete copy of the Application to you. If you require any additional information, please contact the undersigned. Very truly yours, Paul Wharton Staff Landman cc: Hanna Sylte Rebecca Swensen 3S-612 Hydraulic Fracturing Notice Letter November 14, 2018 Page 2 Exhibit 1 3S-612 Hydraulic Fracturing Notice Letter November 14, 2018 Page 3 Exhibit 2 Mineral Owners: Operator: ConocoPhillips Alaska, Inc. 700 G Street, Suite ATO 1226 Anchorage, AK 99501 Attention: Misty Alexa, Manager, NS Development Operator ADL 355038 Caelus Natural Resources Alaska, LLC 3700 Centerpoint Drive, Suite 500 Anchorage, AK 99503 Non -Operators: BP Exploration (Alaska) Inc. 900 E. Benson Boulevard Anchorage, AK Zip 99508 Attention: Mr. Weston Nash Chevron U.S.A. Inc. 1400 Smith Street Room 40116 Houston, TX 77002 310 Attention: Dave White ExxonMobil Alaska Production Inc 3700 Centerpoint, Suite 600 Anchorage, AK 99503 Attention: Mr. Jamie Long Non -operator ADL 355038 Eni Petroleum US LLC 1200 Smith, Suite 1700 Houston, TX 77002 Surface Owners: State of Alaska Department of Natural Resources Division of Oil and Gas 550 West 7t" Avenue, Suite 1100 Anchorage, AK 99501-3560 Attention: Director TO THE ALASKA OIL AND GAS CONSERVATION COMMISSION Before the Commissioners of the ) Alaska Oil and Gas Conservation ) Commission in the Matter of the ) AFFIDAVIT OF Paul K. Wharton Request of ConocoPhillips Alaska, Inc. for ) Hydraulic fracturing for the 3S-612 well ) under the Provisions of 20AAC 25.280 ) STATE OF ALASKA THIRD JUDICIAL DISTRICT i §§ Paul K. Wharton, being first duly sworn, upon oath, deposes and states as follows: 1. My name is Paul K. Wharton, and I have personal knowledge of the matters set forth herein. 2. 1 am Staff Landman for the well operator, ConocoPhillips Alaska, Inc. ("CPAI") 3. Pursuant to 20 AAC 25.283 (1) CPA[ prepared the attached Notice of Operations ("Notice"). 4. On or about November 14, 2018, CPAI sent a copy of the Notice by certified mail to the last known address of all other owners, landowners, surface owners, and operators of record within a one-half mile radius of the current proposed well trajectory. Subscribed and sworn to this 141h day of November, 2018. X -&/�1 � STATE OF ALASKA Paul K. Wharton ) H THIRD JUDICIAL DISTRICT ) This instrument was acknowledged before me this 14th day of November, 2018, by Paul K. Wharton. Notary Public, State of Alaska STATE OF ALASKA REBECCA SINENSEN My Commission Expires Aug. 27, 2020. Section 2 — Plat 20 AAC 25.283 (a)(2) Plat 1: 3S-612 Landowners 2G '' ) Frac Points i Well Trajectory ADL355038 Open Interval CO Half We F.ac Point Radius ® Half e.fse Nell Trajectory Red his - r— — .._ — — — — —. _ — - — CPAI Lease q L ASRC Lease > r- J Caelus Lease qo 71.Y L �J 01 p! \ " ADL025528 3 ; ,, IY j i 434 _ o ADL380106 1 CO I � � as i 3g-11 P s w M� 1 Cp 38-620 A 3S.18 26 3519 1 3S-613 3S-22 1 3S'0B I 23P 3� 3523 3S-06A 1 • p i97 ADL025544 I ADL380107 �5ry ConocoPhillips Alaska 3S-612 Lease Plat 11/13/2018 r ._._._.]0 0.2 0.4 0.6 Miles II Table 1: Wells within .5 miles Wells within 1/2 mile buffer of well track * Data from SDE laver: AK WELL BOTTOM TD ATDR DDR3 Well In Frac Point API WELL NAME Status Type Radius 501032045800 3S-03 ACTIVE PROD 501032045400 35-06 PA INJ 501032045401 3S-06A ACTIVE INJ 501032043000 3S-07 ACTIVE PROD 501032045000 35-08 PA PROD 501032045001 3S-08A PA PROD 501032045002 3S-08B PA PROD 501032045003 3S-08C ACTIVE PROD 501032043200 35-09 ACTIVE INJ 501032044000 35-10 ACTIVE PROD 501032043900 3S-14 ACTIVE INJ 501032044400 35-15 ACTIVE PROD 501032044500 3S-16 ACTIVE INJ 501032044800 35-17 PA INJ 501032044801 3S-17A ACTIVE INJ 501032043300 35-18 ACTIVE PROD 501032046000 35-19 ACTIVE PROD 501032045200 35-21 ACTIVE INJ 501032044600 35-22 ACTIVE INJ 501032045300 3S-23 PA PROD 501032045301 3S-23A ACTIVE PROD 501032045600 3S-24 PA PROD 501032045601 3S-24A ACTIVE PROD 501032036101 3S-26 ACTIVE INJ 501032077400 35-611 ACTIVE PROD 501032073500 3S-613 ACTIVE INJ 501032069500 35-620 ACTIVE PROD 501032069900 MORAINE 1 PA EXPLOR 501032066000 NDST-02 SUSP EXPLOR 501032066070 NDST-02PB1 PA EXPEND 501032064500 NUNA 1 SUSP EXPLOR 501032064570 NUNA 1PB1 PA EXPEND 501032036100 PALM 1 PA EXPLOR Yes Yes Yes Yes Yes Yes Yes SECTION 3 — FRESHWATER AQUIFERS 20 AAC 25.283(a)(3) There are no freshwater aquifers or underground sources of drinking water within a one-half mile radius of the current or proposed wellbore trajectory. See conclusion of the Aquifer Exemption Title 40 CFR 147.102(b)(3) "The portions of aquifers on the North Slope described by a % mile area beyond and lying directly below the Kuparuk River Unit oil and gas producing field" as exempt freshwater aquifers under 10 AAC 25.440" SECTION 4 — PLAN FOR BASELINE WATER SAMPLING FOR WATER WELLS 20 AAC 25.283(a)(4) There are no water wells located within one-half mile of the current or proposed wellbore trajectory and fracturing interval. A water well sampling plan is not applicable. SECTION 5 — DETAILED CEMENTING AND CASING INFORMATION 20 AAC 25.283(a)(5) All casing is cemented in accordance with 20 AAC 25.52(b) and tested in accordance with 20 AAC 25.030 (g) when completed. See Wellbore schematic for casing details. SECTION 6 — ASSESSMENT OF EACH CASING AND CEMENTING OPERATION TO BE PERFORMED TO CONSTRUCT OR REPAIR THE WELL 20 AAC 25.283(a)(6) Casinq & Cement Assessments: The 10-3/4" casing was cemented on 10/27/2018. The cement job was pumped with 80 bbls MPII and 509 bbls of 11 ppg lead cement, this was followed by 64 bbls of 12 ppg tail cement and displaced with 9.9 ppg mud. The plug bumped at 850 psi and the floats were checked and they held. The 7-5/8" casing cement report on 11/4/2018 shows that the job was pumped as designed, indicating competent cementing operations. 12.5 ppg MPII was pumped before dropping bottom plug, this was then chased with 303 bbls 15.8 ppg Class G cement and dropped top plug. This was chased with 9.5 ppg LSND mud. Full returns were seen throughout the job. The plug bumped at 1500 psi. Summary All casing is cemented in accordance with 20 AAC 25.030 and each hydrocarbon zone penetrated by the well is isolated. Based on engineering evaluation of the wells referenced in this application, ConocoPhillips has determined that this well can be successfully fractured within its design limits. SECTION 7 — PRESSURE TEST INFORMATION AND PLANS TO PRESSURE -TEST CASINGS AND TUBINGS INSTALLED IN THE WELL 20 AAC 25.283(a)(7) On 10/28/2018 the 10 & 3/4" casing was pressure tested to 3000 psi for 30 mins. On 11/14/2018 the 7 & 5/8" casing was pressure tested to 3850 psi. The 7 & 5/8" casing will be pressure tested to 3,850 psi prior to frac'ing. The 4.5" tubing will be pressure tested to 4,100 psi prior to frac'ing. AOGCC Required Pressures [all in psi] Maximum Predicted Treating Pressure (MPTP) 7,000 Annulus pressure during frac 3,500 Annulus PRV setpoint during frac 3,600 7 5/8" Annulus pressure test 3,850 3 1/2" Tubing pressure Test 4,100 Nitrogen PRV 8,550 Highest pump trip 8,050 SECTION 8 — PRESSURE RATINGS AND SCHEMATICS FOR THE WELLBORE, WELLHEAD, BOPE AND TREATING HEAD 20 AAC 25.283(a)(8) Size Weight Grade API Burst API Collapse 10 & 3/1' 45.5 L-80 5,210 psi 2,470 psi 7 & 5/8" 29.7 L-80 6,890 psi 4,790 psi 4.5" 12.6 L-80 8,430 psi 7,500 psi Table 2: Pressure Ratings Stimulation Surface Rig -Up Bleed ) Tatpa Tale Tank d V C 7 42 Y a` y J .Y U d i dwnd U 9l L7 Pop -Olt Tank CA ry � OL ry. • Minimum pressure rating on all surface treating lines 10,000 psi • Main treating line PRV is set to 95% of max treating pressure • IA parallel PRV set to 3600 psi • Frac pump trip pressure setting are staggered and set below main treating line PRV • Tree rated to 10,000 psi Pump TruO Noter Dimensional InformaLion reflected on this dra,*ing are estimated measurements orky- 5 6 - 19'4 " 10K Frac Tree 4-111G" 10.000# 4-1116' MOON 4-11I6" 10.000# I�ydrzufic 4-11,16" 10A.'Mi'l 4 " 10K Valre + Tree Cap - 39-F I,. iIOK Valve + 4" 10K x 4" it M 1:2 - 32.25" I 10 CO JDF 91%1 Oil I 'IS '12 11 WE Site 2S- 10K Frac Tree 661, 4-1/16- 10,0004 icose 'mrr, Frac Tree 2" 1502 Weight of entire tree is -6,2&frs 4" 10K F-WO Valves --560 Is Tree Cap -250 Ibs C'CAMERON SECTION 9 - DATA FOR FRACTURING ZONE AND CONFINING ZONES 20 AAC 25.283(a)(9) CPA[ has formed the opinion, based on seismic, well, and other subsurface information currently available that: The fracturing zone, the Torok "Moraine" reservoir, has an average thickness of approximately 280 ft TVD over the course of the lateral section of the 3S-612, from where it intersects the top formation at 13,948 ft MD to TD of the well. The Torok is comprised of thinly interbedded sandstone, siltstone, and mudstone layers. The sandstone and siltstone components are litharenites, moderately to well sorted, and very fine grained. The mudstones are composed of clay -rich, moderately to poorly sorted silt and mud grains. The estimated fracture pressure for the Moraine interval is=12.5-13.5 ppg. The overlying confining interval of the Torok Formation consists of mudstone and siltstone with an average thickness of =1,000 ft. TVD. The top of the Torok confining interval starts at 4,039 ft. TVDSS (9,471 ft. MD). The estimated fracture gradient of the overlying Torok formation is =0.82 psi/ft. The underlying confining zone consists of lower Torok, HRZ, and Kalubik shales totaling approximately 500' TVD. The estimated fracture gradient for this section ranges from 15-18 ppg, with the gradient increasing down section. The top of the HRZ is estimated to be at approximately 5,550 ft TVDSS at the heel, and approximately 5,540 ft TVDSS at the toe of the well. (no MD as the HRZ is not penetrated in the 3S-612 well). SECTION 10 — LOCATION, ORIENTATION AND A REPORT ON MECHANICAL CONDITION OF EACH WELL THAT MAY TRANSECT CONFINING ZONE 20 AAC 25.283(a)(10) The plat shows the location and orientation of each well that transects the confining zone. ConocoPhillips has formed the opinion, based on following assessments for each well and seismic, well, and other subsurface information currently available that none of these wells will interfere with containment of the hydraulic fracturing fluid within the one-half mile radius of the proposed wellbore trajectory. Casing & Cement assessments for all wells that may transect the confining zone: 3S-611: The 7-5/8" casing cement report on 10/13/2018 shows that the job was pumped as designed, indicating competent cementing operations. 12.5 ppg MPII was pumped before dropping bottom plug, this was then chased with 270 bbis 15.8 ppg Class G cement and dropped top plug. This was chased with 9.4 ppg LSND mud. Full returns were seen throughout the job. The plug bumped at 1500 psi. 3S-620: The 7 & 5/8 casing cement pump report on 2/6/2015 shows that the job was pumped as designed, indicating competent cementing operations. The cement job was pumped with 15.8 ppg cement, displaced with 9.7 ppg mud. The plug bumped at 1,000 psi and the floats were checked and they held. 3S-613: The 7-5/8" casing cement report on 5/2/2016 shows that the job was pumped as designed, indicating competent cementing operations. 12.5 ppg MPII was pumped before dropping bottom plug, this was then chased with 15.8 ppg cement and dropped top plug. This was chased with 9.3 ppg LSND mud. Full returns were seen throughout the job. The plug bumped at 941 psi and the floats were checked and they held. NDST-02: According to the Pioneer Natural Resources job log on the AOGCC website, the 7- 5/8" casing was cemented on 2/9/2013. The cement report indicates that the job was pumped with 60 bbl 15.8ppg Premium Cement. Full circulation was seen throughout the job. The plug pumped at 3500 psi and the floats were checked and they held. Source: http://aogweb. state. ak. us/WebLink/DocView. aspx?id=43019&searchid=d7567104- bOf6-4da3-b564-d294f7b6ed84&dbid=0&cr=1&cc=1#, Page 108 NDST-02PB1: According to the Pioneer Natural Resources job log on the AOGCC website, the top plug was pumped in NDST-02PB1 on 1/31/2013. The plug was pumped with 254 sx of Premium Cement with full returns throughout the job. The TOC was tagged at 8,012'. Source: http://aogweb. state. ak. us/WebLink/DocView. aspx?id=43019&searchid=d7567104- bOf6-4da3-b564-d294f7b6ed84&dbid=0&cr=1&cc=1#, page 110 Nuna 1: According to the Pioneer Natural Resources job log on the AOGCC website, the 7- 5/8" casing was cemented on 2/16/2012. The cement report indicates that the job was pumped with 192 sx 15.8ppg Class G cement. Partial returns were seen. Source: http://aogweb. state. ak. us/WebLink/DocView. aspx?id=39505&searchid=edb77d4c- f03e-451 e-ae3b-baa6eeea8f35&dbid=0&cr-1 &cc=1 #, page 201 Nuna 1 PB1: According to the Pioneer Natural Resources job log on the AOGCC website, the top plug was pumped in Nuna 1 PB1 on 2/10/2012. The top plug was pumped with 280 sx of Premium Cement. Firm cement was encountered at-5766'. Source: http://aogweb. state. ak us/WebLink/DocView. aspx?id=39505&searchid=edb77d4c- f03e-45le-ae3b-baa6eeea8f35&dbid=0&cr=1&cc=1#, page 201 O ro L Q O 4-J ro v^ J, W L u f0 L L.L 'm 0 m 0 0 c ~ auo 0 Q 10 � n F � a • c « c OD N vKi N 3 E m„ 3 E E o- �- O 00 0° E a °0 E U E E >> E E E C eNi u eNi lJ N Y o. E N O O f O f A N O � W — iom om a m N AO E E m m t m U U a m O O p u0 H 44 4 v a u w o n a v K a r L N N L C p W n O C O E a a 0 a 0 d a c H N m O N FO N C a V O O � 0 � rci N rcl n Kf x + • a c a n 0 0 O N H v u v v v a0� 0 O Y � � O �"' W O O) N lN0 ♦ � s � a 0 a N C U OD N r OD tll r W N r 00 11 r L 00 N n C N Q Q Q N N W ei c 3 m m m z H Z Z 2 SECTION 11 — LOCATION OF, ORIENTATION OF AND GEOLOGICAL DATA FOR FAULTS AND FRACTURES THAT MAY TRANSECT THE CONFINING ZONES 20 AAC 25.283(a)(11) CPAI has formed the opinion, based on seismic, well and other subsurface information currently available that there is a single fault that transects the Torok oil pool within one half mile radius of the wellbore trajectory of the 3S-611 well. This fault was encountered during the drilling of the offset 3S-611 wellbore (as detailed in the table below). No faults were encountered during the drilling of the subject 3S-612 well. This fault is interpreted to not extend up through the confining interval. CPAI has formed the opinion, based on seismic, well, and other subsurface information currently available that the fault will not interfere with containment. Well Name Depth MD (ft) Depth TVDSS Vertical Losses (bbl/hr) (ft) Displacement ft 3S-611 17,517 5,173 10 None Plat 2: Fault Analysis v V ,II 1 L 010 t 0. 7 IY i i DL390434 I i 1 i I I 1 i i 1 i I I kDL39069,7 i i ADL025544 10) Frac Points Well Trajectory ADL355038 Open Interval Faults within Frac Point Radius ry Y Wells within Frac Point Radius .......................... Half Mile Frac Point Radius QHalf Mile Well Trajectory Radius CPAI Lease ASRC Lease t L _ � Caelus Lease A D L025528 ADL380106 _ _ IADL380107 Conoco -Phillips Adaska 3S-612 N Fault Analysis �- - 0 0.2 0.4 0.6 11/13120111 �025551 i Miles SECTION 12 — PROPOSED HYDRAULIC FRACTURING PROGRAM 20 AAC 25.283(a)(12) 3S-612 was completed in 2018 as horizontal injector in the Torok formation. The well was completed with 4.5" tubing and a 4.5" liner with ball actuated sliding sleeves. After the 1 st stage we will shift a sleeve to close off that section of the lateral. We will then pump the 2"d stage and drop a ball (progressively getting larger) after each remaining stage, these balls will provide isolation from the previous stage and allow us to move from the toe of the well towards the heel. Proposed Procedure: Halliburton Pumping Services: (Torok Formation Frac) 1. Conduct Safety Meeting and Identify Hazards. Inspect Wellhead and Pad Condition to identify any pre existing conditions. 2. Ensure all Pre-frac Well work has been completed and confirm the tubing and annulus are filled with a freeze protect fluid to 2,000' TVD. 3. Ensure the 10-403 Sundry has been reviewed and approved by the AOGCC. 4. MIRU 22 clean insulated Frac tanks, with a berm surrounding the tanks that can hold a single tank volume plus 10%. Load tanks with 1001 F seawater (approx. 29,000 bbls are required for the treatment with breakdown, maximum pad, and 450 bbls usable volume per tank). 5. Ensure lift �+plan is reviewed and signed prior to RU of Frac equipment requiring lifts. P. MIDI RU HES FIQV EglllplllCllt. 7. PT Surface lines to 9,000 psi using a Pressure test fluid. 8. Test lA Pop off system to ensure lines are clear and all components are functioning properly. 9. Pump the -500 bbl breakdown stage (30# Hybor G) according to the attached PDF HES pump schedule. Bring pumps up to maximum rate of 40 BPM as quick as possible, pressure permitting. Slowly increase annulus pressure to 3,500 psi as the tubing pressures up. Ensure sufficient volume is pumped to load the well with Frac fluid, prior to shut down. 10. Perform a hard shut down, Obtain ISIP and fluid efficiency estimates. 11. Pump the Frac job by following schedule with a maximum expected treating pressure of 7000 psi. 12. RDMO HES Equipment. Freeze Protect the tubing and wellhead if not able to complete following the flush. 13. Well is ready for Post Frac well prep for flowback (Slickline and possibly CTU). ConocoPhillips discloses that it will be using Chemical Frac Tracers and Oil Frac Tracers for tracing purposes in the concentrations detailed in the attached ProTechnics Hydraulic Fracturing Fluid Product Component Information Disclosure. In support of this application, ConocoPhillips provides the front page of the Core Lab/Protechnics' MSDSs for each of the chemical additive, as well as the Hydraulic Fracturing Fluid Product Component Information Disclosure provided by Core Lab/Protechnics. Core Lab/Protechnics will supply the AOGCC with additional chemical disclosure information for the proprietary additives listed in the Hydraulic Fracturing Fluid Product Component Information Disclosure f V) v L � c U lD r-I N N N r-I N 61 r-1 00 r-I d' N .--I N Ln N I- rV 00 N lD m N N N rV N N N N N N NLL N bO O O O O O O O O O O O O Q S bO = aJ L l0 m rV m N m N m 00 N 00 N 00 N O �t 00 N 00 N 00 [V N m 73 N N N N N N L"V N N N N N U M LL 4L O O O O O O O O O O O O QJ + Q b0 al m N m m m m m Ln m Ur m (10 cn L r) m m m m m m m M m c- a: C)— a- p d N l0 O 00 N l0 IZI, 00 N l0 9.0 1l- O 00 O 00 O al O al O O r-I O r-i r-I r-I r-I r-I N r-I N r l N r q Q Lr1 Lr7 Lr1 Lri Lr1 Lrj Lr Lrj Ln Lr Lrj Lr� H rH r-I �F O p u1 r� m l0 cl Ol m Ln cl I- m O rn R c» n cl al m I- cl w m � ai c--I ai ri 00 ri 00 ri I� c-i rl c1 kJo ri Lo ri Ln ri Ln c-I e-i It r-I .Q — O O O O O O O O O O O O N O r O N O rV O N O N O N O N O N O N O N O N O N r- O r- O r- O rl O ri O ri O ri O n O n O n O O O 0 N N N N N N N N N rV N N Ul aU 4O r-i N m c* Ln l0 1` 00 al O r-I N ri V).1 aJ U 0 Z L- ai E m U N 0 O +V) LnLn 7 rC0 LJ L C — r0 V) f0 - !� U U M fD C C O O O V) O O � W L � U � C LJ N 0 Q O L 0 0 C C L VI tO .- C c O E v V) Ln 3 Ln :E � � v O *' N N cu bn c c � aj 0 bn -0 p O O E +- E aj a) v v z aj 4- N > to (n M ,C: C � � O O Q L L Q = aJ N Ln N O .CL U = Vf - C bn t C 0- 0 O Ln � O } v U L O _ 4O O a� 12 o L U C O N a, E � L N a) N aJ t t' C 4� N CU 3 O t O 4% `0 L oc E aj m a t Ln v m ►— �' m E Q q N N i/Of N ry N VOi A q N N N N N N N N N N lV N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N 6 6 6 6 6 0 6 o a 0 0 0 0 0 0 0 o 6 0 6 6 6 o O o 0 o o o 0 0 0 0 0 0 0 0 0 0 0 6 0 0 0 0 0 0 0 0 0 I? $ oo 0 0 0 0 0 0 o S o 0 o 0 0 0 0 0 0 00 0 0 0 0 0 a 0 0 0 cV 0 0 0 0 0 ¢ a m cV N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N O -4 N N N N N � m` ti o 0 o N ti O O o 0 0 6 .N-i 0 0 N ti 0 0 N 0 0 H eN1 0 0 .N-1 eN-1 6 0 eT-I .Ni 0 0 6 a o 0 .Ni 0 H eNi 0 0 eNi eN+ 0 0 N H 0 0 eNi ti O N o 0 cc; o O o 6 0 .N-i - O O O O 0 0 O o 0 0 0 0 0 a O S 0 0 0 0 0 0 0 0 0 0 0 0 O O o o O O o 0 O 0 0 O O 0 0 O O 0 0 O O 0 0 O O 0 0 O O O S O O O 0 0 O O 0 0 O O 0 0 O O 0 0 O O 0 0 o o 0 0 0 0 0 0 0 0 O 0 0 0 0 66 0 m m m 0 0 m m 0 0 m m DO0 m 0 6 m m 0 DO m m O m m 0 m 0 0 0 0 0 0 6 0 m 0 0 m m 0 0 m 0 m o O M m m O m O m m 0 o 0 0 m m 0 0 m 0 m va o 0 $ O 0 Oo N N N N 6 N N N N N Vt 6 6 6 6 N N N N a a v v v v v e o Q 0 o O O o o 0 0 0 0 0 0 o O o 0 0 o O O o O o O O O o 0 o O O O O O o O o 0 0 O O U ¢ -^ y m rn m m rn m m rn m m rn m o �i rn 0 0 m m 0 0 m rn 0 m 0 rn 0 0 m m 0 0 m rn m rn rn m m m 0 m rn 0 0 m m 0 0 m m 0 0 m m 0 o m m rn rn m m m o rn m m m v o 0 0 o Q 0 o o 0 o o o 0 0 o 6 o 0 0 0 0 0 0 0 a 6 o 6 o 6 o 0 0 o 6 6 6 0 6 0 0 0 0 ^ y ow ow 0 w 0 o w w ow ao 00 0o a o w w a o w w ow ow 0 ow oo o0 00 00 oro ow o ow w ao ow 0 ow w o 0 w w 0 0 w w 0 0 w w 0 0 w w 0 0 w w o w 0 0 w w 0 0 w w 0 0 w w 0 0 w w 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 no 't Ot 6 0 0 0 rl 0 0 0 O O 0 O o 0 0 0 0 0 o 0 0 0 0 0 0 0 0 H 0 O F H e+ 0 0 O O H H 0$ O o 0 o o 0 0 o 0 0 0 o o 0 0 0 00 0 0 0 0 0 0 o 0 O a o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 .-� H 0 0 0 e+ 0 0 0 0 0 0 0 0 0 O E E N V O N N O N H N O H O H rn d 0 m m N V N rn O N m N m o Q N rn T M N Q N N d .. N d .. w O d 00 N H .. V N I .. r d N O N w O N .-1 O H d 00 N H rn d N H N d N N O O N w w O h N N N N .. E c~ L L H H m r N o 0 r N VNt 0 0 w N m T 0 0 N M N H 0 0 lD 0 0 0 O r vNl d O O M tOD 0 0 ...... 0 0 rn d 0 0 rn 0 0 O N N 0 0 N N a 0 0 0 0 0 0 0 0 O o r 0 0 O(0 0 0 N 0 0 0 0 d 0 0 0 O t� O O O tD O O O O rn O O N 0 0 O VO O VO O N In NO In w0 O N Or dh� m N N rO oM Or rd 0 m a ldMD 0 NO E mF E m H 0 m D 0 0 N O N S O o d o O 0 o 6 6 0 0 o 0 ti 0 0 0 0 0 d d o 0 d O O 0 0 O O O 0 0 M H O 0 0 O O 0 0 O O 0 0 7D d M O OO 0 0 0 OAi 0 0 H O 0 0 0 0 0 0 d 0 0 0 0 dNd 0 0 0 0 0 0 0 0 C 0 0 00 0 0 00 o a o 0. 0 0 o o o Q a o o o. 0 0 S O 0 0 O O 0 0 O 0 0 0 0 o 0 0 0o o d o a o 0 0 0 0 o 0 o 0 0 d o 0 O O F` N O O O O O N S O O O 0 0 0 N o O N S 0 0 0 0 c 0 N o O O O O -m N l0 m V w N d N r b ti N N M QQ r V Q N Q r tD V r d V rl N O r N O n V ' E L` d o d M1 �D w w t0 Q N w M- O N r b w N N d N w M w N- N M tD Q w M1 O Q N N N M1 d N t0 Q1 w d� w N m N N m N M b d� S m M M d M1 N N w rn w d w t(1 Ge0 m N N N N wW N O N �y tD -- Q Q M - tD H H H N N H N N tp H N N N N l0 H H N H L N tD N D1 w w N N M1 w w M Q lD rn ti w Q M1 N N 3 W N N tD N Q Q N N tD H H H H N N N N • J p o 0 m o 0 w 0 o 0 0 S o 0 0 O no 0 0 n pppp o 0 O o m o m o o o 0 0 0 o dm o o ' o w o o o S S d++ S c o 0 0 0 0 0 `r' o W p 0 0 �� O O O o w O N d O w O 0 0 0 0 0 w 0 r! 0 0 0 w 0 O w 'r d O w j �' H N .y ti N .� eH-1 N tD t0 M1 W w r 1p c-I t0 l0 n M W n t0 '-I N m tp r w W n t0 �-1y N b �D h w w r 1p 0 0 0 0 0 0 0 0 0 0 0 f a p� p D o 4 o` N N O o 0 O O .-i N 00 00 nl V 0o N N o 0 0 0 0 0 0 0 0 0 0 O. o 6N rtt O O m N 0 0 0 0 0 0 0 N O 6fV C0 0 O M 0 0 V Lei 0 0 O tp Ih C 0 _ L �E 0 0 d d 0 0 0 0 d d 0\\ 0 d L E � O O d Q \\ N iV O O d d ON N O O Q fo\V O O Q N E E O L d E\\\\\\\ � O V d O d O O O d d N O L d E E O N O O d d O O N N O a d d O N l O O d d N O N O L Q E 0 � O O d d 0 0 O O d Q 0 0 O O d d 0 N 0 o g oo c c c c c o c c ro c c c o0 0o c c 2 2 c c c o c c c c c c c o c c c c c c c ao H 33333 �333333 `' 3333333 `"3333333 `'3333333 -p -2 a a a a a a -o p a -p L3 -p v -p _ = — — C — — LL C W — C w O LL LL L W W LL LL C U1 W LL LL C C W W LL C W m N O ~ W a — C � — — C LL W — — LL w W N — — w c W w O L LL — G LL W c c W — LL c N W m O. — c — — c c — — C C — — c C O N Q m m m N a 6 N 0 0 0 0 o m O o 0 0 0 0 0 o N o o 0 0 0 oo a o - o`., aD aO aD ap nD no n na n a o c l7 C7 C7 (7 (7 l7 l7 l7 C7 U' (9 l7 C7 l7 V l7 U' l7 l7 o u o o o o o U' (7 3 o o' Q (D o w 'D Q u o (.9 U' o o (7 o o o o l7 (9 Z `o `o o o o o 0 0 0 o o o o o o O o W- 0 0 0 o o 0 0 0 0 0 0 0 o 0 0 0 0 o a o 0 0 0 0 0 0 0 0 0 0 o a a Q LL v x x 1- L 1 1 2 2 1 1 x 2 a x 2 .D a x x .n x x .n x S a s x 2 .o n x x a c x re v x .a x 2 a x x x 2 x x 2 2 2 x x 2 2 x x 2 x. S m m m S m m m S S a J y xc a o m u x a u xi x xc u x se xe xe xo v x xc x u u yc u x xc xc xc xx at xc ac x rx xe xc u u xc o xc �x yc u �c x o Q p[ M M M M M T M M M M M m M T M T m M ml O ry m v NE to ql H tDr w1 q] � m H rnn M H N N N N N N N T d N N Z �o S9L 7l SrM - VrM Nei 'A, 99L u crat - ZvEst � A. M u 9989L - 1989L @� J. 9% J. E 2 UUM-Moto 99L 31 L98Lt- 999Lt @7 _ auieioW aweaoW t leniatul Z Ien,a;ul ouiejow £ lenlatul ouiejow auiejow tv"olul lurealul Q n .n In N N o N ( N N N N N N N N N N N N N N N N N N N N N N A m O O O O p C O O 6O O O O O O O O O O O O O p o 0 O O O O 0 0 0 O O o 0 0 0 0 0 0 0 0 0 Q O O 0 0 0 0 0 W 'd U 0 0 0 0 0 S 0 o S o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 a 0 0 0 0 ¢ Q m Q N N N N N N N N N N N N N N N N N N N N N NI N N N N N N N N N N N N N N N U Fy s a �M-I o em-1 e�'1 0 0 rN-1 a -I 0 0 rN-I eM-1 0 0 ��-1 t�-I 0 0 s'M t�-1 0 0 cal N o d ti e�l o 0 N 0 0 N M 0 0 eNi N 0 0 cMi tvi 0 0 ti e�1 0 0 � '�-1 0 0 r�-I e�-I 0 0 r�-1 aN-1 o 0 � 0 eM-I N 0 0 N N 0 0 N N 0 0 0 0 chi 0 0 N 0 o N tNi ci o cN'1 cNi 0 0 e�-I rm-I 0 0 N eNi 0 0 e�-I eMi 0 0 - o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 o S o S o S o 0 0 0 0 o a o 0 0 p o m M o m 0 0 m m o M m o o m m m o m m o m o m m 0 0 m m o m m m m m m m m m m m m m m m m m m m of o m o o m m 0 0 m m o m m oz 0 0 vll tt1 Y) M N N N N 1A N N N VI In Yl In v1 M N V1 VI in N a V m ltlVt o V �I1 O V N C V V a o 0 0 0 0 0 o a d o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 0 o d o a o 0 0 0 0 0 0 0 0 o b m m m m m m m m m m m m 0 m m 0 0 m m 0 b m m g q m m 0 0 m m S S S b m b b m m m m o m m m m 0 0 m m 0 0 m m o m �i 0 0 m m 0 0 or m o a 3 O O O O O O p O O Cl O o 0 0 0 o.. 0 0 0 0 0 0 o b 0 0 0 0 0 O O o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 b o 0 0 n ro m oo co co m 0 m w 0 ca 00 ow ro m O O m m O m m ro 00 0 0 m m 0 0 W co O ro w b 0 m m 0 0 m m Ow OM 0 0 w m o0 o 0 00 m S 0 o� 0 0 ro w 0 0 m m 0 0 w a 00 m0 O oo 00 O w o 0 o 0 0 0 o o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o b o 0 0 0 0 0 o0000 000 0 0 o 0000 0 0 0 0 0 o S o 0 g 0 0 0. 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o o I ti c+ .-i .+ .y r+ a .+ in o o vmi 1 v o m n ry .� o In oo o Ln .+ .+ v vl o .+ m n N v N o �n ry o a o v m N m ro a .� n m o o m o o 0 m m n o o .+ o o m m w E F ri r`i M V 0 oo V N m N N ao m .y fi m v O O o": O V i 1 V N r+i N N 1 m a+ v O 0 O VI io o i6 N oco 0o .�i 0 v o 0 0 .. vrvj VNt .. o o .O-I .mi o v .. 0 0 N V V I N N o N H m N o v 0 0 _.. 0 0 0 0 0 0 0 0 0 0 0 0 61 0 0 0 0 0 0 0 0 0 0 6 o O O O O O O O O O O O O O O O O o 0 0 0 0 611 0 0 0 0 0 m No N N N of o n V m V tp O C N O N m m n n O V M V V V N N N m v1 n n O a til V in V V vt o M N N m Yt O N N O n 0 a m V r0 m V N O N N N O n m V V V �O m a N O O O O O O 0 0 0 0 0 0 0 0 0 0o oO O O o O O O O O O O O O O O O O O O o 0 0 0 0 0 0 0 0 0 0 0 o. 0 a 0 ry g b 0o a o b o o 0 0 0 0 0 o 0 o 0 0 0 o 0 o 0 0 0 0 0 0 0 0 0 o 0 o g 0 0 o o o b 0 0 o 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 0 o r-1 N N o 0 0 0 0 0 0 6 o - O R o rv. n g o b H o M N p p o n o - _ d w ? w -0.. N N N lQ �-1 r-f �� N � N t0 .-I N N N N l0 ci ci c1 ai ii ei ea N N r0 r1 ey ei c-1 rti N > d k m E: --,.o 0 0 0 0 o m o a o o S o 0 0 o m o 0 0 0 0 0 0 0 o m S o o^ o 0 0 0 0 0 0 S S o o 0 0 0 0 0 0 0 0 d> . `� N b g o W r n w o n �* W o 1" °0 `� 0 0 0 0 0 0 0$ 0 0 o o mm o W n M n lD ed N N O rD W l0 e 1 t0 l0 n W M Oi •-I t0 n W- O n tD ci ti N rp tO n m m n tp E o m 0 0 N m 0 0 m m 0 0 m >n 0 0 m m 0 0 m 0 0 m 0 0 0 0 0 0 m 0 0 m m 0 0 m m 0 0 m m o N o 0 m m 0 o m b b m 0 b h o 0 0 0 0 0 0 0 0 o N p o o o m m q m o 0 m H p O n {_J ` N S O ei O O M O S o Y1 p S O t0 n 0 O ri 0 0 N m 0 0 V rt1 0 0 tD n N O O .-' O O N O o 'S ✓i p S 0 �O n N O O O e-i O O O O O vl O N O O O ei N S O o S O VI io O n c r s o` 0 0 0 0 o 0 0 0 o `o O r o O O a a d 0 a o 0 0 0 0 .c p 0 o 0 0 0 0 0,\ 0 0 ,o` o t z O o v O a o 0 v 0 0 0 0 0 0 O m m p p o o o o 0 0 0 0 0 o N O q\ N O o p p W N o o 0 0 o N o 0 0 0 N 0 _ E E N C N C N C G N N L C E N N N N C N N G C E N C N C -EC N N N N C C E 00 N E N N -E N N M N O O S C C C S C S C C C C C C C S G C C C L Nm Il. LL. LL LL LL LL t% m LL m LL LL LL LL LL LL U m LL LL LL LL LL LL m LL LL LL LL LL m O _ O C Ed C d d d d d C d OO C C O C d C d d d a G L d p �, C O C d d d d d d 0 C d a C d C C d vd d 0 a N C C C C G C C 6 G- 6 C Q d m m m m w m m. w 2 2 m m m a N V Q m m w mO Q w w a mLL n m d N Q m N N w U m aO aO LLO a2 aO aO aO0 20 n0 0 a0 0 0 0 aO nO aO aQ aO a` nO 2o (7 U' U' l7 C7 U' l9 U' [7 AO C7 l7 l7 l7 C7 U' l7 l7 l7 l9 l7 C7 C7 l7 U' C7 C7 C7 l7 0 l7 y l7 C7 Ur l7 C7 [7 l7 LD l7 l7 (9 l9 l7 t7 l9 ( (7 LD 0 L9 i7 Ur Z n-6 `o `o Z o` `o -M `o `o Z A o` o a `o `o `o a `o `o `o `o `o `o � a `o `o d a `o `o 2 `o `o a o `o `o `o `o `o `o d o `o `o `o o` `o `o `o `o `o `o `o `o `o `o `o B o `o _p LL T .n 2 .6 } .n ..g T .a T>??> a ,o .o -1 T T a .o T L LL a � a a T .o a T s >?? .n > .i a .n .n n s a� a T O b M (r0'1 M M M MOl M ttt 110'1 M O m O O m [.O'1 O M M O M t/1 M M M m m y O O O O O 0 O O R m m M O M COiI rv01 M Ml M d m Z �o m io �o o in �o In �o n m m ti ti o 0 ti .� 0^ mvrn I n r �000m.�m is r� a ro m co oo ao 00 ,� ry m m m o m m m T m m a m m m md m .+NNmE o� d, H o 0 0 0 0 0 0 0 0 E Z jo S9L �, j; S9L J. M b108£LL - 6L£LL � A. 99 L 8 LLM - OLM W7 1l L069L-0069L� S94 318YE9L-14£9L 34 Z6£S4 L6ESL@ awwow aulejoW ae"aly - awejoaweaow — 9lenrla Lu I lenla u eN8 u 6 IeniaLul aMa u Q A rn m N N O O o N O m N O rn o N V1 O O o 0 0 0 0 0 0 0 0 0 v o d o N 0 0 o N S S N N S S N o 0 S o N N o S N N S$ N N o S S o ¢ a m t� N N o T ti N N N N N O O O O O O 00 00 O O O O O O O S S O f] O O O O O b 0 O O 0 0 O O 0 0 O O m m m m c4i m m m m m G a y S 0 0 p o` v 0 0 0 0 0 0 0 6 0 0 0 0 0 0 0 0i 0 0. o 0 a_ o rn m m m o rn m m D o rn rn m o 0 m m 0 0 m m 0 0 m m 0 0 M m 0 0 m m 3 R ` s" y w W W m w O $ ro W W W oo W m W W W W W W 00 W m` o 0 0 o p o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 � pc0 0 0 0 o 0 0 0 00 0 o c0 0 b 0 o o 0 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 b N� M E o N n 0 0 co 0 0 m �o a a .y V m m O m of N N m 0 o o N ro m M N a N p �a, m m N O N ao v N .. F. E v"i v mu''i .n+ v a m (%' vi N ry N .+ a o o S m E o N ry m rn vl n n o e o m g v in a a v o a ry v o ry vi m n m o rri n o a m v a v �o m v v� N¢ F E o 0 ci o 0 0 ni o p 0 0 v o 0 0 0 o S m o ti ri p o 0 0 v a 0 0 0 0 0^ 0 '^ S S S o o S S S o S S o a-c N o N o N � a w �� n co rn H m m �n io co n co m m m N m p rn o M .a c m E n �o m n o o n ca M m n o o n m m rn m N N a e ro o S o o m a N ao S S S S w S �' �v rn t0 t0 n W W n O W N t0 n o 00 n m t0 W N e�i Y£ O O O O O O O O O �I O O N m O N YO1 O O N O O N m O O m V1 O O O t(1 tt1 rtl r Q +? O C N O O O O S O O N S S O O S O O c 4 L v a e v a o a r a h vb a� v a s a 3 3 3 3 3 3 3 3 3 3 3 3 3 3 m o m a a 0 n 0 0 0 0 0 0 0 0 a 0 0 0 0 a 0 a` p. U' l7 U' l7 l7 l7 l7 C7 U' l7 V' l7 l7 (7 0 U Ur I .. W `oo `o `o `o `o D M Z EZ do 594 it SL944 - 4L9Y4 @7 594 L 49Efi1- U9EV4 aulejow ,�, auweaow — LL len qpj ZG leniaaul 6 a — A o vrni a w o o 0 m � � N F a � u J 2 LL m o w d 0 N N m N O m m L a m N m N m N U U 5��11 V o U @ U (J W O S E 0 2 E O= E d E R Z R V E R Z LL a O w m p C R E C C ol L O = x x u) p O C O O zlco II F Q = N m d E W n L) O¢ z ¢ ¢ z z ¢ ¢ ¢ ¢ ¢ z z z z z ¢ ¢ 2 z ¢ ¢ z zcc w m INA d .O d C v m m m M N C •- T E 7 d ' E '� LO •Q N � X c R O R C wo LL E o 0 0 C LL U = � N rn5 w c � R Eo E � m'- T a � c o 'x � o U vT Q o o O o O O L� yd m m m m O O mm m m m O m m o O m m Apr m N y r N m v i QUJ 7 N N N N .d. N l0 r N O ,Dorn O O C et N i rn Oa a` r a a m rn m m o 1 _ 'moo 5 n U � c n E 9 .01 rn o ° o a 3 o 3 3 0 o c T E 1 m m m m m m -a v m m m m m d m m mm m E c E w Em w m a a m c 1 • ?! > J w m Li J J J v w JiJN w a E 2• ¢ ¢ m :° U O w U W m C7 2= o m r Y A a W N N N IV -W ro a { ' Q O N O W m ` 02ya. N O 3: ir d j0 u w W 1E.d N C W • EO a a o o e= U U z0= m` m a mID` C7 lo Oc ol ._ y o U ZZ U S a CL o L m 2n Y ,a' - c° C 'C r r n n C Y W LLQ m J U p O x x x x x 2 x S IT A y O O. E a a Z j > W O w p N Y U' w J w u Z m a O w N W O w fa W U w N¢ 3 N O Q}Q W¢= Q}Q m a dL6 J �U m H J J W F- J J W z U1 an Omwwwa wwwz>: is W U(7 W 2 (O m O D U J OO a'mO 0 d'm fn' 2 w �: J N \ �\ {/ // \\ ) kk \\ k/ ID LL // //jj ƒk / ## ,) \ \ ) / |2 \} /%}!7§2 2&b 6cn o.,a :kk 7fk `6 - )[ /«f \§ { D! EEE:E27°! - - ! #/f!««eEeEEE } / __---oIj —oo _ t} k � § {§j ){{ - \/\ 1 E 2 ©«u) _ :e; §{( {d§ 7}f §7, )°° o kol k\ (kk ({# »E£ SAFETY DATA SHEET 1. PRODUCT AND COMPANY IDENTIFICATION 1.1 1.2 1.3 1.4 Product Identifiers Product name Chemical Frac Tracer Date -Issued: 05-2015 SDS Ref. No: CFT Date -Revised: 4/10/17 Revision No:007 Product number 1000, 1100, 1200, 1300, 1400, 1500, 1600, 1700, 1900, 2000, 2100, 2200, 2300, 2400, 2500, 2800, 2900, 3000, 3700, 3900, 4000, 4800, 10100, 10125, 10175, 10200, 10225, 10250, 10275, 10300, 10325, 10350, 10375, 10400, 10425, 10450, 10475, 10500, 10525, 10550, 10575, 10600, 10625, 10650, 10675, 10700, 10725, 10750, 10775, 10800, 10825, 10850, 10875, 10900, 10925 Generic name CFT-1000, CFT-1100, CFT-1200, CFT-1300, CFT-1400, CFT-1500, CFT-1600, CFT-1700, CFT-1900, CFT-2000, CFT-2100, CFT-2200, CFT-2300, CFT-2400, CFT-2500, CFT-2800, CFT-2900, CFT-3000, CFT-3700, CFT-3900, CFT-4000, CFT-4800, CFT-10100, CFT-10125, CFT-10175, CFT-10200, CFT-10225, CFT-10250, CFT-10275, CFT-10300, CFT-10325, CFT-10350, CFT-10375, CFT-10400, CFT-10425, CFT-10450, CFT-10475, CFT-10500, CFT-10525, CFT-10550, CFT-10575, CFT-10600, CFT-10625, CFT-10650, CFT-10675, CFT-10700, CFT-10725, CFT-10750, CFT-10775, CFT-10800, CFT-10825, CFT-10850, CFT-10875, CFT-10900, CFT-10925 Relevant identified used of the substance or mixture and uses advised against Identified uses Diagnostic Uses advised against Not available Details of the supplier of the safety data sheet Company ProTechnics Division of Core Laboratories 6510 W. Sam Houston Parkway N. Houston, Texas 77041 Telephone 713-328-2320 Emergency telephone number Emergency phone number 713-328-2320 Transportation emergency 1-800-535-5053 (inside US) 1-352-323-3500 collect (outside US) 2. HAZARDS IDENTIFICATION 2.1 Classification of the substance or mixture GHS classification in accordance with 29 CFR 1910 (OSHA HCS) Skin irritation (Category 2), H315 Eye irritation (Category 2), H319 Specific target organ toxicity — single exposure (Category 3), Respiratory system, H335 2.2 GHS Label elements, including precautionary statements Pictogram <t> Signal word Warning Hazard statement(s) H315 Causes skin irritation. H319 Causes serious eye irritation. H335 May cause respiratory irritation. Precautionary statement(s) P261 Avoid breathing dust/ fume/ gas/ mist/ vapours/ spray. P264 Wash skin thoroughly after handling. P280 Wear protective gloves. P302 + P352 IF ON SKIN: Wash with plenty of soap and water. P304 + P340 IF INHALED: Remove affected person into fresh air and keep at rest in a position comfortable for breathing. P332 + P313 If skin irritation occurs: Get medical advice/ attention. 2.3 Hazards not otherwise classified (HNOC) or not covered by GHS - none 3. COMPOSITION / INFORMATION ON INGREDIENTS 3.1 Substances Substance/ mixture Mixture CAS/Exempt No Percent HazardousIngredient Proprietary Ingredient supplied as 10% w/v Proprietary 10 No Aqueous Solution Water 7732-18-5 90 No 4. FIRST AID MEASURES 4.1 Description of first aid measures General advice Consult a physician. Show this safety data sheet to the doctor in attendance. Move out of dangerous area. If inhaled Move person into fresh air. If cough or other symptoms develop, consult a physician. In case of skin contact Remove contaminated clothing including shoes and immediately wash affected area with plenty of soap and water. If irritation continues, consult a physician. Wash contaminated clothing and shoes before reuse. In case of eye contact Immediately flush eyes with plenty of water for two to three minutes. Remove any contact lenses and continue flushing for 15 minutes. If irritation continues, consult a physician. If swallowed Wash out mouth with water and keep at rest. Consult a physician. 4.2 Most important symptoms and effects, both acute and delayed The most important known symptoms and effects are described in the labeling (see Section 2.2) and/or in Section 11. 4.3 Indication of any immediate medical attention and special treatment needed No data available. 5. FIRE FIGHTING MEASURES 5.1 Extinguishing media Suitable extinguishing media Use fire -extinguishing media appropriate for surrounding materials. 5.2 Special hazards arising from the substance or mixture Carbon oxides, halogenated hydrogen gas. 5.3 Advice for firefighters As in any fire, wear full protective clothing and equipment. 5.4 Further information No data available. 6. ACCIDENTAL RELEASE MEASURES 6.1 Personal precautions, protective equipment and emergency procedures Use personal protective equipment. Avoid breathing vapours or mist. Evacuate personnel to safe areas. 6.2 Environmental precautions Do not let product enter drains, if safe to do so. 6.3 Methods and materials for containment and cleanup Construct temporary dikes of dirt or any appropriate readily available material to prevent spreading of the material. Cover with appropriate absorbent and sweep or shovel into an appropriate container. 6.4 Reference to other sections For protective clothing, see Section 8. For disposal, see Section 13. 7. HANDLING AND STORAGE 7.1 Precautions for safe handling Avoid contact with skin and eyes. Avoid formation of aerosols. Provide adequate exhaust ventilation at places where aerosols are formed. For precautions, see Section 2.2. Handle and use in a manner consistent with good industrial/manufacturing techniques and practices. 7.2 Conditions for safe storage Keep container tightly closed in a dry, cool, and well -ventilated place. Do not store with, or close to, strong acids. 7.3 Specific end uses(s) Apart from the uses mentioned in Section 1.2, no other specific uses are stipulated. 8. EXPOSURE CONTROLS / PERSONAL PROTECTION 8.1 Control parameters Components with workplace control parameters No PELs, TLVs, or OELs for this product or its ingredients are listed in the current issue of ACGIH's Guide to Occupational Exposure Values, nor have they been determined by the manufacturer. 8.2 Exposure controls Appropriate engineering controls Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of the workday. Personal protective equipment Eye/face protection Safety glasses with side -shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN166 (EU). Skin protection Handle with chemical -resistant gloves. Gloves must be inspected prior to use. Use proper glove removal technique (without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. Body protection Impervious clothing. The type of protective equipment must be selected according to the amount of dangerous substance at the specific workplace. Control of environmental exposure Do not let product enter drains. 9. PHYSICAL AND CHEMICAL PROPERTIES 9.1 Information on basic physical and chemical properties a) Appearance Form: aqueous liquid Color: translucent b) Odor Odorless c) Boiling point Approximately 100°C d) Freeze point 0°C e) Density 1.05 g/mL f) Flash point Not flammable g) pH Approximately 9 h) Evaporation factor Not determined i) Solubility Soluble in water j) Vapor pressure Not determined k) Oxidizing properties Not determined 1) Vapor density Not determined m) Viscosity Not determined 9.2 Other safety information No data available. 10. STABILITY AND REACTIVITY 10.1 Reactivity Strong acids. Oxidizing materials. 10.2 Chemical stability The product is stable under normal ambient conditions of temperature and pressure. 10.3 Possibility of hazardous reactions Will not polymerize. 10.4 Conditions to avoid Extreme cold. 10.5 Incompatible materials Strong acids. Oxidizing materials. 10.6 Hazardous decomposition products None. 11. TOXICOLOGICAL INFORMATION 11.1 Information on toxicological effects Acute toxicity— oral Based on available data the classification criteria are not met. Acute toxicity— dermal Based on available data the classification criteria are not met. Acute toxicity— inhalation Based on available data the classification criteria are not met. Skin corrosion/irritation Skin irritant 2 — H315 Causes skin irritation. Serious eye damage/irritation Eye irritant 2 — H319 May cause severe eye irritation. Respiratory sensitization Based on available data the classification criteria are not met. Skin sensitization Based on available data the classification criteria are not met. Germ cell mutagenicity Genotoxicity — in vitro Based on available data the classification criteria are not met. Genotoxicity- in vivo Based on available data the classification criteria are not met. Carcinogenicity IARC: No component of this product present at levels greater than or equal to 0.1 % is identified as probable, possible, or confirmed human carcinogen by IARC. ACGIH: No component of this product present at levels greater than or equal to 0.1% is identified as a carcinogen or potential carcinogen by ACGIH. NTP: No component of this product present at levels greater than or equal to 0.1 % is identified as a known or anticipated carcinogen by NTP OSHA: No component of this product present at levels greater than or equal to 0.1% is identified as a carcinogen or potential carcinogen by OSHA. Reproductive toxicity Reproductive toxicity — fertility Based on available data the classification criteria are not met. Reproductive toxicity— development Based on available data the classification criteria are not met. Specific target organ toxicity —single exposure STOT SE 3 — H335 May cause respiratory irritation. Specific target organ toxicity — repeated exposure Based on available data the classification criteria are not met. Aspiration hazard Not anticipated to present an aspiration hazard, based on chemical structure. Additional information RTECS: Not available. To the best of our knowledge, the chemical, physical, and toxicological properties have not been thoroughly investigated. 12. ECOLOGICAL INFORMATION 12.1 Toxicity No data available. 12.2 Persistence and degradability Presumed to be persistent. 12.3 Bioaccumulative potential No data available. 12.4 Mobility in soil No data available. 12.5 Results of PBT and vPvB assessment PBT/vPvB assessment are not available as chemical safety assessment not required/ not conducted. 12.6 Other adverse effects No data available. 13. DISPOSAL CONSIDERATIONS 13.1 Waste treatment methods Product Dispose of at a supervised appropriate waste disposal facility according to current applicable laws and regulations and product characteristics at time of disposal. Contaminated packaging Contaminated containers should be cleaned and disposed of in the same manner as the product in accordance with applicable regulations. 14. TRANSPORT INFORMATION DOT (US) Not dangerous goods. IMDG Not dangerous goods. IATA Not dangerous goods. 15. REGULATORY INFORMATION SARA 302 Components SARA 302: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302. SARA 313 Components SARA 313: This material does not contain any chemical components with known CAS numbers that exceed the threshold (De Minimis) reporting levels established by SARA Title III, Section 313. SARA 311/312 Hazards SAR 311/312: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 311/312. CERCLA (Comprehensive Response, Compensation, and Liability Act) Not Applicable. TSCA (Toxic Substance Control Act) The components of this product are in compliance with the chemical notification requirements of TSCA. German Water Endangerment Class WGK: 1 16.OTHER INFORMATION HMIS Rating Health Hazard: Chronic Health Hazard: Flammability: Physical Hazard: NFPA Rating Health Hazard: Fire Hazard: Reactivity Hazard: MANUFACTURER DISCLAIMER: Information given herein is offered in good faith as accurate, but without guarantee. Conditions of use and suitability of the product for particular uses are beyond our control; all risks of use of the product are therefore assumed by the user. Nothing is intended as a recommendation for uses which infringe valid patents or as extending license under valid patents. Appropriate warnings and safe handling procedures should be provided to handlers and users. Prepared by: ProTechnics Environmental Compliance Department Date of revision: 4/10/17 Contact information: 713-328-2320 SAFETY DATA SHEET cam 1n" t Date -Issued: 05-2015 SDS Ref. No: OFT Date -Revised: 04/10/2017 Revision No:008 1. PRODUCT AND COMPANY IDENTIFICATION 1.1 Product Identifiers Product name Oil Frac Tracer Product number 15000, 15010, 15020, 15040, 15050, 15070, 15110, 15140, 15150, 15160, 15170, 15190, 15200, 15210, 15250, 15300, 15350, 15400, 15450, 15500, 15550, 15600, 15650, 15700, 15750, 15800, 15850, 15900, 15950, 16000, 16050, 16100, 16150, 16200, 16250, 16300, 16350, 16400, 16450, 16500, 16550, 16600, 16650, 16700, 16750, 16800, 16850, 16900, 16950, 17000, 17050, 17100, 17150 1.2 1.3 1.4 Generic name OFT-15000, OFT-15010, OFT-15020, OFT-15040, OFT-15050, OFT-15070, OFT-15110, OFT-15140, OFT-15150, OFT-15160, OFT-15170, OFT-15190, OFT-15200, OFT-15210, OFT-15250, OFT-15300, OFT-15350, OFT-15400, OFT-15450, OFT-15500, OFT-15550, OFT-15600, OFT-15650, OFT-15700, OFT-15750, OFT-15800, OFT-15850, OFT-15900, OFT-15950, OFT-16000, OFT-16050, OFT-16100, OFT-16150, OFT-16200, OFT-16250, OFT-16300, OFT-16350, OFT-16400, OFT-16450, OFT-16500, OFT-16550, OFT-16600, OFT-16650, OFT-16700, OFT-16750, OFT-16800, OFT-16850, OFT-16900, OFT-16950, OFT-17000, OFT-17050, OFT-17100, OFT-17150 Relevant identified used of the substance or mixture and uses advised against Identified uses Diagnostic Uses advised against Not available Details of the supplier of the safety data sheet Company ProTechnics Division of Core Laboratories 6510 W. Sam Houston Parkway N. Houston, Texas 77041 Telephone 713-328-2320 Emergency telephone number Emergency phone number 713-328-2320 Transportation emergency 1-800-535-5053 (inside US) 1-352-323-3500 collect (outside US) 2. HAZARDS IDENTIFICATION 2.1 Classification of the substance or mixture GHS classification in accordance with 29 CFR 1910 (OSHA HCS) Flammable liquids (Category 4 - Combustible), H227 Skin irritation (Category 2), H315 Eye irritation (Category 2A), H319 Specific target organ toxicity — single exposure (Category 3), Respiratory system, H335 2.2 GHS Label elements, including precautionary statements Pictogram < 0 i> Signal word Warning Hazard statement(s) H227 Combustible liquid. H315 Causes skin irritation. H319 Causes serious eye irritation. H335 May cause respiratory irritation. Precautionary statement(s) P210 Keep away from heat/sparks/open flames/hot surfaces. No smoking. P261 Avoid breathing dust/ fume/ gas/ mist/ vapours/ spray. P264 Wash skin thoroughly after handling. P280 Wear protective gloves. P280 Wear eye protection/ face protection. P302 + P352 IF ON SKIN: Wash with plenty of soap and water. P304 + P340 IF INHALED: Remove affected person into fresh air and keep at rest in a position comfortable for breathing. P305 + P351 + P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P332 + P313 If skin irritation occurs: Get medical advice/ attention. P337 + P313 If eye irritation persists: Get medical advice/ attention. P362 Take off contaminated clothing and wash before reuse. P370 + P378 In case of fire: Use dry sand, dry chemical or alcohol -resistant foam for extinction. P403 + P233 Store in a well -ventilated place. Keep container tightly closed. P403 + P235 Store in a well -ventilated place. Keep cool. P501 Dispose of contents/ container to an approved waste disposal plant. 2.3 Hazards not otherwise classified (HNOC) or not covered by GHS - none 3. COMPOSITION / INFORMATION ON INGREDIENTS 3.1 Substances Substance/ mixture Mixture Ingredient Proprietary Ingredient CAS/Exenipt No Proprietary Percen 0-30 .� No Proprietary Ingredient Proprietary 70-100 No 4. FIRST AID MEASURES 4.1 Description of first aid measures General advice Consult a physician. Show this safety data sheet to the doctor in attendance. Move out of dangerous area. If inhaled Move person into fresh air. If cough or other symptoms develop, consult a physician. In case of skin contact Remove contaminated clothing including shoes and immediately wash affected area with plenty of soap and water. If irritation continues, consult a physician. Wash contaminated clothing and shoes before reuse. In case of eye contact Immediately flush eyes with plenty of water for two to three minutes. Remove any contact lenses and continue flushing for 15 minutes. If irritation continues, consult a physician. If swallowed Do NOT induce vomiting. Wash out mouth with water and keep at rest. Consult a physician. 4.2 Most important symptoms and effects, both acute and delayed The most important known symptoms and effects are described in the labeling (see Section 2.2) and/or in Section 11. 4.3 Indication of any immediate medical attention and special treatment needed No data available. 5. FIRE FIGHTING MEASURES 5.1 Extinguishing media Suitable extinguishing media Use dry chemical, alcohol -resistant foam, water spray, or carbon dioxide. 5.2 Special hazards arising from the substance or mixture Carbon oxides, Halogenated hydrogen gas. 5.3 Advice for firefighters As in any fire, wear full protective clothing and equipment. 5.4 Further information Use water spray to cool unopened containers. 6. ACCIDENTAL RELEASE MEASURES 6.1 Personal precautions, protective equipment and emergency procedures Use personal protective equipment. Avoid breathing vapors, mist, or gas., Ensure adequate ventilation. Remove all sources of ignition. Evacuate personnel to safe areas. Beware of vapors accumulating to form explosive concentrations. Vapors can accumulate in low areas. 6.2 Environmental precautions Prevent further leakage or spillage if safe to do so. Do not let product enter drains. 6.3 Methods and materials for containment and cleanup Construct temporary dikes of dirt or any appropriate readily available material to prevent spreading of the material. Cover with absorbent and collect spillage with an electrically powered vacuum cleaner or by wet - brushing. Place in container for disposal according to local regulations. Keep in suitable, closed containers for disposal. 6.4 Reference to other sections For protective clothing, see Section 8. For disposal, see Section 13. 7. HANDLING AND STORAGE 7.1 Precautions for safe handling Avoid contact with skin and eyes. Avoid inhalation of vapors or mist. Keep away from sources of ignition. No smoking. Take measure to prevent the buildup of electrostatic charge. Provide adequate exhaust ventilation at places where aerosols are formed. For precautions, see Section 2.2. Handle and use in a manner consistent with good industrial/manufacturing techniques and practices. 7.2 Conditions for safe storage Keep container tightly closed in a dry, cool, and well -ventilated place. 7.3 Specific end uses(s) Apart from the uses mentioned in Section 1.2, no other specific uses are stipulated. 8. EXPOSURE CONTROLS / PERSONAL PROTECTION 8.1 Control parameters Components with workplace control parameters No PELs, TLVs, or OELs for this product or its ingredients are listed in the current issue of ACGIH's Guide to Occupational Exposure Values nor have they been determined by the manufacturer. 8.2 Exposure controls Appropriate engineering controls Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of the workday. Personal protective equipment Eye/face protection Safety glasses with side -shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN166 (EU). Skin protection Handle with chemical -resistant nitrile gloves. Gloves must be inspected prior to use. Use proper glove removal technique (without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. Body protection Impervious clothing. The type of protective equipment must be selected according to the amount of dangerous substance at the specific workplace. Control of environmental exposure Prevent further leakage or spillage if safe to do so. Do not let product enter drains. 9. PHYSICAL AND CHEMICAL PROPERTIES 9.1 Information on basic physical and chemical properties a) Appearance Form: liquid Color: colorless b) Odor Mild. Resembling mothballs. c) Boiling point Approximately 175°C d) Freeze point Not determined. e) Density Not determined. f) Flash point Approximately 65°C — closed cup g) pH Not determined. h) Evaporation factor Not determined. i) Solubility Not soluble in water. j) Vapor pressure Not determined. k) Oxidizing properties Not determined. 1) Vapor density Not determined. m) Viscosity Not determined. n) Auto -ignition temperature Not determined. o) Explosive properties Not determined. 9.2 Other safety information No data available. 10. STABILITY AND REACTIVITY 10.1 Reactivity No data available. 10.2 Chemical stability Stable under recommended storage conditions. 10.3 Possibility of hazardous reactions Will not polymerize. 10.4 Conditions to avoid Heat, flames, and sparks. 10.5 Incompatible materials Strong oxidizing agents. 10.6 Hazardous decomposition products Other decomposition products — No data available. In the event of a fare: see Section 5. 11. TOXICOLOGICAL INFORMATION 11.1 Information on toxicological effects Acute toxicity— oral Based on available data the classification criteria are not met. Acute toxicity — dermal Based on available data the classification criteria are not met. Acute toxicity— inhalation Based on available data the classification criteria are not met. Skin corrosion/irritation Skin irritant 2 — H315 Causes skin irritation. Serious eye damage/irritation Eye irritant 2 — H319 May cause severe eye irritation. Respiratory sensitization Based on available data the classification criteria are not met. Skin sensitization Based on available data the classification criteria are not met. Germ cell mutagenicity Genotoxicity — in vitro Based on available data the classification criteria are not met. Genotoxicity- in vivo Based on available data the classification criteria are not met. Carcinogenicity IARC: No component of this product present at levels greater than or equal to 0.1 % is identified as probable, possible, or confirmed human carcinogen by IARC. ACGIH: No component of this product present at levels greater than or equal to 0.1 % is identified as a carcinogen or potential carcinogen by ACGIH. NTP: No component of this product present at levels greater than or equal to 0.1 % is identified as a known or anticipated carcinogen by NTP. OSHA: No component of this product present at levels greater than or equal to 0.1 % is identified as a carcinogen or potential carcinogen by OSHA. Reproductive toxicity Reproductive toxicity — fertility Based on available data the classification criteria are not met. Reproductive toxicity —development Based on available data the classification criteria are not met. Specific target organ toxicity —single exposure STOT SE 3 — H335 May cause respiratory irritation. Specific target organ toxicity— repeated exposure Based on available data the classification criteria are not met. Aspiration hazard Not anticipated to present an aspiration hazard, based on chemical structure. Additional information RTECS: Not available. Prolonged or repeated single exposure without adequate ventilation can cause: Nausea, headache, vomiting. To the best of our knowledge, the chemical, physical, and toxicological properties have not been thoroughly investigated. 12. ECOLOGICAL INFORMATION 12.1 Toxicity No data available. 12.2 Persistence and degradability Presumed to be persistent. 12.3 Bioaccumulative potential No data available. 12.4 Mobility in soil No data available. 12.5 Results of PBT and vPvB assessment PBT/vPvB assessment are not available as chemical safety assessment not required/ not conducted. 12.6 Other adverse effects No data available. 13. DISPOSAL CONSIDERATIONS 13.1 Waste treatment methods Product This combustible material may be burned in a chemical incinerator equipped with an afterburner and scrubber. Offer surplus and non -recyclable solutions to a licensed disposal company. Contact a licensed professional waste disposal service to dispose of this material. Contaminated packaging Dispose of as unused product. 14. TRANSPORT INFORMATION DOT (US) Not dangerous goods. IMDG Not dangerous goods. IATA Not dangerous goods. 15. REGULATORY INFORMATION SARA 302 Components SARA 302: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302. SARA 313 Components SARA 313: This material does not contain any chemical components with known CAS numbers that exceed the threshold (De Minimis) reporting levels established by SARA Title III, Section 313. SARA 311/312 Hazards Fire hazard — Combustible. CERCLA (Comprehensive Response, Compensation, and Liability Act) Not Applicable. TSCA (Toxic Substance Control Act) The components of this product are in compliance with the chemical notification requirements of TSCA. German Water Endangerment Class WGK: 1 16.OTHER INFORMATION HMIS Rating Health Hazard: 2 Chronic Health Hazard: Flammability: 2 Physical Hazard: 0 NFPA Rating Health Hazard: 2 Fire Hazard: 2 Reactivity Hazard: 0 MANUFACTURER DISCLAIMER: Information given herein is offered in good faith as accurate, but without guarantee. Conditions of use and suitability of the product for particular uses are beyond our control; all risks of use of the product are therefore assumed by the user. Nothing is intended as a recommendation for uses which infringe valid patents or as extending license under valid patents. Appropriate warnings and safe handling procedures should be provided to handlers and users. Prepared by: ProTechnics Environmental Compliance Department Date of revision: 04/10/2017 Contact information: 713-328-2320 SECTION 13 — POST -FRACTURE WELLBORE CLEANUP AND FLUID RECOVERY PLAN 20 AAC 25.283(a)(13) Flowback will be initiated through a third party flowback vendor until the fluids clean up at which time it will be turned over to production. (Initial flowback fluids to be taken to appropriate disposal well until they are clean enough for production.)
