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GMC Data Report No. 285
Total organic carbon (TOC), Rock-Eval and gas chromatography of core (8,846.2' - 13,508') from the Husky Oil NPR Operations (U. S. Geological Survey) Inigok Test Well No.1. ~ ~ f~\~M' ..'~::~\' ""1. ~1· .' ~ ,,':'~'¡¡ .~~:'f."~' ..~""~:~::,,, . ~':~ ~', ¡ """, , _ v~. ...,1' , ,.,., ." ..J '.... '. \.,.,.,.\0 ..-....~.' ','v ~' ~.. .. ....;.¡¡..... ~ ~ . Received 22 March 1999. Total of 246 pages in report. Alaska Geologic Materials Center Data Report No. 285 Q labnum well corenum t_depth b_depth du form_res urnl ~ geo_age type n 98R0382 HUSKY INIGOK TEST WELL 1 16 13505 13908 Ff KAVIK Permian CD d 98R0383 HUSKY INIGOK TEST WELL 1 13 12283 Ff . SHUBUK Triassic P' 00 ~ 98R0384 HUSKY INIGOK TEST WELL 1 13 12278.5 Ff .,' ~tfUBUK Triassic CD ~ CD 98R0385 HUSKY INIGOK TEST WELL 1 13 12273 Ff SHUBUK Triassic CD '"0 0 98R0386 HUSKY INIGOK TEST WELL 1 12 11705.8 11706.4 Ff KINGAK Jurassic CD ., .-+ 98R0387 HUSKY INIGOK TEST WELL 1 12 11708.5 11708.75 Ff KINGAK Jurassic CD N 00 v-. 98R0388 HUSKY INIGOK TEST WELL 1 12 1171.1.5 11712.5 FT KINGAK Jurassic CD 98R0389 HUSKY INIGOK TEST WELL 1 12 11713 11714 FT KINGAK Jurassic CD 98R0390 HUSKY INIGOK TEST WELL 1 11 10999 Ff KINGAK Jurassic CD 98R0391 HUSKY INIGOK TEST WELL 1 11 11006.5 Ff KINGAK Jurassic CD 98R0392 HUSKY INIGOK TEST WELL 1 11 11001.5 FT KINGAK Jurassic 00 98R0393 HUSKY INIGOK TEST WELL 1 10 1 0304.5 Ff KINGAK Jurassic 00 98R0394 HUSKY INIGOK TEST WELL 1 10 10301.5 FT KINGAK Jurassic CD ~ P' 98R0395 HUSKY INIGOK TEST WELL 1 10 10298 FT KINGAK Jurassic (JQ CD CD 98R0396 HUSKY INIGOK TEST WELL 1 10 10296 10297 FT KINGAK Jurassic CD ~ 0 98R0397 HUSKY INIGOK TEST WELL 1 9 9457 FT PEBBLESHALE Cretaceous Lower CD ~ N 98R0398 HUSKY INIGOK TEST WELL 1 8 9341 FT PEBBLESHALE Cretaceous Lower CD .þ.. 0\ 98R0399 HUSKY INIGOK TEST WELL 1 7 8846.2 Ff TOROK Cretaceous Lower 0) Total Organic Carbon (TOC) and Rock-Eval Report Q ~ n d II 8-11 ~ ARCO EXPLORATION & PRODUCTION TECHNOLOGY ~ (1) '1:S REF: Y74549 0 ::¡ ATfN: Alhert lIolba N 00 v-. II(;S SAMPI,E TOeANDROeK~VALDATA INTERPRETIVE RATIOS NOTES NO. ID. TOe Sl S2 S3 TMAX III 01 S2IS3 PI SIrrOe Check Pyrogram 13255 98R00382 0.30 0.04 0.08 0.10 532 * 27 33 0.80 0.33 13 c n 13256 98R00384 3.25 0.38 0.52 0.13 499 16 4 4.00 0.42 12 'n 13257 98R00385 4.11 0.26 0.50 0.14 568 12 3 3.57 0.34 6 n 13258 98R00386 1.52 0.13 0.21 0.20 522 * 14 13 1.05 0.38 9 n ~ 13259 98ROO389 1.25 0.13 0.19 0.10 515 * 15 8 1.90 0.41 10 c n ~ (JQ CD 98ROO390 1.21 0.35 0.54 0.11 482 45 9 4.91 0.39 29 N 13260 n 1.23 0.28 0.33 0.09 484 * 27 7 3.67 0.46 0 13261 98R00391 23 n ~ 98ROO394 1.84 0.92 0.90 0.05 465 49 3 18.00 0.51 50 N 13262 C n .þ.. 13263 98R00396 0.53 0.16 0.19 0.07 440 * 36 13 2.71 0.46 30 0\ n 13264 98R00397 1.80 0.73 1.84 0.12 469 102 7 15.33 0.28 41 c n 13265 98R00398 1.60 0.61 1.44 0.40 464 90 25 3.60 0.30 38 n 13266 98R00399 1.17 0.38 0.80 0.15 457 68 13 5.33 0.32 32 c n 11198.545 PAGE 1 * Tmax data not reliable due to low kerogen S2 value Toe = weight percent organic carbon 51,S2 = 109 hydrocarbonslg rock 53 = mg carbon dioxidelg Jock Tmax = °c HI 01 PI Slrroc S2*100rroc· S3*100rrOC S1I(SI+S2) SI *100rroc NOTES: Check c = sample analysis confirmed Pyrogram n = nonnal Humble Geochemical Services Division (\blÚ1dãr';ë9'-' - ,.............-..--... I 1100000 I 1050000 1000000 TIC:A990ooo1.D - ---- ~-_.- 98ROO382 ARO tJ ~ (1 tb :¡:) <rl- ~ :?'J (t) "d Ö :µ. ~ OC Y' 950000 900000 850000 800000 750000 450000 'to ~ OQ ç¡ ~ Ö trt> ~ I 700000 650000 600000 550000 500000 400000 350000 300000 100000 50000~--~---~~"'~~' l,' J, ~,q~l~ 250000 200000 150000 !offll, n 0-..- 7"'1"" . ..fj.~9º.. .. ~.O._...O,.,O 1 . . I . 35.90 4 I . · I . 1 I I I I .......9:.99.. ..~?:ºo ?_O~o~ I J I I ' I I I I J I I I _....,..__5~:ºº 60.00 I I , . I __ ..............._...,..,f:??:OO 7 I I I . I I ' I I I ....,..,..º~O 75 00 I . . I I _..,..__......-=-,.. ~'O:.O..Q.... ª?~O_,~_' I . I I I I !:JQ.Q() g5~0~" I I I . . J ~º-Q.Oº 10~.~ I I 1 . I . J ..., .....___..J..1():9º 115 I . . I.¿~ '1;0,00 '1 ;~,OO "Ii PJ~~.~e--~~ Ion 156.10 (155.80 to 156.80) : A9900001.D . - 98R00382 ARO Peakfl: Ret Time 'l'ype Width Area Start Time End Time 1 55.124 BV 0.118 1150763 54.873 55.278 2 55.304 VV 0.096 257226 55.278 55.544 ,Ç} 3 56.845 PV 0.157 8692135 56.568 57.242 4 57.616 W 0.118 2622462 57.432 57.815 ~ 5 57.980 W 0.116 2163962 57.815 58.110 n 6 58.248 W 0.123 5075118 58.110 58.455 d ~ ï 59.326 ìlr,¡ A .. An (;:1A1()O 59.074 (;:0 "1011 .-+ V..LVJ .J...L-:!:-L.VU J..J.J.J-:% ?' 8 59.560 W 0.128 3185640 59.394 59.831 ~ 9 60.484 VV 0.110 1241047 60.343 60.863 (1) '1:S 10 63.557 nv 0.089 626418 63.403 63.693 0 11 65.206 PV 0.111 341281 65.070 65.380 ::¡ 12 65.745 VV 0.101 345296 65.526 65.879 N 00 13 66.824 BV 0.086 430484 66.694 66.955 v-. 14 67.381 VV 0.085 220859 67.307 67.538 15 68.803 VV 0.105 484373 68.695 68.994 ~ P' (JQ (1) .þ.. o ~ N .þ.. 0\ u _.n__u' b)33~,'~~~~~1 ,~h,,~~J\~~~A~IN~ 59. <>.º__._nn._6..9..:.<>..<>......n._§.1 .0º_._n.'_...§?~ºº.....'.'_n..§ª.:ºº_'_m..__~~gQ__.n.n,_..§?·.º,º.._...._,__§§:º-º_.nn_..'..§.?:~ºº_'.nn_....§8:{)0 6 9 .00 631~56 60.48 59156 ..--n·',-----ò ~ ÇJ tJ ~ ~ :?J (Þ I-Q Ö J,4. N 00 r ~ ~ oQ ~ Ý' ò ~ ~ .p.. Ç\ lon-1S&'f0 (155.80 to 156.80): A9900001.D _......_._...._.._.... . ........._._.u ___......._.... .._._..·.......H._h_.._.._..._..____.__._~__~.____ ~bïJI1ctar;çe ¡ 5000 5 ).~~í} I 0 ,~"",",' ,~~-.,-,"\v, ) , ' ¿¡~~¡.E;-->54-º()... n' 55J>.() 56.0() n n ...,5?00 n' . ..?º:OO 57~9G 57.62 SEL2S 5t1..84 10000 55.12 15000 20000 25000 70000 65000 60000 55000 50000 45000 4??oo· 35000 30000 75000 80000 Ion 168.10 (167.80 to 168.80): A9900001.D 98R00382 ARO Peak# 1 2 3 Ret Time 62.124 63.022 64.744 Type PV VV BV width 0.098 0.098 0.101 Area 2813736 1628775 1825356 Start Time 61.990 62.908 64.499 End Time 62.342 63.280 65.109 Cl ~ n d P' .-+ P' :::0 (1) '"0 o ::4- N 00 v-. ~ PJ (JQ (1) 0\ o ~ N .þ.. 0\ rr.-¡~\~?-:->.. .... .. ... 6Q.?0. fJ..9. 40 ~.9.6º..60:1}.9 .~.!.:ºº..fJ.J:?-º..~J.:~.9J>..~ߺ.f:)J~ªº..~?:ºº,~?_·£9_~~º,..£>.?~§.()..§.?~ªº..~?...:9-º..,~ª,-.?ºß-ª,Aº_£>.?·60 6ª--!l.Q_~~:º.9_~4.:.?Q_£>.4,:~9_§5&0_§4.:ª-º..§.~:º-º!>.?~.?º_.~§~4º.~§.:.?_(),!J§:ªº_".. .J 64.74 W (Jp fD f-J b ~ tv ~ 9\ -------_.._--'~--_.._Q ~ <f1 b ~ ..... !1º :Þ:1 (t¡ ""0 o µ N QO ~ fj~}}2 Ion 168.10(167.80 to 168-:'80): A99o'oö-6:¡~D--- 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 20000 30000 32000 34000 36000 30000 40000 42000 6¿,:12 f\Gür1diÏr;C9 ,... ¡ 44000 "._.. .u.·._.·_.···_·__.··_·__·_·__._ ____....~_.___ ._.____._....___________.._______..__~_ Ion 178.~0 (177.80 to 178.80): A9900001.D 98R00382 ARO Peak#: Ret Time 'l'ype Width Area Start Time End Time 1 78.345 PV 0.090 12804335 78.207 78.613 2 78.640 VV 0.067 203420 78.613 78.698 3 79.910 PV 0.092 229388 79.776 80.053 Q ~ n d PJ .-+ ~ ~ CD '"0 o ::¡ N 00 Vt ~ P' (JQ (1) 00 o ~ N ...þ.. 0\ ...-.......-.------.....------------- Ion 178:ïO(177ßÖtOTiá]fu): A99000õ=[O--- ?f.35 ----~------------------... 170000 Q ~ (1 b ~ p þj (1) '"ö o ~. N 00 r 210000 200000 190000 180000 160000 150000 140000 130000 120000 110000 100000 90000 80000 t"O þ QQ fD }O b ~ N J:::.. 70000 60000 50000 I :: i 10000 7!3-{34 79.91 \ O~~~~'ífr{'¡ï{\ 'Î" ,~,.,' I"")';' 'I" "' I'" 'I' "'I'" 'I'" '1'" I "'"" I'" 'I' " 'I'" 'I'" 'I" "1'" 1 I"" I'" ,,', "., [¡.!!¡.2-.~>... ..........~6..:?<>.. 7,6.:4º 7.6:.6.º !():ºº..!J.ºº..?.!..:?ºTr4.º..T!:_6.º,TU:\º,7ª:º-º.?.º_:?.º1ª·~,º1~6.º,.Zª:,ªQIª-:º-º-7.~~º_?Q.:4,º,.Z~.:,6.ºJj},:ªºßº:ºº,ªº:?º_8.9.-,!.Q,ªº.:!?º..ªº:t3-º-ªJ-ºº..t3.!:,?9J!.!:'!º..ª.1,:E:캪.1..:ªº_...,., .~ Ion 192.10 (191.80 to 192.80): A9900001.D 98R00382 ARO peak# Ret Time Type Width Area Start Time End Time 1 82.680 PH 0.084 2578673 82.526 ,82.947 2 83.085 HH 0.089 3609348 82.947 83.256 3 83.749 HH 0.086 1671652 83.571 83.840 4 83.924 HH 0.089 1376579 83.840 84.049 a ~ n d p:¡ .-+ p) ~ CD '"0. o ::4- N 00 v-. ~ P' (JQ (t) ~ o o ~ N .þ.. 0\ rGÙr,clë.ïnl;·g' ._.n._._·__h"~"_.'-- ...........__...-.-..-.-.---_._---_._..._.._.._~._--------~-~ Ion 192:10(191.80 to 192.80):Ä9900001 j) 8J ~ oa -~--_..-.._-..,..,----..,..-_.._,---,-,------ ~-ì n¡ di P'; .-+ ; ~¡ ?:! ai N~ oo~ v-./ 60000 55000 50000 82.58 45000 30000 83.75 I ~¡ P'¡ (JQ ; (þ¡ ~ ~ ~¡ 01 ~¡ ~i 40000 35000 25000 83.92 , 20000 15000 1 ??oo 1 500) ^ ^ ¡ l-y h 1 ì~^~· LA ^ I ¡ O~~I ,m I.G~ 0·" (\,·0·,·, I'" ' " ,', I'" , ,', f ' "" I" II I ¡,.. I J. I-'YI~:-:~'{';:'~~ I ~¡ pirr:c--;.81..o0 81.20 ?1.40 81.60.. 81.80 82.0,0 8?:2~ ?2:~0 8.2.~O !3~:ª-O_ .!3ª:.09....!3ª-"-2Q _..8ª:19 ....8.3:§0.... 8_~:..8..º ~1·9º_..-ª-1gQ._8'!.-~º.. -ª-~:~0__,~~:ª-º..mª.~:OO....,!3§.:20 ...ª.!:):1º...ª:?:.f>-ºª!?}!0 ..__....¡ Ion 182.·1,0 (181.80 to 182.80): A9900001.D 98R00382 ARO peak# Ret 'rime Type Width Area Start Time End Time 1 67 .238 BH 0.095 223148 67.141 67.415 2 68.189 HH 0.055 163715 68.120 68.216 C) 3 68.304 HH 0.095 821321 68.216 68.495 ~ 4 69.067 PH 0.086 941765 68.907 69.271 n 5 69.788 HH 0.102 520352 69.562 70.082 d 6 70.430 HH 0.104 1225532 70.321 70.591 P' 7 71.326 PH 0.103 717623 71.û38 71.4û9 ~ ~ 8 71.462 HH 0.107 598849 71.409 71.728 ~ 9 71.833 lIB 0.105 433471 71.728 71.992 (1) '"0 10 73.507 PH 0.095 259418 73.332 73.662 0 11 75.566 PH 0.057 150002 75.485 75.735 ::¡ tv 00 v-. ~ p:¡ (JQ (1) ~ tv o I-t¡ N .þ.. 0\ rGlÙ~jf.Ú:;ëë 18000 17000 16000 15000 14000 13000 12000 1 1000 10000 9000 8000 7000 6000 ~ ITirne.. ..:;~ ..._..._ .__.u_ ._u _0 _._.. __ __ ."....0 ....._.. .u..___...· .__....____._.. ..........----'-..-,..·----'------lünT82.i0{181.80 tolÆ~'~B01:Ag9000oTIj----- 7C43 ~-_.-.--~--_._-...--_.---...._---.-....._----____:<o. <b ~ o tb sÞ ~ sp ~ (D "Ø o ~ w 00 f fu ~ ~ ~ ~ <Þ ~ 10 .þ. r 69.07 Go.30 71.33 ,1.46 69.79 71.~3 75,,57 58.1 ) 5000 73,,51 4000 67.2·+ 3000 2000 1000 ,I \ ", JM~ \ ( .~ ' t ~ \' n j. ~ .~ ~ ~.~ ,f .1l, >\.,~. ^ ~. r..  ~ \ I IUI Ü U Ii ~ J ~r d \ If . 1^ I I' I I r I ~ I \lfil~ U II f ' ~ '''1 \ h ft ~ . \dh A l ^ \ ~ l' ~I Lf1 I o ~ ~ lP\IIII ~~ I I ~J ~. IV" " -.-r-PJft, II II I II II "" ,I 'I .n........-' 1 I ~~, W 1 I II I 11. II r I "' . J II II I .. II II II I ~ I' )1) "I ~JII . I(I)\ . I ' J. J" ~J I, ¡ ..... ()~..?º... ()?~ºº..()??º...E).ª.ºO..,(),ª.·~º...()ª·ºº.,.()ª,~?_º..?:º~.ºº,.1º:?Q.]!:.º.º-.Z.1.:§Q,]?:ºº,]g,:~º.._Zª-:º-º_..?~~5.Q,_?1::.º,ºc.z4:,~º..?..~:ºº_?.~.:?.,º-?_~.9_q,1.():?_Q,_T!..:ºº_.Z?:.!),ºJ-ª,:ººJ.ª:.?º.,?_~:ºº...z~:,?º..._....! Ioo 231.20 (230.90 to 231.90): A9900001.D 98R00382 ARO peak# Ret Time 'l'ype Width Area Start Time End Time 1 89.623 PH 0.081 40204 89.487 89.769 2 90.460 PH 0.121 65084 90.332 90.599 Q 3 92.058 PH 0.070 45477 91.978 92.136 ~ 4 95.149 PH 0.087 44675 94.924 95.241 n 5 96.011 PH 0.076 40279 95.913 96.043 d 6 97.105 HH 0.056 54183 97.048 97.145 ~ .-+ 7 97.191 fIB 0.092 86548 97.145 97.318 ~ 8 97.408 PH 0.074 147853 97.318 97.570 ~ CD 9 97.764 HH 0.201 151472 97.698 97.948 '1:S 10 98.108 fIB 0.055 79746 98.032 98.137 0 ::¡ 11 98.155 HB 0.092 97947 98.137 98.294 N 12 98.381 fIB 0.074 58333 98.343 98.448 00 98.719 PH 0.106 83604 98.652 98.869 v-. 13 14 99.050 PH 0.126 201579 98.869 99.145 15 99.167 HH 0.106 41935 99.145 99.301 16 99.519 HB 0.077 49690 99.437 99.577 17 99.743 HB 0.078 46326 99,.716 99.858 18 99.937 PH 0.089 62950 99.858 100.096 19 101.533 PH 0.098' 99369 101.381 101.661 20 101.900 PH 0.107 41197 101.828 102.074 ~ 21 110.425 PH 0.064 46275 110.300 110.495 P' (JQ 22 111.757 PH 0.057 53444 111.513 111.819 CD 23 112.107 PH 0.102 117480 112.011 112.213 - ..þ. 24 113.575 PH 0.094 112303 113.331 113.721 0 25 114.415 PH 0.097 92399 114.314 114.542 ~ 26 114.676 PH 0.091 55578 114.542 114.789 tv .þ.. 27 116.479 PH 0.078 82118 116.247 116.593 0\ . .. II -, I .. ~ I ~ ~ , I. II I I( , I r I j: ~ ~~ ~ _. oil I r _I _ I .,t, 84.00 86.00 .__ª8.ºº __ _J~Q:..ºº _ ~?:Oº_ _,~'!:ºº- , __ ~~:Qº_u~ªßO ,_J-º9.oo_._!ºg:º-º-,J-º'!.:º-º--J_~Qº--J-º-ª,:.ºº_~JQ:ºº___1..1.?ßQ..!.1~:.ºº ...!J_~:-º.º_,J..!.8.:ºº- ¡ . ]Ll,; ¡ ~ l', ~¡ : : >- :- : I "I . ¡~l!.,. ¡ :: : . . -~-- r I II .- ~ . I I ~I ø r I'- Et,'1.:';...) 1 ,,-4J5!3 :H}.b: 9J.1'J ~, t )301 . .92.06 11 {) .42 95.~5 ';8.'":"2 - --,---- ---. ----Q ~ (þ tJ ~ ~ ~ o 'ö o :+ N.> 00 f Þ-tJ ~ ~ q ~ ~ Ö '7J N.> ;.. þ.. q'I 1;)153 97 'It"'L3? 114.41 116.48 97. ~f 99.94 112.11113.57 111."1'6 I ~7.7S 9L16 9ft 11 99(5 89.62 90.45 1'-' 76.00 78.00 80.00 82.00 ..~. .. _h__ _ .........-..... [~.~~i.?~~·> .. I ----.-.......--.-..-.--'-----...--,...-..,----..-----.-----..------10,123-1-:20 (230--:90 to 23'T90): A9900001.D 97A1 ........._._..._.._.... ___._h... 400 600 800 1000 1200 1400 1600 1600 2000 2200 2400 2600 2600 3000 f\burdËince" .. Ion 230.20 (229.90 to 230.90): A9900001.D 98R00382 ARO peak# Ret Time 1. 81.087 Type PH width 0.096 Area 104211 Start Time 80.975 End Time 81.170 Q ~ n t:1 P' .-+ ~ ~ CD '1:j o :¡ N 00 v-. ~ P' (JQ CD ~ 0\ o ~ N .þ.. 0\ -... --. - ._--..._--_...~..- -..-.-...-.-..-----..--..-...-.-.---....-..----------------_.~._---- íbUr.:ã::- 1700 1600 1500 1400 1300 1200 1 100 1000 I 900 800 700 600 500 400 I 300 200 100 ...... p IrrH:~--'> o -"L ~ I \, I '. 76.50 77.00 --Ion 230.20 (229.9Ó"to-230.90): À99Ò-Õ001-:-o------..m......'..-m..'.... 81.09 ._-_..._-~----_._~----._------~- ,h I I . . . I . . . . I . . , I I , . ,I, I 77.50 .. ,..?ª:.ºº..___.?ªßQ,..,.. h'?ª~-º-º""'" ?,~:.~Q...m_..ªQ:9_(),..__f:J,º~º.......nJ!,1,:Qºn...._'ª~..:?º_.....,_,ª?:..Qº,___,_8~~º....__nªª·ºº_.._,ª-ª,:!?º,_, 'mª-'!:ºº..'....m_f:J4~!?..0_n_ª~:00 -------------~-------, CD ~ o d ~ S ~ ~ '"OJ 01 ~ Ñ O¢ 1 ~ P'~ (JQ¡ CD) H ~ o¡ Hj¡ N ~ 1 ª?~.~ò..~......h........IJ Abundancg- ..'-.--..'.. ,- ----+----------.-... .- _.--_...----------_.._-------------_._-------~ _._-_._--_._----_.__._--_._~---._---- ----------- ---- TIC: A9900002.D 98R00384 ARO 2800000 2600000 2400000 2200000 2000000 1800000 1600000 1400000 1200000 1000000 800000 6??oo0 --Q ~ (þ tj $.)J ...-+- ~ ~ (} ~ Q ~ N.> 00 I ~ ~ ~ ~ go cD I-j+) to .þ.. r 200000 ~~~.tlM.w.I"r ¡!tIn ie, :1'1 ~\'rl,J\"~~\'~t.\ .l~ ~. ,I I,! . .~! ~. , ',I' I I,Jl" ~v ,*'N~ ¡ . ".' ~ A.. ¡rr'/l ! 400000 IT~rn2--:''"T o ~,,---,-, I I I , 1 I I I I f I I . I I I I I . I I I I I I I I I I I r I I f I I I I I I . I . . I I I I I I I t I I I I I I I I I . I I I ~ I I I . r I I I I I I I I I I I I I I I I I I I _ I I I I I I , I 1 I I I ~ 25~OO. 39:(),t),.... .35·9.9_..._.~º_·º9.........~?&().._m~9_·Qº.,.. . ~§:ºº.._..J,}9_·_º9_.__()~~Q.º___!º:ºQ__...1§.:..()º_..JJº~9_º_.m.JJ.?.OCL_-ªº:ºº..__.ª~·,ºº,J_º_º~ºº.....1º_~:,ºº_....l!º,~ºº_..JJ~QQ_J,?Q,,ºº, 125.00 . ......_,. Ion 156.10 (155.80 to 156.80) : A9900002.D 98R00384 ARO Peak# ReI: Time 'l'ype widt.h Area Start Time End Time 1 55.177 PV 0.102 1950825 54.967 55.274 2 55.346 VV 0.102 915079 55.274 55.533 CJ 3 56.893 BV 0.146 13628330 56.648 57.184 ~ 4 57 . 670 VV 0.110 6479470 57.454 57.865 n 5 58.011 W 0.117 5655753 57.865 58.156 d 6 58.307 W 0.114 10086081 58.156 58.581 P' 7 59.350 PV 0.096 1493789 59.072 59.434 .-+ P' 8 59.585 W 0.127 5928415 59.434 59.930 ~ 9 60.514 VV 0.116 2068754 60.381 60.777 CD '"0 10 63.583 PV 0.076 708869 63.484 63.699 0 11 65.250 PV 0.103 712145 64.945 65.315 :4- N 12 65.770 VB 0.102 714000 65.569 65.921 00 13 66.436 PV 0.129 620072 66.234 66.573 v-. 14 66.827 VV 0.111 482166 66.683 66.989 15 68.820 VV 0.095 613650 68.714 68.989 ~ P' (JQ CD ~ \0 o ~ N .þ.. 0\ Fbur,danC9 140000 . --~.._..-_.-._-~.__._-_.-_._------~------- 58.31 "-ïoñ15f3~To (155:ao to 156.aoj:'A9-9006o2~D _._-_..._--~.._-----~-_.__.----- "_.-_._'--"''''-'-a ~ q o ~¡ PJ) ?d, CD¡ '1:S ¡ oj ~¡ N Od ~ 56.[\9 130000 120000 110000 100000 59.58 Þ¡:j ~J N q oj Hi N ~ I 90000 57.67 aoooo 5ELO' 70000 60000 50000 4??oo 30000 6051 55.18 59 ~~,5 1:.:::0:.'::::::::: 21000000~'\~_,rvv}~(_:.5..:JL'ì;!ì:i.·35 '\., _, ~'I ., _, ,'.: I I-;-,~. " 63.58 · \.. _~-' ~_!_ ""'}"-'..M~'"~'M^ ~.A . 6~25r fiA4~r. ^ n ~r : , I' , ~. 1""",-.,' ,H,',', f,ty-, ,y,v"N,N. I j.V--l!0'~~~j tr¡r!¡é~· ~>5't..º.9 .. . 55~0º . 56.00 _ .?7 ·()9. u_..?..f3.:ºO,.. ,u._..~~.:-º-Cl._,__u___~º~º.9..,_._._,º-1..:'ºº._,...__,u,_,ª'?.:.ºº__.._'_§}:.9_º_'n____.§_4:º-º._'___'__£>.~:.Q.º_,____,_§.£:):ºº___'u.__'ªZ:ºº____._.§~ºº_..__..u~ª.:ºº_, _ _ j Ion 168.1C (167.80 to 168.80): A9900002.D 98R00384 ARO Peak# 1 2 3 Ret Time 62.204 63.082 64.770 'l'ype BV PV BV Width 0.109 0.099 0.105 Area 25912804 13691501 1406957 Start Time 61.893 62.863 64.643 End Time 62.525 63.322 65.022 a ~ n d P' .-+ ~ ~ CD '"0 o ~ N 00 v-. "ï:1 P' ?~ N o ~ N .þ.. 0\ rGì::: 320000 300000 280000' 260000 240000 220000 200000 180000 160000 140000 120000 100000 80000 60000 4??oo ....._-_._..-.~...-..._-..-. .-.-..-._.._--_...-_.-.---_..-_.__..._---_._~._--_.._---'~ 100168:ï0(1 67 _80 to 168-:80): A9900õ02:B---------- _..._~-----._--------- o¡ ~¡ n¡ d¡ ~1 .-+ , p~ ¡i ::¡¡ Nª 001 v-.¡ 6........,~{"\ .- c~ 63.08 ii 1'01 Nj ~I 1'01 20000 . ~~. 7\1. I O..-r"'t-'J'-rf"I" '"'I....,., .."ì ("", J r'-("'-r''} 'îÎfl'1r"' ' r. ("îf'"I (""'1'" 'I'" 'I'" 'I'T' 'I'" 'I" "1'" 'I"" I"" I'" 'I'" 'I ~~~¡ .f?.<J:~9...fJ.º ~.4_º..E?º.:fJ.º.§.9.~ªº..f? 1.:ºº...fJ.J.:,~-º..?J,:4_º...f?~.~~<!..~!.:ª_(}..,E>..0º_º_fJ.?.:,~_º_~~Aº..Q~~-º_6..~·ª_Q..fJ.I·Qº-§ª:?,º 63..:4_º..f3..;!;~º_~~.:ª-º..§4:º,º_§~g_º..§i:iº..f3.4:§º,f3.4:_ªº.{)..~:º-º.~~:.?º,§_!).:4º_~?·~_º,fJ..!):ª,º... ... ....! ~;.~.~.~ e,~. ~::.. Ion 178.10 (177.80 to 178.80): A9900002.D 98R00384 ARO Peak# Ret 'rime 1 78.407 Type PV width 0.097 Area 43822994 Start Time 78.115 End Time 78.878 GJ ~ (1 d ~ .-+ ~ ~ CD '"0 o ~ 1'0 00 v-. Þ-r;j ~ (JQ (1) 1'0 w o ~ 1'0 .þ.. 0\ 5??oo i ) ¡ o I r.... 1 I I , ....-rr.,.-, r-, ,.. r--r-I 1111 r-rr. r ¡Ii I I J II? n 11 ~I I ~I I' I' . I I I , I I I I I I I I ¡ I . I I I I I I . . I' I I I I I I I I 1 I I , I I . I I I I I I , I I I I I I 1 I I I I I' ~ I I I I I J I I I . I r I"'-¡-; r, I , I I I I 1 I I I I I . I ~ ...!§.:g(). ?~.4º.?{):§-º ?§~.~º..??~ºº..??:?º??:~-º,.T!:§-º.Z?:_ª.QIª:.Qºl,ª-·~O_?~~Q?ª-§º..?ª~.ªº..?~=-ºº_~_gº,]:.ª:~º.?_~f?º...?ª,:,ªº,-ªº~.Qº,ªº:?-º--ªº-·,~-º-ªº:§º.ª-º-:ªº..ª.~..:ºº,ªJ.:?()J3.t:4º..ª!ߺ..ª_!:ª-º ...,_J 100000 150000 200000 250000 300000 c ~ rp tj ~ ~ ~ ~ '1:::f o ::1¡ N 00 1 ~ ~¡ <§! N .þ. 01 ~ N ~ Oi 350000 400000 450000 500000 550000 600000 650000 -_._..._---------------~ .u·---·-..-..-------'·....---------'()n178:1 0 (177 .äÖ-tõ178~80): Ä990ÖOO~Ö-' 78.41 700000 -....----...--.-..----.-- . "'-.--..'--."- f:G'Jrdan-ë·e·------·- - Ion 192.10 (191.80 to 192.80): A9900002.D 98R00384 ARO Peak# 1 2 3 4 Ret 'rime 82.707 83.115 83.764 83 .949 'l'ype BH HH HH HH width 0.083 0.083 0.079 0.080 Area 9610606 13382761 4807679 3587209 Start Time 82.562 82.963 83.619 83.856 End Time 82.871 83.343 83.856 84.080 Q ~ n tJ ~ .-+ P' ~ (1) I¡:j o ""1 .-+ 1'0 00 v-. ~ ¡:I) (JQ CD 1'0 v-. o ~ tv .þ.. 0\ f\bur;dar:;cë'--....-·- _..__.._.~._.--.-. ---....-.--- ...... ---.-...__._--_.._.-_.-----_._~------~~_._---_._-~-- ~-_._.._------~----------_. -'---'-_._'_....,-----,..,--,._----'_..._-Q ~ o d P'j ~ ~~ ~ .g¡ oj ~ N 00 I Ion 192.10 {191.80 to 192.80}: A9900oo2.D K.12 250000 240000 230000 220000 210000 200000 190000 82.71 I 180000 170000 160000 150000 140000 130000 120000 110000 100000 83_75 90000 80000 70000 60000 50000 ~ p)¡ (JQj (1)1 N Oi oj I--fi N ..þ.¡ 83.95 \ 4??oo 30000 20000 ªJ.20. 81.40 .81ßQ.. i ~ ~ 1. . .. I . , . i 1"'ì-r1 f" '1r r~1 I I I I I I :. I I , 1 , I I .- . I I I I j I lit·' I I I I .', I J I ' i I I I . 1 I I I I I I I I I , I I 1 I . I , I I I I I I I I 1 I I I I , I I I I , I I I r I I I ~ 8 .1..:.ªº_,.ª2. 00 82.2ºª..?~~º.....,ª?::f>ºh...ª.?.:ª_º_,_,ª~..:Qº....,!3__ª,:?.:.Q...,' 8~:~º_.-ªª:§-º_,_ª_ª,:..f!º,_ª~:-ºº...._ªi:?º-..,ª~A,º..nª'!':.(Jº,_ª/:1::f~º_..ª'~:ººn..ª~:?_º._....8_5.:4_º......ª~:.f?º... 13.5.·ªº_........._ ¡ 10000 ¡ 0 frinïe·-> 81.00 ,.......-.--.........-. ........'. . Ion 182.1'0 (181.80 to 182.80): A9900002.D 98R00384 ARO Peak# Ret 'l'ime 'l'ype Width Area Start Time End Time 1 67.257 PH 0.082 517275 67.063 67.396 2 68.213 PH 0.066 1675874 68.088 68.253 Q 3 68.326 HH 0.088 4698358 68.253 68.564 ~ 4 69.099 PH 0.087 3979479 68.947 69.357 () 5 69.808 HH 0.084 1193357 69.715 69.958 d 6 70.453 PH 0.081 2260257 70.247 70.720 P' 7 71.358 PH 0.106 502707 71.158 71.434 .-+ ~ 8 71.850 HH 0.085 400888 71.751 71.992 ~ 9 73.516 HH 0.075 357489 73.397 73.616 CD '"0 10 75.594 HH 0.090 333495 75.508 75.754 0 ::¡ 1'0 00 V'I Þ-O ~ (JQ CD tv -......J o ~ 1'0 .þ.. 0\ 'Dur=~:- ----------- - ------ - -, - - - -- ----- -- ---- ----Tõñ182.1 0 (1-81~äo-¡o182.80j:-Ä9900002]) -'--- --- - ----- 6f!.33 ---~---~ ------- - -- -- - __._____.._.___~_.u_____.~__... 70000 69.10 Q ~ (1 d PJ~ ~ P'¡ ~ CDj '"OJ OJ ::¡¡ N 00 Î 75000 65000 60000 55000 70.45 ~ P'j (JQ j CD¡ to ooj O¡ ~ tv! -Þ>i I 50000 45000 40000 G8.2; 35000 30000 25000 G9.H1 20000 15000 10000 6'1.28 5000 '1/_3~5 'ì.52 7559 I O~~~. '~1'~-~;~~~~" .,.A/(YM',¿~1>()~&~~~f¥:'{! 66.50 67.00 67.50 68.00 68.50 69.00 6~:~º.?0.0º_.7Q·50_ 7~:.Q.0..zl~.?_~X?..:º-o..,?~~Q..?ª':ººn.Z.ª-:~-º,2'!:ºº-1i~~º-25..:ººJ?:,!>.º...!~:ºº?_~_:?9,I7.0_Q!.7.5º ?8.QQJ8.?0 79·90 79.50 ¡ rrirnø--~'7 on 231.20 (230.90 to 231.90): A9900002.D 98R00384 ARO >eakit Ret 'rime 'I'ype Width Area Start Time End Time 1 7'7.467 PH 0.019 16012 77.407 77.530 2 81.113 BH 0.054 40602 80.972 81.188 3 90.494 PH 0.072 2111372 90.281 90.649 Q 4 90.670 HH 0.041 26288 90.649 90.713 ~ 5 90.741 HH 0.093 41460 90.713 90.892 0 r 91.848 nIT 0.045 12607 91.797 91.877 t:1 V c.. 7 91.930 HH 0.063 21683 91.877 91.969 pj .-+ 8 92.058 HH 0.071 482397 91.969 92.218 P' 9 92.269 HH 0.043 13877 92.218 92.302 ?:' (1) 10 92.439 PH 0.082 100904 92.383 92.554 "0 11 92.647 HH 0.076 25354 92.554 92.811 0 ::¡ 12 93.009 PH 0.093 122644 92.932 93.184 N 13 93.258 PH 0.053 20016 93.184 93.285 00 Vt 14 96.732 PH 0.072 30358 96.640 96.868 15 96.928 HH 0.071 38350 96.868 96.994 16 97.021 PH 0.034 17960 96.994 97.053 17 97.092 HH 0.053 40263 97.053 97.151 18 97.201 HH 0.056 44804 97.151 97.303 19 97.410 PH 0.065 73577 97.303 97.532 20 97.632 PH 0.046 21589 97.532 97.696 21 97 . 824 PH 0.097 113715 97.696 97.898 ~ 22 97.935 HH 0.059 46284 97.898 98.032 P' {JQ 23 98.091 PH 0.079 139031 98.032 98.311 (1) 24 98.467 PH 0.073 98015 98.379 98.577 N \0 25 98.765 PH 0.089 126652 98.668 98.927 0 26 99.010 PH 0.060 84953 98.927 99.178 ~ N ~ 0\ r6ur~~~ _.un '.""_~_""'_"",u"_n·.__ '....hh...__._...__ ----------- ---lon231~20(23òjjÖ to 23·1~90):A99ÕOÕÕ2~B---'--------- _. -- -. ---- gOA9 -- .- ._~-- --- ---- ----... ¡Q ¡~ ¡n ¡~ I£" i:;ö ~(1) 'd b Þ- ~ Do r 38000 36000 34000 32000 30000 28000· 26000 24000 22000 20000 18000 16000 14000 12000 92.06 10000 8000 6000 4000 'i1 ~ OQ ~ W q oi I--+) N , 98·§''fl77 ~ 2.rti1lo 1 200: ~~«~;~~Ù lll~~I~~I.I~'l\Þt~:~~.~~~ rr.¡~:r~~--'>h".' . ?f3.ºº. 7ß·90ß9·ºº.fJ.?:9(). .h.ª,:t()(), h h~~:()-º_m,,ª-ª:()º..~º:º9_._~_?:ºº_..._~~Qº.. '_~§.:'º()U_h~ª:9() . ; rW ~ 11'Í¡~~ /tI1\1 ~ ¡ ÞII~I~.I , I¡II~ ~I' 1\ 111I,bl~~I, ¡ W~1I I( ,. ~~~ ~ I ~I ~I ,~ I.I~ q~ i h.~.º-º-:-º_º..__l.Q?~º-Q'h!'º,!:.º.Qh..1hº§':º()__1()ª:º9_..,!,1Q:.º.9.,J.~.?:º-ºu,J.1'!:-ºº...~J.§~ºº.._1Jª:.()0"h"_h" .,.j 230.20 (229.90 t.o 230.90): A9900002.D 98R00384 ARO Lk# Ret Time 'I'ype Width Area Start Time End Time 1 81.103 HH 0.080 331753 80.980 81.249 2 81.700 PH 0.054 33091 81.566 81.747 3 82.110 PH 0.053 26616 81.840 82.143 4 82.919 PH 0.040 14731 82.835 82.950 5 84.438 PH 0.032 17261 84.334 84.486 Q ~ () t;1 i:IJ .-+- P' ~ .g o ;:¡ tv oc V. "1:1 P' (Jq (1) w o ~ tv -J:::;.. 0\ undance 7500 7000 6500 6000 5500 5000, 4500 4000 3500 3000 2500 2000 1500 1000 500 ,.. _... _ -- -... _.__ ...., ..-...... _" .__uo__ ......_.._ }{\, tr!r~~~~---.> O-,-r..-',r-T 1 . I I 76.50 77.00 ..-.... ......_...,-._-_....._~. ....__·.._...._-..··..····__.._....--lö-ñ..·23-<l20(22~90tö 23Ö~90): Ä9900ÕÕ~D'---_·__··__..__.._..,_··,·,_.._..·..·..·...._,..,_....·-..-..-......-.....-..-----.....-..'..'-----' 81.10 82.. 11 B1]O B~t.. 44 82.92 Æ ,/ , \ I 1 .·~r·l, .I ,~pJ~l·,~r ,t.,C..J- ~ ~'I'~~'+ J~TI . , .'-~+n' . I' ,'-' -~J -"~"T~~- ~,.l,-! 77.50 78 ·99. 7B.50 ......?~~º.º...,_.?~g~Q....,-ª_º&º..'n....ª.9..:§.9_,._....ª 1n·º().n_'..ªJn:~º...... Jl..?:º.9......._,--ª.?~.~º..n.'ª~:º.ºn.n.'ª-~.:~gh n..n..ª-1:':9º..n.n.ß'!'~?..º_..nB!).~,º0 . . n,~?~~º..'.n.. : ~. a ~ (') tJ ~ .-t- ~ þj ('D "a o :4- 1'0 00 VI ~ SJ;¡ (Jq CD W N o ~ N .þ.. 0\ ~ f -Ii - r¡jÚï~ÚÚ;¿e" 3400000 3200000 3000000 2000000 2600000 2400000 2200000 2000000 1800000 1600000 1400000 1200000 1000000 800000 600000 400000 ... . __.~_____._... ... ....._.._nu___._.____ ----------"-_.---_.-- ------------------~._.+-~---~---_. Trc';.A99ÖOOÕ3:0'---'_...,--_..,___·__n_'_,__n.....__.._'.._._n_.._,_..__,.._.._.._....,..,__,___.__..~....___..,. cD 98R00385 ARO st o tj1 ~ ~ ?Þ (t¡ "0 Cí ~ N> OÞ I ~ ~ aq <1! w t.f Q I--!-,¡ t-b ~ 1 ïJ,)',,'\ ¡"M.\~,~l~\~¡J~,"h,~'j .J~, 1 ~M l~~1 ~ u/J ~,N /I~ JJ 'fW' \Io I' ¡ 200000 I I 1,1 ,.,.11 I . . ~~~yo1~~ ,.J o -""'T-TI~,-----Y--Y-~--"-"-I I t I I 1 I I I I I I' ( I tI~rj,~-~> . 25.00 3000 3500 4000 45100 50100 I ' I I I . , I I I I I I , I I I . ) I I , I I I , . I I I I I . I . . ' .. '.. _.... ._..___... .m~_"."'" ..............., ..m__..~......._....-=_._.._..____-=_____.....~§=-Qº-.._f:)º-·OO_n_f:)~:º_º..,..,..!º~Q9__L§,:..Qº ....JW.OO ,_.-ª5.Qº...._..,~º.º9..._n_Q~:'º,~_~1i>,~ºº_..:!. Q~:..Qº_n~1iQ.:ºº.._~~_1~~Qº'.._1~º=º_º_~~ 2{-ºº,,'_n:_.~J on .156.10 (155.80 to 156.80) : A9900003.D 98R00385 ARO 'eak1t Ret 'l'ime 'l'ype Width Area Start Time End Time 1 55.178 VV 0.097 2084726 55.023 55.276 2 55.323 VV 0.096 922898 55.276 55.531 C1 3 56.902 VV 0.154 15409196 56.665 57.161 4 57.654 PV 0.114 7248390 57.485 57.849 ~ 5 58.011 W 0.112 6207575 57.849 58.151 n 6 58.302 VV 0.104 11384531 58.15,1 58.557 d ~ 7 59.352 PV () 1 (), .... rrr'\.I"'\............, 59.166 59.428 <""t- v _ J.....VJ .L:::>O::;1U¿f ~ 8 59.575 VV 0.138 6637175 59.428 59.870 ïO 9 60.500 VV 0.110 2293876 60.363 60.761 (J) "d 10 63.599 PV 0.097 931154 63.388 63'.734 0 11 64.692 PV 0.111 410825 64.532 64.805 ::4- 12 65.236 W 0.134 990474 65.121 65.646 tv 00 13 65.762 VV 0.087 693977 65.646 65.879 VI 14 66.410 W 0.107 596854 66.271 66.554 15 66.844 PV 0.091 626333 66.671 67.035 16 67.406 W 0.086 336263 67.320 67.507 17 67.665 PV 0.073 254741 67.507 67.821 18 68.822 W 0.106 590685 68.724 69.015 I¡j P' (Jq CD W .þ.. 0 ~ tv ~ 0\ j&':::::: .._ ....___. _0. _h.._.....__..._ - '--"--~'---~----~-------.+---~-~-~---_._-.----_._-~~--------_._---.__...-~---~._--_._._--- Ion 156.10 (155.80 to 156.80): A9900003'J5---..'-----------'--·----·'..'-·..--............-·--..-,.._....-...,-,-_.._--.~ 5G.~~O ~ 140000 130000 120000 110000 100000 90000 80000 70000 60000 50000 40000 30000 65.H1 20000 ,..~. ':t'., 10000 ~·L'-í"< __~ O~- (~I"I P.:~(n~~~:;:~4.ºº.. 5~~()_0. 5§:º0 57.00 Sf-3D ~~7.65 58.0" 59,57 6t1",5Ü 59.35 I D0",Q.;.J 65.2465.76 i \ . t:k . I . .~-/ I ~~~1^{h1'~^~f':~, I"~ I " . 58.00 m'....§~~ºº...___..._.§_º~().Q..__._...._.!>1,~ºº-..___.._,_~?:º-º_......,__~=?,:Qº,_..__,_..M--º,º____--.-Ê5-ºº.._____§.f:),-ºº --CD ~ Q tj pp ~ ff IÞ (þ '1:j o ~ NJ do G-. '"t; ~ (It¡¡ 0> w o ó ~ NJ ..þ. t' Io~ 168.~p (167.80 to 168.80): A9900003.D 98R00385 ARO peak# 1 2 3 Ret 'rime 62.219 63.081 64.762 'I'ype PV PV BV width 0.116 0.094 0.086 Area 32011115 15240995 1221817 Start Time 61.923 62.899 64.631 End Time 62.523 63.368 64.894 Q ~ n t:j P' .-+ Pù ~ CD '"d o ., .-+ 1'0 00 v-. t-rj P' (JQ (1) w 0\ o ~ 1'0 .þ.. 0\ AbÚn'diii;cë- - I 440000 420000 ... --....-,.---.-....... . ,..______.._____.____..______u_.____ - -- ------- ------,------ B'i.22,on 168:10{167~80io168.80): A9900ÕÓ3j'j-------- ---- ------,---- --- - --- -- ------~-- - - -~ - 340000 Q ~ o tÞ p:! .-+ ~ ~ (U '1:::f. Q ~ ~ i 400000 380000 360000 320000 300000 280000 240000 6~~~D3 I Þ-d1 P:! C1Q ~ w -...µ d ~ Ñ ~ i 260000 220000 200000 180000 160000 140000 120000 100000 80000 60000 40000 ù4.7ú , 2000:~p-"">rr'~1'"r<"r'" ''', .~-r¡m"" """., ,-".,,-/,,, '" ,~!,"" """"""'''''''' "'"'''' '"., A~,-rpT1o"""Í1 Time- -> 60.00 60.20 60.40 6Q.69 6,9.8-º ~1·QQß 1_ .2~ ~ 1.40 6~A)Q. ~_1ß,9 ~~.ºº ~~.~º.ß.?1-º ~~§'9 J~.?:-ªº_ ~~:Oº- ~3.2.9_!J~:1Q..ª~6(~ ß3ß_Q !>1:.ºQ.M.:~ _~!1º §4~6-ºJ~1·.?..<g)~pº~5.:~º 65.40 65.§º,§?.:..~º__.h_'~ Ioµ 178,.10 (177.80 to 178.80): A9900003.D 98R00385 ARO Peak# 1 2 3 4 Ret Time 78.425 78.771 78.955 79.955 Type PV VV VV vv Width 0.097 0.091 0.116 0.090 Area 59583601 341640 504831 621925 Start Time 78.200 78.748 78.855 79.848 End Time 78.748 78.855 79.046 80.148 C1 ~ (J tJ µ:¡ .-+ PJ ~ (1) '1:S o ;:¡. 1'0 00 v-. ~ P' (JQ (D w 00 o ~ 1'0 .þ. 0\ ) -~ -- 70 Q;- , ¡x7¡'HQS .,,-.~~) , ~ v~ ~. .: '- ......,_. : 0...." r I II I'" I ~I I I " I I II I 1"1 1'-' I I I' I I ¡ II 11 -. II') , . 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I 1'1 11 IT' I I ,-I I ., II I I I I' I I J II " .~ ~ . .. 7~:?º.?€?~40.?~ߺ?~·ºº.I7~ºº.??:?-º_Z?:~º]1:!>º}·'?&()nZ-ª:.ºº-.!.~~,?-º]..!!:i()J8~~º..?ª,~~..9J~::!?gnZ~?º]~AO ?!!~60 7~~ªQ_t!º:º_0 8-º:?º..ª0_4º-ª.Q.:§º_t!º---ª,()...ª.1-.,ºº_ª.!.:~9_ª-1:~º-ªJ&ºª1.&º~__,..j ~!j~~.~:'>: 50000 100000 150000 200000 250000 300000 350000 400000 ~i ~¡ (1)¡ vi I..d O~ ~ to ~ 450000 500000 550000 600000 650000 ---"'-'-"""---3 ~ n¡ ~I P'¡ ~ CD~ '"0 ~ 01 ::r N¡ 001 v-.¡ 700000 750000 800000 850000 - .- - --- --- ~ -~-- -- -- .----- ---- -·--··--'--..----------------ïoo 178~fò-(1i7~äÕ'ton:¡-7t3.80T:..Ä9900003~6--·--'----- ntA2 __.___ - __ ____un . _.......__. . _____.____..___4____.__ AÚ(Ù~dár;c'ê" - 900000 Ion 192~~0 (191.80 to 192.80): A9900003.D 98R00385 ARO Peak#: 1 2 3 4 Ret Time 82.715 83_128 83.766 83.942 Type PH HH HH HH width 0.084 0.088 0.075 0.077 Area 14790578 20786740 6665196 4962175 Start Time 82.423 82.940 83.623 83.860 End Time 82.940 83_522 83.860 84.254 Q ~ n t; P' ........ P' ~ (1) '"0 o ~ 1'0 00 v-. ~ p:¡ fJQ (1) ~ C> o ~ 1'0 ~ 0\ Áhü¡~Úä¡::;¿ë-'" , ! 380000 _ ......_ u. _" _.0__ "4__ _ _n._. _..... _,".. _. .4._._ "H"'_h '--~---"'--------'----'--'----'--"-----~.'-'-'._-"-_.._----_._---_._-._._--------~------~-- --------------~-------~-~------_._~~--------~-----_.-- Ion 192.10 (191.80 to 192.80): A9900003.D K3.13 d ~ Cl tj ~1 .-t< P'¡ ~ CDª '1::)1 01 ~ N 00 vt 360000 'JAnf\nn v-yvvvV 320000 300000 8'1 ,,") G. f #- 280000 260000 180000 ~ ~ aq¡ CD¡ ..þ.. ~ d J-þ Ñ .¡:1. 9' 240000 220000 200000 160000 140000 83.77 120000 100000 H3.9,t BOOOO 60000 40000 . 20000 I 0 ^ _.~~ _ ~~. J ~ \ .' \ . . ~~. 1 ~, , 'í'ì r-, . , I · . Î' (' . 11 I . ,.. I '~I . , , . I .,.. I' . '-'-I~'" I .. I , I .. , . 1 .. .. , · .. I . I , , I' , . ~J (' , "1' ., I . , . . I roo-'1¡ ~Ií(:r~?~.:~':'. 81.()º_ ._ln~.?º. 81.40 f3!:~.º_ 81.0.0. 0.2.00, ...ª?·_~()__ª~:~º___ª?_·§()__..ª?~ª_º.__ª~:º_º.__ªª:.?_º_!!.ª_:.1()__._ªª.&Q...._ª-ª:_ªQ.... B.4,:i>_º_....ª_4:,?_º__,§4.4<L, 84.60 .-ª'!:!3Q__ª-~:-º.9_....~_5...:gº__ 85.40.. ,_ª,~~~º..ª~:,ªº_,_.._ i Ion 182,10 (181.80 to 182.80) : A9900003.D 98R00385 ARO Peak# Ret Time Type Width Area Start Time End Time 1 67.260 PH 0.082 654070 67.103 67.463 2 68.225 PH 0.072 3150106 68.004 68.261 Q 3 68.327 HH 0.086 6615725 68.261 68.567 ~ 4 68.652 HH 0.086 310070 68.567 68.750 (1 5 69.098 HH 0.089 5415054 68.946 69.266 tJ 6 69.811 HH 0.087 1554847 69.706 70.073 ~ 7 70.456 HH 0.086 2637404 "7 A ,....JI 7Û.764 ~ IV.";>¿;Z± ~ 8 71.351 ¡-If I 0.159 1017080 71.189 71.648 ~ 9 71.824 HH 0.106 527303 71.717 71.994 (1) '"0 10 73.522 HH 0.110 462605 73.278 73.633 0 11 75.584 HH 0.093 389477 75.505 75.750 ::¡ N 00 v-. ~ P' (JQ (1) .þ.. 1'0 o ~ 1'0 .þ.. 0\ 105000 100000 95000 90000 85000 80000 75000 70000 65000 Oß.i;;1 60000 55000 50000 45000 40000 35000 30000 25000 rbil::d:::: 20000 15000 . _..... ......._nn_.____._.____..._~_.. - - -- - ,..'''_U -'- ---- --- ---·---¡õñ-f82. fo Tf81:80 -to-i82_8ÖT:Ag9ÓOb03~6-------- -, --------- a ~¡ o¡ tJi P'~ r-t-¡ P'¡ ~¡ (1)¡ '1:S¡ oi ;¡.¡ N~ oo¡ v-.¡ -- ~"- ---~~- ..~-~--_._~._.__._----- 5f!.~33 69~ 1 G ~¡ P'i ~I -J::..! v.>i 8J ~ o 70.46 G9.81 Gï2G ~ 71 ~35 71.82 i 03.65 ~ ~ 73.52 15.58 ! 5000 ¡. ¡ O~f.I~'r,-N'\¥'{'>.L~p,~ '~'" " ,',' ,.' ,~ ~fY¡~~!\~! _~f?:I>_0_ ._f??~ºº...!>?~.!)o._ ~.ª.~ºº...~~:~9 ...€ì~.:ºº._()~:~P_.?-º~-º--I9-5Q.21.:ºQ..I1.~~_?~:º-º-...!...?:-5Q.,l~:QO 73:§'º-?.i.0Q.u?:,!:?-º,..?.~:.ºº-..?5.50_.J§: 00,_.!...t>.~º._V::.ºº-,!!:~-º'?-ª.:.º-Q_?~?9_'!~:P_QuZ~~~º__...._.J 10000 t!"k~~~~.~~> Ion 231.20 (230.90 to 231.90) : A9900003.D 98R00385 ARO Peak# Ret rrime rl'ype Width Area Start Time End Time 1 81.102 PH 0.064 77830 80.977 81.152 2 90.512 PH 0.081 4246305 90.272 90.706 Q 3 92.053 lIB 0.075 851226 91.964 92.205 $: 4 92.451 HII 0.092 316593 92.331 92.546 n 5 93.058 PH 0.125 252952 92.763 93.189 d 6 94.140 PH 0.057 64514 94.061 94.216 ÇI) 7 95.275 HH 0.128 102937 95.189 95.387 .-+ ÇI) 8 95.844 lIB 0.140 119880 95.811 96.063 ~ 9 96.386 PB 0.103 106671 96.204 96.441 (1) '1:S 10 96.839 IIII 0.073 69673 96.776 96.891 0 I-t 11 96.941 HH 0.092 103825 96.891 97.036 .-+ 1'0 12 97.090 HB 0.065 117294 97.036 97.138 00 13 97.186 lIB 0.077 152602 97.138 97.278 v-. 14 97.411 HH 0.097 323747 97.278 97.586 15 97.641 lIB 0.116 87728 97.586 97.722 16 97.776 HlI 0.087 163700 97.722 97.850 17 97.875 lIH 0.063 92514 97.850 97.935 18 97.965 lIB 0.069 70795 97.935 98.022 19 98.105 HH 0.112 371762 98.022 98.288 20 98.448 HH 0.089 212581 98.362 98.579 ~ 21 98.752 HH 0.085 214581 98.695 98.919 ÇI) 22 99.003 lIB 0.085 181494 98.919 99.121 (JQ CD 23 100.433 PH 0.099 67639 100.231 100.563 .þ. 24 101.197 PH 0.082 80683 101.116 101.328 .þ.. 25 102.336 HH 0.079 87332 102.236 102.452 0 ~ 1'0 .þ.. 0\ .h .._u.._u_ ...~__.'..uh.. _u._·._._·_·u_.~.._. "__._______. --'--'--------'-'---'-----.----uu.u-------'-U'U-¡on u2'3T2C)"(23'(Ü:iõnio 231.90}: 7\9-g0()OO3:"D----n-.-n-n-nuu.-unn-..,--. GO~51 -_.._------~._-~-_..~..._-_.-~._-----_._--- '--''''Q ~ (þ tP ~ M- ~ :;¢ ~ "'á Q ;f N> oò I 80000 75000 70000 65000 60000 55000 40000 'ïi1 p.::! (JQ ~ ~ ~ ô ~ N> .ß. I 50000 45000 35000 30000 25000 20000 82.05 15000 10000 ~-2A5 974J.l1 5000 ,.~ f7 :§ft,;;J?O J3.0UA 1-1. 'g! H 1. Hi . ~-T. <)'rpt1. " 'f.;"-v- 10~ß:,\,2@2.84 o 1~.,}t1~µ.,w~I~IAlIh¡1 ~~1I,Ik\1 Iln~~tI'4y~~~'~ OJ. . u 1I' ~f \~i¥ ~1It"1.lf ~l~II,III"~~I~lhf \II~liI,lw, ,,¡\~""~IP."I~IMIII\ "II}IIL\I~~lf"J~..; ¡ ..z~~ºº. ..__Z~~º-.. 81:!:Q9. 82.0º___..!34.0Q.u_.!3_~ºº... ..uª,l3~.º-m.. ~.:ºuºn_,..~?,:Qº._.~4.00u._~Ê~º-~!!:Qº_~-º~Qº J,92.OQ_J94:QQ....!Q£!ßO ..!",®.:,QQ..J_!º:-ºº_.t~,?O~LI 14:,9-ºu_JJ.6~º_Q.1.~_ª·Qº.._.n'..u..¡ rrirne--:..' ~..."..__"_.._ .h ____ Ion 230.20 (229.90 to 230.90): A9900003.D 98R00385 ARO Peak# Ret 'rime 1 81.104 Type PH Width 0.089 Area 367750 Start Time 80.981 End Time 81.254 Q :;: n t::1 PJ .-+ P' ~ (1) >ö o ::¡ 1'0 00 v-. ~ PJ (JQ (1) .þ.. 0\ o ~ 1'0 .þ.. 0\ j . r i ..~ \ " . 1 I Iii Ii I I . ,Ii I; ¡ ,Iii ; I II ' I ¡ , ¡ ,I I I I I I I I I I I (I I I I I I I I -I I ' It.· I I 1 I I I I I I I , I . 1 I I I I I t "t ] \ ... I r I I ~ I I I; ,...._I9.·00 __L9.50 .__--ª-~-º-,_.,__ª~~9_,_._,~.1:.º9_..._JU .50 __'_ª~º_h.._ª2.5_º_ ...,_ª_3__,º-º__,__._ª~~0___tL~~-ºº..__,._ª~_:§º,_ ..ª§~º-º,__....~_~.~5--º_,__'m_,j ~ I 78.50 __._,__ ___,__.' ___u. __.____.,.,_.__.__._____u.__.______. 78.00 I-r-"r-'-- 1 " I" , 77.00 77.50 h:; $:\.) aq Çb .þ.. -N Ó ~ Ñ .f:::,. <P\ !Q \~ 1tJ iP' ; .-¡.. ¡~ ¡~ i(1) td 10 ¡;¡ 1W ¡oo ~Vì I I r I \. . --------------." _.._----------~._--~---.-----.-----~_.-. ---~-------~-- -...'..-.-'-h------..'-..--'---..-..-'-··..--'--·----Tòn230.2Õ(229~90 to 23Ò:9'õ): Â9900003.Ö----..,---- 81-10 1 000 ~ I 500 '!\ ¡ O..,-rl' hïrne--::-. 76.50 ........_-. .-....... 1500 2000 2500 3000 3500 4000 4500 5000 5500 6000 6500 7000 7500 Al~ur;;¿ia~;ëe·..- . .-..... ¡ 8000 ~:\b'¡ji~aiinëgnh I 2500000 2400000 . noon' hn_________n _..________.._..... __._..._..._.____....~._________~....._._____.___.__·___h__~____ 'TIC: A9900004Jj-- -------- -~---- ---- ------ ~~~--- ..·_--..--'-_.._~-·_.._....'''O ~ (1 b ~ é-+- ~ :¡:o (þ '"d cD :µ. N 00 ~ 98R00386 ARO 2300000 2200000 2100000 2000000 1900000 1800000 1700000 1600000 1200000 ~ fJQ ~ .þ <Po b tj-t-) N .þ. Q\ 1500000 1400000 1300000 1100000 1000000 900000 800000 700000 600000 500000 400000 ::: I. I "I ,L¡. ¡(",Ud ~,; ~*~ ,~ ì}, ~. 1rnmOO~~~~~~I~ ,~!, ~ \~1' '.~I~~tJ~.t~~~ .~~~i1~~1 O----rl~ I 1 . I 1 I I , I I , I , I I 1 I I I .. I I f I I r I I I ' I I I I I I I . I I I I I I I . . I I I I . I I J I I , I I I I I I I I I I I I I I I I I I I I I I . I I I I I I I I I I I I I I I I I I I I I I I ~ tIí.r:r.~~:~.> ...h...... . ?§..QQ. . ..ªº~Q().......~.~ºº.. . 1º~º9.....':t.?~ºº.._._, 50..ºº-....n55.09__i>Q~º..,_-ª?~ºº..__z..0_&º__?:?-.:9-º-._..mª0·Q(L__ª?~.º-º-.....-ªº::.ºº_..-ª5_0_Q.,_.!..00.0..9_..!.º!}~º_Q,_J..1.º-:..0()mJ..:L~~º9_..1.?º..:ºº....t~?:9-º-.._,...._..! Ion 156.10 (155.80 to 156.80) : A9900004.D 98R00386 ARO peakU Ret. 'l'ime 'l'ype Width Area Start Time End Time 1 55.184 VV 0.120 2340328 55.012 55.295 2 55.350 VV 0.111 932420 55.295 55.636 Q 3 56.908 BV 0.156 19235481 56.663 57.198 ~ 4 57.677 W 0.119 8237519 57.276 57.862 0 5 58.027 W 0.123 7515453 57.862 58.161 tj 6 58.315 VV 0.108 12791583 58.161 58.552 P' .-+ 7 59.363 PV 0.108 1542241 59.217 59.436 PJ 8 59.589 W 0.136 7602371 59.436 60.213 ~ 9 60.515 PV 0.098 2641839 60.328 60.964 (1) '1:S 10 63.598 PV 0.093 1018784 63.358 63.718 0 ;:¡ 11 65.238 BV 0.121 979676 65.106 65.467 tv 12 65.770 VV 0.085 959701 65.645 65.994 00 13 66.437 VV 0.112 792585 66.285 66.599 v-. 14 66.852 VV 0.096 822727 66.701 67.071 15 67.425 VV 0.084 494957 67.322 67.578 16 67.686 PV 0.070 305088 67.578 67.804 17 68.843 VV 0.094 840564 68.729 69.000 ~ P' (JQ CD .þ.. \0 0 ~ 1'0 -+::>. 0\ Al1unúfmC9 _.. '_""_'_U_.__uh ___'___n_ "0___'''____ __.._ .-...'-.--..----·-...-.--..---...-·ï"õn.-1-5'6..1'ÙTi55~80'tõ..1ss:-8o):"Aggooo04--:-ö·----- -- --,_. 58.3'\ - -- - ----~ --~- - -- -- - --- ......._..h.____________ SCgj Q ~ rþ tj Þ r-f- ~ ~ @ >-ö d ~ N 0$ ¡ 180000 170000 160000 150000 140000 130000 120000 110000 100000 90000 80000 70000 60000 50000 40000 30000 55.1ß I 20000 !3S.35 58.œ ~ þ (JQ (l)j ~ d ~ ~ <J¡\ 57.63 5H.S9 ßt1..52 S9aS6 63jJO 65.T! 10000 1 ~~ o~....-·. ~~''''--I-' , I I I I I I I I I ¡r!r~ie_-_~> 54~º'p_. .... ....55~~)Q. ........ 56.ºº_ 57.00, m.._....~E!:ºº........nn.....?_ª..·º..Q,.., I ~T ~1h~.~ I I ....__..,~_º:Qº_......,.. _JD..~ºº-..... .._,..,!>,.g__@_,_,..,__J~3.00__....._ 68.84 '......m.§-ª,:º,Q...._ Ion 168.10 (167.80 to 168.80) : A9900004.D 98R00386 ARO Peak# Ret '1' ime 'l'ype Width Area Start Time End Time 1 62.174 BV 0.100 10998895 61.921 62.572 2 63.062 PV 0.093 4782091 62.776 63.250 3 64.761 BV 0.103 1601903 64_614 64.959 a ~ n d P' .-+ P' ~ (1) '"0 o ;¡ 1'0 00 v-. ~ P' (JQ (1) v-. o ~ 1'0 .þ.. 0\ FbÚì~Úar;G9' 160000 150000 140000 130000 120000 110000 100000 90000 BOOOO 70000 60000 50000 40000 30000 20000 10000 [rime--:;. .. ........._-........ .". ........._....___...h..~. .-...uu--.-'-...u-u.----...-----'.-----iorì-168~1ë,_(167 .BO"to -1'68~80): A990Ö004.0-- --- _,__u --- --- 6~17 a ~ o d ~ ~ ~ ?; "'t::1 a ~ N <X> vr --~--- ----~~- ----~------------------ 63.06 ~ ~ aci CD¡ u. t'f c Þ-f> Ñ +:i- 1 64.76 ~-.4-.r>.~^--~~ ~-'\_"^-d'-.. ~ .. . . ~~--.^~ ¡ o Jj'-{- I "1 . , . . I .'. , . I . . . . I T'T . . I . . , , I ' , . , I . r I "I ,-, T 1 I . . . I I I f I , I . . I I I ' . . . I . . . . I I . . . I . . . I I . , . . I . . . . I . I . . I . , . . I . . I . I . I . I I' . T' I I . I . . . . I . . I . I I . . J I I . , . 1 .~ I r .' I J I . . I ¡ ......6.º-~?g.~_º..49_~ºßº.f3º~ªº_.f3j~ºº..~1~?º.~.1~4,º,~~.:.~Q.§..1~.Q 62.00_~~20 i>g:19_§?:E!..QJ~_2.BO j)3.00 ~~go ~,.40 6_~.~6-º_§'~ªº,f3~.OO 64.?Q 64:~9_~.:!>-º-§1.._ª_º..f3~:º_º_~!):~()....§..~~~ºJ)_~:..~Q_f3?:ªº,_._,_.! Ion 178.10 (177.80 to 178.80): A9900004.D 98R00386 ARO Peak# 1 2 Ret 'l'ime 78.394 79.956 'lype VV VV Width 0.094 0.104 Area 35302212 547797 Start Time 78.058 79.851 End Time 78.757 80.167 a ~ n tJ P' .-+ PJ ~ CD '1:S o ::t N 00 v-. ~ PJ (JQ (1) v-. IN o t--iJ 1'0 ~ 0\ ~ o -rrr'ì 1 TT~1 ''T-f'TT''1 '-''TT'T i"T¡ r 1 ïT '" I T ~~I ¡ I I I I I I I I . I , I I I I . . I I . . . I I . , . I ' I . . I I . I I I . . . . I . . , I I . , . . I . . . . ¡ I , I . , . . , . I I' . I I ' . . . I . . . . I I . . , I ' , , . .. ?~.~?º .?t?:~.0. ?f>.:~.º _ ?f>.:ªº.?.?:ºº..?.?.~?º..ZI:iº-.?X~~º.X?.:,~.?-ª.:,ºº..Iª·~º..?..ª:,~QZª=~_?ª=.80 79 ·ºº..?Q,:?Q..Z!!·iº-Z~:§_(),_?~..:ª,º...r~.9-=ºQ,ª-º-?º,.º--o.:~Q..!!º~f>.º..ªº~.ªº..ª1.~ºº..ª1:?,º.ª1:~Q..ªJ.:~º..ª..1.:ªº.......... ~ P' (JQ (1) VI .þ.. o ~ tv ..þ.. 0\ u~_u_~ ~! .-+ ; p:>~ ~¡ (1)¡ '1:S ~ O~ ::¡~ ~! v-.¡ 7f?.~JÐ ------------~--------------------~---------- ..ïõnTj~L10(177J3Õnto 178.äõF'Ägg00004.Ö-- 7[: .39 ....-------- ......._..__.._.____.______n_____._________n.._____ n_______________ __________._____~__..~_. rríme· -> 50000 100000 150000 200000 250000 300000 350000 400000 450000 500000 550000 ÄlJundm';(~fJ .. Ion 192.10 (191.80 to 192.80): A9900004.D 98R00386 ARO Peak# Ret Time 'l'ype Width Area Start Time End Time 1 82.714 BH 0.081 13344535 82.576 82.974 2 83.127 HH 0.088 18949288 82.974 83.512 3 83.768 HH 0.078 5995673 83.616 83.862 4 83.946 HH 0.083 4636612 83.862 84.166 a ~ n a ~ PJ ~ o '1:S o "'i .-+- 1'0 00 v-. 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I 4400 4200 UU _ .n__.____n_.... ..........,..,..·-·....·..,....,......-,........·-'----'--..·---lon 231.20 (2'3([90 to ~:~1~FA99Ö·OÕõ4~Ü-'---- ------------_.,--_.~--~-~---------------------.... 4000 3000 3600 3400 3200 3000 2000 2()00 2400 2200 2000 1000 1600 1400 1200 ~IL10 ¡ 1000 I 800 ~ \ 6OOu,", \ 400 \ 2~ l.-< JI J~,J J "', tI~n:~,g_-~.?:.._ . . . ?.fJ.~º9_..?.ª~º9..J~9..:ºº__ª?:9_9._...!3.~:...Qº.,.~6.Q..(L.J!~:º0 90.49 92..46 H2-CE) 93,05 /-., .)-' ~ 85.2B '39.00 g7~41 £ß~ 77 97_21 fJ7 ..~~Á 97~IP r' 96,'!: ~,¿, a" ~~ ...,\}.~~ i (J2~27 11 fL82 110.32 \~ (1 b ~ '<""!-- ~ þo (þ >tJ b Þ- N be r ~ ~ (Jþ ÇD 0\ ? ö ~ ~ r r;. f t n ~ :: H . I . 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Cf\ 5G..g9 200000 190000 180000 170000 160000 150000 140000 130000 120000 110000 100000 90000 80000 70000 60000 50000 40000 30000 55.15 2??oo I 58.28 S7.G4 57.9~ 59.57 5!:.i ..:~3 60.48 , 10000 ' ~30 157 E~22 5~Y5 6'j;-16 00.83 67.39 o'~~~";-)~'~~'" . I · .~ . .\.-~~'0~~\-t W~, , . , · · I" ,.... 'i tr.íiI~~::::...~<1.9º_.._.~.___.~5.~º0 . ....?_9_~º_º..__.. ,___~?:_ºº_._,__§ª.:º~__..___..?_~.OQ_.__ 60.0O'____ß1-Qº-____,_.§.?..:ºº-.._.__~~.:..QQ__~_º_CL_..,___~5~º9. ........._.,_9.E!:9...9_______..!>7 ·Qº..._.__,~~J?_º__u__.._?~~º,º-_..__u.,__i Ion 168.10 (167.80 to 168.80): A9900007.D 98R00391 ARO Peak# 1 2 3 Ret 'rime 62.160 63.042 64.740 'I'ype PV BV PV width 0.110 o .09-6 . 0.097 Area 18572201 936z993 1303519 Start Time 61.821 --62 ;.&4-2- 64.520 End Time 62.491 -63 ·~3'~± 64.948 -e ~ n d P' r-+ P' ~ CD '"0 o ::+ 1'0 00 v-. ~ P' (JQ CD \0 0\ o ~ 1'0 .þ.. 0\ rGU::::: ...._..-.--_..- .----...-....--. . _..._..-.-_.__...._--_...._------~..__._._------------._-~_.-_.._~- lon-168-A&{+67-.Wto-H>iLOO};-A900eOO7,O 6J,16 -----------~-~------- '-'---'--~--'-~=Q , ~ Q Ó ~ ~ ~ IP ~ ô ::!- K> 00 ! 240000 220000 200000 180000 63,04 ~ s:$ aG ~ \b -µ Ó I-jt) Ñ ~ Q\ 160000 140000 120000 100000 80000 60000 40000 64..74 ~ ~ ~ J ~ J. A~~ _rv-_ I O::::r-tIi'(7r"1T(~~""'~~"'IÎlllpr. rl~1 rllll'" "111111111111111111 '1IIII,"t '11111111111 'I' '1111 III I 11111'1 J] I'l" Ilf)~-tT"-'l' (1í1~ r:).r~E~'~~~'h_h____hf3Q~?.º..º9.40 ~(}-f3_º_.!:!º~~9J~~~º-º_l),~~?-º_§J.:1.º_§!~~º_§1&º_§_~00 62.20 62·4.9_.§?.:..~º..fi2.89_§,~9Q~3.20 63~~º-&ª=-f3..9_~ª-.80ß4.Qº_~~º~~.!L 64:~0 64.80 6§:.Q9_f3'§:?..9J~_!?':~Q 6~~~Q ~5.8º_n_.J 20000 Ion 17~:10 (177.80 to 178.80): A9900007.D 98R00391 ARO Peak# Ret 'l'ime 1 78.358 Type BV Width 0.089 Area 22059862 Start Time 78.175 End Time 78.525 Q ~ n d $:IJ .-+ P' ~ (1) '1:S o ~ 1'0 00 v-. ~ $:IJ (JQ (1) \0 00 o H) 1'0 .þ. 0\ ¡..cj p:¡j ~I \.d '-q oj t-t) N .¡:,¡ Oi ...'....-'--....--=0- , ~ c-:t d p:¡~ .-+; p:¡j 7d, (1)~ '"OJ 01 :4¡ N od V'i --~--_.._--..--- ....- ·····..··--··-,··....-··-'-,..,......-------:-:~...ï7.ß~'w:~{177:ãòt().l7ßßÒ}~.A990QOO7.D ----------'..-...-....---,- 78.,36 . hu·.._.....·.···.._..·.· .. ....---..........-....-- ¡rime--> ".-.- -- .--------.... 20000· 40000 60000 00000 100000 120000 140000 160000 100000 200000 220000 240000 260000 200000 300000 320000 340000 360000 380000 ~bÙI~Úár;¿~e Ion 192.10 (191.80 to 192.80): A9900007.D 98R00391 ARO Peak# Ret 'rime 'rype Width Area 1 82.692 HH 0.083 12945463 2 83.101 HH 0..085 17446.9-65 3 83.750 HH 0.081 7752684 4 83.931 HH 0.078 6891612 Start Time 82.556 - -~. 9-5.6. . 83.584 83.841 End Time 82.956 83_-5.M 83.841 84.273 -G ~ n d P' .-t- P' ~ (1) '1:S o ::¡ 1'0 00 v-. ~ ~ (JQ CD ~ C> C> o ~ 1'0 .þ.. 0\ f\b-üí1C1är;{;s '..--'" "'. ..-..' .__._.__ _ _._.__n._._.__....._..____..___.___·.__________~·_·__·_-__~___ Ion J92."10T191.BO to 19:LaÖ):A99QQÕO'lD--'-- 8~(.10 .__._-_.----~_._----------._-_. --·------a- ~ o¡ d ~¡ P'¡ ~ (1)¡ ~I .,¡ .-+; Nj 00 Î 300000 280000 260000 82,69 240000 220000 160000 B3.75 ~ P'¡ (JQ¡ CD¡ . -'! d ......¡. o¡ Hl t--.i ..þ.¡ 200000 180000 140000 83.93 120000 100000 80000 60000 40000 20000 O ~^ ~~ ~~I ~ ~ ì i ~rl'?'rlll" 11-' ..r,'lfll r-In I'll III1 rill. 111111111111111'1111 t 1.1 ,rllllllllllllll" 111111111.111111'11 II 'I1111I1 1'1; Ülr.n~-:·~ ~ !~OO__ 81.~0_.. ªJ .40 __ ~ 1._~9, !3_1.~0___ 8.?-QO _ ª~?º- .~.g.!O , 8~§!L -ª~:ªº-,'!!?-=QQ. .~-ª-:.?-º-_ª3.4Q....J!.~.60 _ªª.80 -ª1:º-9_ª~:.?º_, ª4.4Ç> ."ß_4·§Q . -ª.4:..8_O. _~_~.O-º,__ª,~.::~º_ J!5·19. ª!j.6Q. 85.ªº- _,_.1 'Ion 182.. 10 (181.80 to 182.80): A9900007.D 98R00391 ARO Peak#: Ret Time 'I'ype Width Area StartTÍffie End Time 1 67.240 BH 0.086 713381 67.112 67.401 2 68.206 PH 0.076 3617-12-3 68.9--5-6 ' -68,.;,2-33 Q 3 68.314 HH 0.088 9888052 68.233 68.543 ~ 4 69.088 HH 0.092 9401788 68.876 69.505 n 5 69.795 HH 0.090 2535989 69.586 69.985 d 6 70.436 PH 0.094 3313888 70.229 70.903 P' .-+ 7 71.333 HH 0.089 477135 71.177 71.412 P' 8 71.838 HH 0.087 458268 71.701 71.934 ïO CD 9 -,3 .203 PH 0.083 438779 73.008 73.354 '1:S 10 73.510 HH 0.079 607421 73.354 73.658 0 ::+ 11 75.564 PH 0.079 443284 75.365 75.690 N 00 v-. ~ P' (JQ CD ~ o 1'0 o ~ 1'0 .þ.. 0\ 7??oo I ~ ¡ 6??oo ! 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T~)6':; ~" f 2000 , 91 ~1: .. -3J{ 1500 ; ~ '" ¡ ,~JI! lill ~t 5~ j "" 11-T'" '~T'I'--l J . ~,q~11 ,'" I .lrJ[lJ~ trin}..?.::"2".. _ ,..16.00 ....?-ª..-º_º_ ,.., º-9~º-º.. __ ~..?:º-º __,!J.!~_J!!?oo ....-ª-ª.oo __§J0.<!º-_~?.::~!!4.00_~6,00 .. ~8.ºQ.....j oO~..1Qg.oo ... 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G ~ n d P' .-+ P' ~ CD "'d o ;¡ 1'0 00 v-. ~ P' (JQ (1) ~ o -....) o ~ 1'0 .þ.. 0\ r f \ I, , I' . ¡ I ' , ., ,I, . , I : , , , I · , , · , · I ' , , · I ' , , , I '.. """".1 'I" I · I ' , , " 78.00 . ....Zª.~~..,.._z..~.:9-º-,..._ 7~.50 ,~O.Oº-....._.!JO_~º___..~1:.ºº-.., 81.5º--ª-2_00...._ 82.§º____~:9,º,__.!!3.S-º..,..-ª-1:º-º-..ß4.S0.....~ß5.0-º._..._..ª-S.Sº--............,...J 7000 6500 6000 5500 5000 4500 4000 3500 3000 2500 2000 1500 1000 500 fríme--> · I I J , 0·-, I I . I 1"---'-'-' , ?~ß~L._.q?Z~,ºº , . -_._....-.._----_...._--~.._._-----_.._-------~--_.- 'I..,,~,I "\ \ ~ ?L~º...,q_,!ª.~ºº_. ,_,.!ª~~º_,.....,?~º()_ ron 230.20 (229.90to-230.90): Ã9900008.D 81.09 Cl --,---- - ----, -- -..- ~ Q t:J ~ f"!t'- ~ ~ ~ o :µ. to 00 r ----~-------- ~. ~ OP Þ I!--< b ?o ò 't1') N ;þ. v I I ......?~~§º'_~o,ooL~º,§.~.J!1.Q.O......!J1~º:. ' 8ÙQ~_'8?,W..... 83.(){)-º3~!iº_I~i410º'~8Ú.O'_·~!i,ºº,I.:.85~~º,_,_IJ Ion.230.20 (229.90 to 230.90): A9900008.D 98R00394 ARO Peak# Ret 'rime 1 81.091 'l'ype PH Width 0.066 Area 276575 Start Time 80.977 End Time 81.189 a ~ n d P' .-+ P' ~ (þ ~ o ., .-+ 1'0 00 V\ ~ PJ (JQ (þ ~ o \0 o ~ 1'0 .þ.. 0\ f\buncTiir1c'9......·----·....· I ::::: ------ - - TIC:Ä99"ÕOOO8-:D 98ROO394 ARO ---,------'--'---'--,--Q ~ o tj pj .-t' ~ :;¢ (tl '"á d >-i <""! N> oó 1 1900000 1800000 1700000 1600000 1500000 1400000 1100000 ~ ~ c-, ~ ~ ¢ d >-h Ñ) ~ 'r 1300000 1200000 i 1??oo00 900000 8??oo0 ¡ 7??oo0 ! 600000 I ::: i 3~00 I 0 P!.!t@:.~.?,.. 2??oo0 1??oo0 ~ ~JJ! A.~ V~ ~~ M ~ II ~'Ni .~ ....,.... .. : 25.00 30' . · I . , . , , . , , . : _ ' _, .. __:00___35.00 4000 I · .. , I .. " ; _.. '. 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J ~r'~ j~ tl ~~ ~,~~ ~~~~~ Ion. .156. :\-0 (155.80 to 156.80) = A99000.08.D 98R00394 ARO peak# Ret 'rime 'l'ype Width Area Start Time End Time 1 55.148 BV 0.115 16629~9 55.006 55~2}8 C1 2 55.307 W 0.101 567624 55.278 55.469 3 56.898 BV 0.164 24555398 56.608 57.105 ~ 4 57.670 PV 0.117 11397906 57.446 57.845 () 5 58.021 W 0.125 11082391 57.845 58.147 d 6 58.305 W 0.115 15531822 58.147 58.569 ~ P' 7 59.341 BV 0.106 1671859 59.105 59.417 ~ 8 59.577 VV 0.138 9031887 59.417 59.855 CD '1:S 9 60.499 PV 0.134 2022674 60.161 60.762 0 10 63.566 PV 0.093 826684 63.404 63.707 ::¡ 11 65.223 W 0.117 1355217 65.083 65.572 N 00 12 65.765 VV 0.091 1273747 65.638 65.946 v-. 13 66.384 W 0.121 1043057 66.193 66.558 14 66.842 VV 0.083 1039647 66.710 66.960 15 67.402 W 0.084 667203 67.309 67.544 16 68.807 W 0.116 587234 68.731 68_945 ~ P' (JQ CD ~ ~ ~ 0 ~ 1'0 .þ.. 0\ ___..__."u _.... ..__._._.._...__.____0_.._. '-'-'...-.......,..,.......'..-..--'..nn'--·..·-'..----,---..--,---:¡o1T1'5'{f.·O (155.80to156Jro): A990ÕOa..Š~'b-·_":-:--:--·:'..n--,...n-,---.,--c·-_··_··_-'---:--.-nn-.,--...,-----,'O ;:;t~ (Jl) ?o' ¡ -,.~.. , ¡:::::...- n¡ di p:¡¡ .-+ : P'¡ ¡OJ CD~ ~¡ ~ I ~ p:¡¡ (JQ ¡ CDj .......¡ ¡-..o.¡ Nj gJ ~ 58~31 240000 230000 220000 210000 200000 190000 180000 170000 160000 150000 ..~ J 57 .G7ö.~iã 140000 130000 120000 110000 1??oo0 59.56 I 90000 80000 70000 60000 50000 40000 30000 5~1,34 GO.50 , 63~57 55.15 I ::: . ~'31 ~.~ ~J , o~-r'-v-~"'" ¡..-;-, ' . · , I · , , , I · , .~, ~"",-, · IT~~?~~?:_~~:PQ_.........?~Q..O,_ .... ...~!3~ºº....... ..!?I:ºº..... ,.._,_~~:Q9...n__.._..?_9.:.Qº.__.___§.º-·Q~___,~~~9 Ioµ 168.10 (167.80 to 168.80): A9900008.D 98R00394 ARO Peak# 1 2 3 Ret Time 62.182 63.058 64.759 rl'ype vv VV VV width 0.108 0.104 0.118 Area 22875413 11852946 515829 Start Time 61.958 - 62. 8-49 64.587 End Time 62.439 63u.373 64.972 Q ~ n d P' .-+ P' ~ CD '1:S o :4- 1'0 00 v-. ~ P' (JQ CD ~ ~ w o I-ot) 1'0 .þ.. 0\ ~. . . . i - ~4~ ~ . . "- .-, - - I O~~~""'"l" f'1 r"" rt' Y'r,--rrr~"" 1'""'1 i 11'1" """'" ""1"'" '"1'"' 'I" J "1"'1'1'" J 'I' "I' ~~~,I?('o~1 t~f!!~~-::?~u~º:ºº-§-º.:?-ºßº~~Q.§..o&º.~9ߺ.§.~..:()º..~1..:?JL~,.40 61.=-@_.Q..~@_ 62.0q. 62~_6,g~10 6~,~~9 62.80 6~ºº--*?-ª.=-~º..63.40J~;3.~º_§ª.80 6~=º0 fi'!.20 6.1:.40 64~~Q,~~ªº.§~:ºº_~!:):gQu~!:)=~º-f??,:§Q§~~Q..___j 20000 ~¡ ~¡ CD¡ ~¡ ~~ .þ..¡ O¡ ~¡ N¡ .þ..¡ O\¡ 240000 220000 200000 180000 63.06 160000 140000 120000 100000 80000 60000 40000 ----~----~---------------~i t:;¡¡ ~¡ P'¡ ~¡ CD~ ~¡ :4.¡ N~ oo¡ v-.~ 260000 280000 300000 320000 Ion 16.8.10 (f67 .80 të)'168'ßO): Ä990ÔOõïiD-----..- ûj.18 _________.__..,_. _____________.__________.__n____________ ¡A'G'LlI1J"ar;C9'''''''''' Ion 178.10 (~77.80 to 178.80): A9900008.D 98R00394 ARO Peak#: 1 2 Ret 'rime 78.360 78.604 Type PV VV Width 0.088 0.080 Area 19467144 223223 Start Time 78.209 78.579 End Time 78.579 78.736 Q ~ n d P' .-+ ~ ~ CD '1:S o ~ N 00 v-. ~ P' (JQ CD ~ ~ v-. o ~ N .þ.. 0\ 78.60 _ . ) . 1 I o~~~, I I I I I I " 1" " \' ,.. I I IJ JI ,. IJ I '" '\ I '" \. '" I I., I I I I' 'I ""\ IJ "\' I II 1" I 'I" I 'I ""1 "'/" I '11 tUI!~ª~~.?.... __.... ._?~?_º_?º~~.º_?:~~º..?~:.ªº..!J.J)JL!?~.º-T!.:iº-zz:.§Q-rr:ªº_?:8.00.18:.20,78.40 78.60 7~80 7~:Q9J~~Qz..9~.º-_~.6º-z..!!&ºJ:!Q:º9 80:~º-8.Q.iº-ªºßO !:J.9.8(~-ª.~_.00 _ª-1.:?Q..ª.1.:4º_ª1~®J!1.:ªº__~j 20000 40000 60000 80000 100000 120000 140000 ~ ~I ~ ~ Oi oj t--t) N -Þi Oi 160000 180000 200000 220000 240000 260000 -----'=---..-~--~~------_...~--'--..----'--_________c1 ~ o d P'1 s-¡ ~ (1)1 '"'0 ¡ OJ ~ N 00 U! 280000 300000 320000 ]ori"178.1 0 (177.80 to 178.80): A9900008.D 7~36 .__h_____._..._._.._._·_·...__·__n_.___..n____~____. f'bÚr:Úancf;·-...... -.,... Ion 192;10 (191.80 to 192.80): A9900008.D 98R00394 ARO Peak# 1 2 3 4 Ret Time 82.701 83~109 83.763 83.949 'I'ype PH HH HH HH width 0.086 0.087 0.085 0.086 Area 12078618 15203225 10362209 9592993 Start Time 82.522 82.927 83.612 83.856 End Time 82.871 '-83.326 83.856 84.394 Cl ~ () d P' .-+ P' ïO CD '"0 o ., (""'t- 1'0 00 v-. ~ PJ (JQ CD ~ ......... -..J o ~ 1'0 .þ.. 0\ ~ 1 ¡ ~ ~ ~~ ~ r-. ) ~, L I ~ 0- T.-. I I '-I "'1'·" I I .""f""'". 0...... I'll I f I f· I ~II I I I I' I' I 11 I. (1" I I I' I' I 1.1 J' 1.1.. II_I' I 11.1 I II I I I I' I I I I' I I I II I I I I' I I I I' 1. I 1'1 I I 1'1 I I IÊ tIÎt!~~=.~~-:..º)_:.ºº...,_ªJ.:?-º .... º~. :~º_...ª ~.:.§.9,.--º1:ºº.....ª?..:Qº....,º?,:.?º,_~:~..J~.?,:~º--._,ª?:-ª-!L-ª~00 ªª~º_..-ª-ª:1g_!J-ª.:~<L,_83.ªg_-ª~.00 84.=?º._J!,!:~,_,-ª.~~§º--_~.8{L.ª,?-=ºº,J!?:.?º--,J!§.:19._ª~:§º'_.nª_~:'ªº__,___.J 20000 40000 60000 80000 100000 120000 ~ pj (JQ (1) ~ ~ 00 o ~ 1'0 ~ 0\ 160000 140000 83.95 180000 B3.76 200000 ·--------~1 n¡ ~I p:¡~ þO¡ CDj '"OJ o¡ ::1.¡ Ni ooi v-.¡ 220000 82.70 240000 260000 ---_.--.-_._--------_._~------------_._._----_.- ~bundance---..-----'-' ------------·-·--·--'---..-....·-'--·~'-~~'~-~Ion 1:~:1\0 (191.8()tö-192.80): A9900008.D 280000 Ion 182,.10 (181.80 to 182.80): A9900008.D 98R00394 ARO Peak# Ret '1' ime Type Width Area Start Time End Time 1 67.248 PH 0.092 914485 67.021 67.401 2 68.212 PH 0.073 3924481 6-8 ~ 033 6fL 238 a 3 68.327 HH 0.094 11675836 68.238 68.531 ~ 4 68.646 HH 0.100 542161 68.531 68.818 () 5 69.101 HH 0.090 11119798 68.892 69.380 d 6 69.807 HH 0.095 3410424 69.380 70.023 P' .-+ 7 70.438 HH 0.084 3869064 70.321 70.622 PJ 8 71.824 HH 0.113 371866 71.715 71.936 ~ (1) 9 73.206 HH 0.095 566135 73.079 73.345 '"0 10 73.916 HH 0.073 257526 73.835 74.018 0 ::¡ 11 75.227 I-lH 0.088 408088 75.107 75.337 1'0 00 v-. ~ P' (JQ CD ~ ~ \0 o I--t) 1'0 .. ::::.. 0\ rTjui~'aar;ce"-''''''-''-''-'''' 190000 __ _____. ____n__n_..___..__....._.._. ___..h_________________h__________ 68.33 62.'10 "---Tö"n-1t32.1 0 (181:8ötö~f82.80): iÙJ90oo68-:ö-----------..,-'-'---·- -------.--- ....-..'----0 ~¡ nj dj p'1 .-+ ¡ P'¡ ~¡ CD; ~I ~I Chi 180000 170000 160000 150000 140000 130000 6g·¿1 ~I (JQ 1 CDj ~; N¡ OJ 2.! ~I 0\\ 120000 110000 100000 90000 80000 70.44 70000 60000 69.B1 50000 40000 30000 20000 tF.25 I 10000 68.G5 71-82 ~73.2i 73.92 75.23 I ^_ j \ r/oÞ. -"A,y1 L.^ \-.J ~ I,. . "-". f\ /I ^ "" . tvAÅ-.. ~"^- ¡ O---y-r'T-t¡-~I'·'..}II^r-rr-r~~,.-.,'IIII'f·'..'I~·;~I7;~ll, III I"I' '" '1"'1""1 "'1' "1" I II 'I"l I" ·.I'.'·. ..'.·,Î\ .. .~~:~9_..~7.:~ººßl·50 ._~_ß_:ºQ..§.ª:~,º-~j!:.ºº__~~?9_ 70~º-º._Z~?.º 71.Q.º-_7.:.!:.~Q....Z?.:90 72.5Q...lª-:.<>Q2ª-·50 _?. 4.00 ? 4.5Q.. 75.Q.0 7!j.50_7.:ª~-ºQJª~§..9_V·OO ...zz:~QJ8.0_º,_Zª.:.?º-..Zg-Oº.2~5-º_.____i h:í!f.i~·-.:;' Ion 231.2U (230.90 to 231.90): A9900008.D 98R00394 ARO Peak# Ret 'rime Type width Area Start Time End Time 1 90.481 PH 0.069 134143 90.327 90.560 2 91.932 HH 0.087 184154 91.814 91.987 Q 3 92.060 HH 0.092 167351 91.987 92.172 ~ 4 92.439 HH 0.087 605025 92.333 92.539 (1 5 92.645 HH 0.104 189066 92.614 92.854 d 6 93.060 HH 0.128 663479 92.854 93.199 P' 7 93.281 HB 0.078 138188 93.199 93.332 ..-t- P' 8 93.695 HH 0.163 221317 93.490 93.766 ~ 9 94.123 PH 0.100 184450 93.879 94.208 CD '"0 10 94.368 HH 0.125 124477 94.315 94.569 0 11 94.946 HH 0.107 136508 94.871 95.062 ;¡ 1'0 12 95.183 PH 0.089 134237 95.062 95.231 00 13 95.303 HH 0.100 373295 95.231 95.465 VI 14 95.599 HH 0.131 205009 95.465 95.691 15 95.758 HH 0.094 219555 95.691 95.894 16 96.014 HH 0.127 458551 95.894 96.249 17 96.370 HH 0.096 295541 96.249 96.509 18 96.652 HB 0.120 178873 96.573 96.813 19 96.978 HH 0.097 166041 96.875 97.046 20 97.194 HH 0.079 214965 97.122 97.279 ~ 21 97.761 HH 0.094 123715 97.688 97.815 P' (JQ 22 98.081 HH 0.105 115379 97.991 98.169 (1) 23 98.437 HH 0.086 252940 98.363 98.556 ~ 1'0 24 98.751 HH 0.102 307041 98.613 98.874 ~ 25 98.979 HH 0.121 178144 98.874 99.091 0 ~ 26 99.463 HB 0.132 270096 99.355 99.594 1'0 27 99.738 HB 0.120 139008 99.594 99.786 .þ.. 0\ 28 105.910 JIB 0.132 137573 105.733 106.028 -----,-..--...-----.-.- bu~danCH 11000 10500 10000 9500 9000 8500 8000· 7500 frirne·-:....., .--.-.---.-.---... ...'._......n.....'..._.......,........_.,........._......,......._.._..._------···---'-----------¡ûñ 23·1'~20(230.90 to 231"]'0): A9900oõã.o 92.44 7000 6500 6000 5500 5000 4500 4000· 3500 3000 2500 2000 1500 1000 5~JJlJ .?!?º..º..._...?:ª}?..º..._.~-º:ºº.,. ---~-----_..._-,--~.-._~--_._.__.. -93JJ5 a ~ (") tJ ~ .-+ ~. ïO ~ o ::t N 00 VI 'ì:1 P' {Jq (þ 95p3gEt~37 (,(} (l'1 ~ N N o I--f) N ~ 0\ 9~µ;.45 97.19 9(L48 t?5. Ii! 9i _þ't~ ~.. ~Y·I ') Cl4 i? g;~A qß ,þ5l w)'~r~J::¡¡, ~ 99ø-46 ;H_~.74 3.28 J3..7'G951tl ~-'7.7;;~ 94.~~~ ~L3'f ff1. ,~ ~Ç}5_fn - I ,,-, ,l]Û~L.1 II 1 t:;j I ~ ' ! ; '1 ~i III ' ..d ~I·j t¡ t ~ ,r ~,I I , ! ~ I! i ! ¡ " ì, ~ ¡ ; ~ I~·~· l' 1 1 :, ~ L ~'. ',. :, ~ ""er"'a ... 1 00, I .. .J! l . ¡ I II ~ ¡ J I UI! ¡ J I; ,!. J -. . ~ - ¡ ,t 1 ., ~ ~ ~ 1 .. ~ : :'. , 1 I I 1 ~- ~ : . ¡~ " I T -r I . 1 1 I I I' ~ \ 1 I '1 " I' , ' I tl..'- .. Ÿ " .', I ...ª.g:º-º__.ª-1:..®____ª..~:ºº_,_,ß_ª·00., 90.0Q....~2.00 ___~~~_.~~:-ºº_,_..J8·-ºº--..J.ºº.::9_Q.._1 02·º-º--l-º'!:·Qº-.1Q!5.:.QQ_ 1 Oª~ºº.,lJ O·-ºº.._1!~~º-º-...1J~:QQ.,_11É:ºº-,JJ~~.(L__.._J / Q ~ cþ t±J ~ <"!+- ~ ::Þ .g G ::¡t. tU do I 'i::1 ~ (fq¡ (þ 1300000 ~ Ñ L!J 1200000 d I-?') t-b .þ.. i ~ If I tl' i 2??oo0 i i j I , / ~ . § 110??oo ~~ ¡ WI ,~¿ r \ · III ¡ ~ 0 I I . I I . I f I , I I . I I I I I I I I I I I I I I I I I I I I I I . I I I I I I . I I I I J I I I . I I I I I I I I ( I I I I . I I I J I I I I I I I I I I I I 1 I I I I I I t I I I . I . J I I I I I . t I 1 I .. I I ~ rIí.~?.~::?'. ...._ ._....,.. __??º-~..... ..ª-<>'~.<>'ºn."...ª.~·ºº_....,~_º=ºº_.._n~§'·Qº...__l?º.:ºQ.__"?"!)..:ºº_n_~Q·-ºº_._"§§':ºº____ZQ&Q,_?...?.:9-º-_.-ª-()·Q..º-_-ª§~()º~0·º9_.._,~5.ºº__,1-QQ~Q9__!º-~:Qº,__!1-º:00 _.1..~:.º-º-.....1.?0.ºº__J.?5.QQ_,_ ¡ 3??oo0 400000 500000 600000 700000 800000 900000 1000000 1100000 1400000 1500000 1600000 1700000 1800000 1900000 2000000 --_.--------'-----'------.:---.-----------~-------_.._---- -Tfc':A99000õ["b-------- -.-.-"..----.-. -----.........-...--.--.-..---.-..-.------.---...--.-.------ rbuñ'dfir;C9 ....._.n.. I 2200000 ¡ 2100000 98R00396 ARO ~ IoÙ 156..1:0 (155.80 t.o 156.80): A9900009.D 98R00396 ARO Peak#- Ret 'l'ime Type Width Area Start Time End Time 1 55.187 VV 0.121 1809919 54.891 55.301 2 55.338 VV 0.103 844734 55.301 55.585 C) 3 56.905 VV 0.151 21400592 56.667 57.317 ~ 4 57 . 696 VV 0.124 10219906 57.427 57.859 n 5 58.029 VV 0.124 9954948 57.859 58.173 t:I 6 58.330 VV 0.107 15096606 58.173 58.575 P' 7 59.369 W 0.100 1761868 59.232 59.440 .-+ P' 8 59.590 W 0.139 8670597 59.440 59.860 ~ 9 60.511 PV 0.090 2135887 60.358 60.756 CD '"0 10 63.605 PV 0.107 895094 63.451 63.736 0 11 64.694 PV 0.075 214397 64.498 64.796 ::t. 1'0 12 65.254 BV 0.106 1062589 65.040 65.458 00 13 65.787 PV 0.095 1230821 65.663 65.965 v-. 14 66.423 W 0.128 1014285 66.276 66.627 15 66.863 W 0.088 900462 66.715 67.031 16 67.435 W 0.086 701292 67.332 67.551 17 67.694 W 0.085 322066 67.551 67.794 18 68.852 W 0.098 753085 68.748 69.010 ~ P' (JQ (1) ~ 1'0 .þ. 0 ~ 1'0 .þ.. 0\ 100000 90000 80000 70000 60000 5??oo 40000 30000 59/J7 I rj5~ 1 H 155..79 20000 . 65.25 I ~'Ô r¡;:: ¡ 10000 :~~.34 I ~63'G1 B4ga. ' ~6B..A2'"',,(2V 671Ì::~() j \ \ ¡. - _w /Iv. .t..'';; ¡ ~r!..~¡ ~ ~ O~r,· ~·I·"'llr. '1.~t"I" . . "I""I~ ,j (0-1'" " '" '/"" h:í~~~:.~,~,:_§~.Qº-... . ......?.~.'~" . ....!)§.·99___.._ .._~~º_º-_,.._.._..~:ºQ_._... .._'§9.ºº_.._..____60.00 _____ 61·9_IL__n__ 62:Qº__.._,_... 63.Q!L_,_~.O.Q___.__ª-§:90 ,..._._ß6.QQ____,__ 67.0.Q....,___,__~,~_º_Q_.....,__...~~._ºg__..____1 60.51 ----- -- -~ -- -~--.. a¡ ~¡ C1~ Ö¡ P'j .-+ : PJ¡ ~i '"OJ OJ ::¡.¡ ~I ~I ~1 PJ1 (JQj CDi I---' ¡ 1'01 VIi o¡ I-t)¡ ~! O\¡ 59.59 110000 120000 5ELO~, 57.70 130000 140000 150000 160000 170000 180000 190000 200000 58,33 5C,91 -~------ Ion 156~ 10 (155.80·to·156.80):A9900009"D ------,--, -.._.._.-_...._----------_._--.._----~-- --......-....-----.. }Äbun'{jãr;cë-"'--"" Ion,168.10 (167.80 to 168.80): A9900009.D 98R00396 ARO Peak# 1 2 3 Het 'rime 62.190 63.083 64.790 'l'ype PV BV PV width 0.107 0.108 0.099 Area 16287770 8421799 1232708 Start Time 61.952 62 .903 64.632 End Time 62.478 63.447 64.967 Q ~ n d P' rot- P' ~ CD '"0 o ;¡ 1'0 00 v-. ~ P' (JQ (1) ~ 1'0 0\ o ~ 1'0 ..þ... 0\ AGÚñ(ïãr;i~9-'-"h'_" 230000 220000 210000 200000 190000 I ::: 150000 140000 130000 120000 110000 100000 90000 80000 70000 60000 50000 40000 30000 2??oo n' _h'_ _ _.__~.. n___.' __ ....._ ..... ._______ .--.----.-.-...-.--~---.u·------------~_______¡Õn -16871 0 -(167-..80-t~-168~8(}}: A99OÖÕ-G9~O _0_- --.. -.----~----. ~- .-- -.---- ---. 6à¡g --- --------- ----..... CJ~ ~j nl ~I .-+ : P'¡ ~¡ CD~ '"0 ~ o¡ ~¡ 1'01 oo¡ v-. 1 63.oe ~¡ ~I CD¡ ~¡ ~¡ 01 H-J1 ~¡ 0\1 64.79 ! 1??oo ,,! ~) ~ ¡ 0 II" (1. ,i~?';'-' '1' II ('" ,'1II1'f'r~fÏ"I'1Y I' "'11"'( r1 " '" 'I"" I'" II' I' '11~~rl" I' I r, , I II frime--> 60.00 60:?-º ~_Q:40_ ~0.60 60..!!º ~1.Q9 §1·gQ.~J.=~º, §1:§0 _~!&º-,~~.:()O 6~.?-º.Ê~-i.Q_~~60 6?80 63=º9_~~:gOh ~?.:.40 63.6º,.~-ª.8QJ~.1:.()Q~'?º- 61·~ ~&º_.~.:f3() _~~.Q~ ~~2.9 §5Aº ..6~·~~~.?.:.l!..Q.___l IOL.178.10 (177.80 to 178.80): A9900009.D" 98R00396 ARO Peak# Ret 'rime 1 78 . 3 82 'l'ype PV Width 0.088 Area 20326822 Start Time 78.200 End Time 78.8'75 c;J ~ n d P' .-+ P' ~ CD ~ o ::4- 1'0 00 v-. ~ P' (JQ CD ~ 1'0 00 o ~ 1'0 .þ.. 0\ Fbur,dahG'B··..·nn , ...---.-.----...'....---.---'--.'-----'--'--'---'-------lon ·178.1õ117f~80tOl'7á:8'0): ·A~fg00009:b---~---,-"-~-o-.._~~ 78...38 '_.c·,·,-~~~-~---'--al ~! n¡ dj P'1 s¡ ¡oj CD~ '"01 01 ::4.j N¡ 001 ~I 340000 320000 300000 280000 260000 240000 180000 ~¡ P'1 C§! ~ ~ ~¡ 01 ~1 N¡ ~I 220000· 200000 160000 140000 I ¡ I I ~ 120000 1??oo0 80000 60000 40000 20000 O' '" I . . . ~ ........... . I I . . . I . I . . I . . I . . . . I I . . . I . . I . rf· , . 1 . . . . J . . , . I . . . . I . I . . J . . I . I . . . . I ' . . . I . I . J I . . . . J . . . . I I , . . I . . . . I I . I . I ' . . , I . . . . I ' . . I I ' . . . I . . . . I ¡ [!i~Q~~?:..._ ..._ .. ....?§...?.o ?~:'!º.?..6..:§º.?.~:ª_()_??.·Q.9JZ:~().Xz::_1..()..?Z:~0 TUJQ,78.ºº- 78·_?º..J-ª=-~º..Zª.:?-º-?J!-80 I9.0º_z:~QJ9-~'O'_?9-6º_L~:.8.Q-ª-º:Qº__8_º:20 8º.:..1Q.-ª.Q,:~0 8():ª_º_~:-º-()J!!_20_,ª_1.:~º-ª1.&()-ª-!&fL...._j Ion 192.10 (191.80 to 192.80): A9900009.D 98R00396 ARO Peak~ Ret Time rl'ype Width Area 1 82.718 HH 0.086 10956481 2 83.121 HH 0.089 14263250 3 83.778 HH 0.078 9190616 4 83.957 HH 0.082 8988727 Start Time 82.5'29 . '82.9'85 83.641 83.869 End Time 82.985 83~55-o 83.869 84.612 C1 ~ n d P' .-+ P' ~ (1) '"0 o ::¡ 1'0 00 VI ~ P' (JQ o ~ w o o ~ 1'0 +:>. 0\ rbU::::: ....._.. ....__......._....__.__..........h...______.______________-.---- --~-_._---- Ion 192.10 (191.80 to 192.80): A9900009.D 82.12 - -- ._-~-- - - --- ~----~- Q¡ ~\ di s.¡ P'j ~¡ CDj ÞOQ ¡ ~I i:0j oo¡ v-.¡ 220000 82~72 200000 8:3.78 180000 ô3~96 140000 ~j P'¡ (JQ 1 CD¡ Þ---' j wj ~¡ 01 ~¡ N¡ ~¡ 160000 120000 100000 8??oo 60000 40000 \ 2~ ~~ _'-p rf',""f"Y> ,.,.-,-;,I "".¡ , , , , ~ ' , , , ~ ' , I ,', . . I ~, I ' , . , I ' , , , I ' , , , I ' , , , I ' , .. I . . , . I ' , , . I "'.. ITí.!I!?----:~. ~1:Qº.. ß..1:g9--!! ~ .4q_...!JJ:~º_.. ~J:!)~_ªg&º_._ª.?_.,gº__, 8~.40 _.!J_2_.§9___~:ª-0_ªª.OQ_, ª329 -ª3.40 83.60_ _ ªª:-ªº- ?4.ºº-_84.20 _~.40 ~:!>_O__?..1:@--ª?.OQ _ ª.§..2-º__--ª~.:.~.Q..._~~~~_ª-ª=80 __.~....i Ioe.> 182.10 (181.80 to 182.80): A9900009.D 98R00396 ARO Peak# Ret Time 'l'ype Width Area Start Time End Time 1 67.274 HH 0.089 780541 67.173 67.550 2 68.240 PH 0.080 3034043 68.091 68.268 Q 3 68.343 HH 0.089 7638730 68.268 68.564 4 68.668 HH 0.092 379485 68.564 68.790 ~ 5 69.114 HH 0.093 7365278 68.911 69.282 (J 6 69.825 HH 0.088 2229536 69.569 69.973 tJ P' 7 70.469 HH 0.096 3311299 70.248 70.764 .-+ P' 8 71.362 HH 0.117 599087 71.235 71.486 ~. 9 71.869 HH 0.094 605304 71.734 72.019 (þ '"0 10 73.242 PH 0.106 351634 73.111 73.371 0 11 73.524 HH 0.078 398960 73.433 73.611 =:4. 12 75.246 HH 0.091 325893 75.088 75.354 N 00 . 13 75.596 lIB 0.089 341860 75.526 75.758 v-. ~ P' (JQ (þ ~ W 1'0 o ~ 1'0 .þ.. 0\ rbÙndar;cë-" _,..,......__,..,..n' _..u___·__...____·~·..··_· ____._...___u_._u. ~~-~--'-- ._._-----~-----_._---- -- ------------- ----- --- - - - -- ----- Qi ~¡ 01 di ~¡ P'¡ ~¡ CD¡ ~j oj ::¡¡ Ni 00 j v-.¡ Ion ·182.1 o {181.80 to 182.80): A9900009"D 6f.34 69.-11 125000 120000 115000 110000 105000 100000 95000 90000 85000 80000 75000 70000 65000 68.-24 60000 55000 50000 45000 40000 69.H3 35000 30000 25000 7lt 4-7 ~¡ c§ ~¡ w j w¡ oj ~¡ N¡ .þ..¡ 0\1 20000 15000 67.27 10000 7L3B 71)37 7352 50:~I"~'~m~¢r,-r, ,ÿC" ,~, ,~"~~X\~~,, 'I ,~~~~5,~~""""" ,,~~J tTj~~je~.-:?:.,._ ..... ,_,_f}§':~º__f>.Z~ººnf>.!}~~L~8:.ºg...§-ª-:?º_~9.0ºJ:~~~ºJO.{)º-...z<l:,~!>-..L!,.OO 71.5(L?~-00 7~:~º_.zª:.º-0_..~.:.!)-º-Z~º_Q.. 7 4·~Q,Z5.00_ 75.5º-z..~~9.,..?6.!iº--7Z:.º-º_,J7 ·!?,!L!ª:.9.!>_?.ª.:?-º..]~:º,º,_Z~~..n___¡ Ion ..231.20 (230.90 to 231.90): A9900009.D 98R00396 ARO Peak# Ret Time 'rype Width Area Start Time End Time 1 90.489 PH 0.055 108429 90.415 90.640 :2 91.935 HH 0.075 95278 91.8.86 92.001 3 92.085 HH 0.102 130381 92.001 92.168 Cl 4 92.450 HH 0.088 381911 92.335 92.542 ~ 5 92.664 HH 0.164 209420 92.542 92.812 (1 6 93.032 PH 0.130 437359 92.900 93.213 0 P' 7 93_278 HH 0.101 83502 93.213 93.421 .-+ p) 8 93.711 HH 0.072 72837 93.680 93.851 ~ 9 94.126 PH 0.086 71295 93.992 94.240 (j) 10 95.307 HH 0.078 200362 95.237 95.449 '"0 0 11 95.613 lIB 0.077 78010 95.517 95.674 ;¡. 12 95. 771 HH 0.085 131164 95.674 95.862 1'0 00 13 96.014 HH 0.105 262472 95.923 96.288 v-. 14 96.374 PH 0.069 148807 96.288 96.452 15 96.721 HH 0.074 80516 96.662 96.810 16 96.937 PH 0.102 134944 96.862 97.070 17 97.201 HH 0.089 170770 97.070 97.273 18 97.793 PH 0.118 173014 97.659 97.862 19 97.957 HH 0.083 71678 97.928 98.060 20 98.128 HH 0.066 76128 98.060 98.195 ~ 21 98.443 HH 0.088 226151 98.363 98.581 p) 22 98.779 HH 0.077 262799 98.671 98.891 (JQ CD 23 99.007 PH 0.093 143209 98.891 99.130 ~ 24 99.450 HH 0.114 248485 99.383 99.635 w .þ.. 25 101.299 HH 0.075 77246 101.264 101.441 0 26 104.411 PH 0.138 90662 104.332 104.678 ~ 1'0 .þ.. 0\ '.', ..... ~ -. ...- - . ~'GïJ¡:;'dãr;¿e'---' . . _._._ .u.' .......n .___.. __. _~ _.... _.. .._ _. _..__.~._. ...__ _.__..__h_.______.·____··____ 6500 6000 5500 5000 4500 4000 3500 3000 2500 2000 1500 1000 5~1' ~ \J L ~ I ),1, IT.~~~~.:-~~ . ..._ ]~.:º_9.__.!.8.~9º.__._ªº.!>_º..__,ª.?___ºº__!!1,:.ºº_.. 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P'¡ ~ ~¡ ~ N 00 1 ~ ~ ~ ~ ~ ~ d ~ N» .¡::¡.. 83.80 \ 340000 320000 300000 82;72 r 280000 260000 240000 220000 200000 180000 160000 140000 120000 100000 80000 60000 40000 20000 i O~I ,-" '1 '-'-'-"-;-"YI~" ,-or~"..-n«.,."., ,,-, '-In,' ,~, roT,J·'T~" I'" """ I"" I"" I"" I"" I"" I"""", Ii rrïme--:.>:..!JJ_~º.._ªJ:~º .J!,!:.1.0 81.60 ß 1.ߺ .. _~:Qº- ª_~:?O _J!?.40 _ª-2.:_~º..J!~ª-Q. _ß3·Q!Lj@.:~_º_,_®:.!<L_ ß3.:~Q._.f!.~~q __ªi·º0_ª-4:~º- 84.40 ..84.6º.. ª-1·ª0 -ª-§:9.Q__~:?-º_~:1Q_.!J~.60 _ 8_!?~§Q,__,__.: Ion 182,10 (181.80 to 182.80): A9900010.D 98R00397 ARO Peak# Ret 'l'ime Type Width Area Start Time End Time 1 67.255 PH 0.097 685524 67.089 67.461 2 68.339 HH 0.110 11720453 68-.-079 68.5/8 a 3 68.672 HH 0.090 227147 68.578 68.757 ~ 4 69.103 lIB 0.089 5894320 68.940 69.408 n 5 69.816 HH 0.086 1357217 69.625 70.067 tJ 6 70.458 HH 0.092 5630468 70.316 70.813 P' 7 71.370 0.076 1361999 71.188 71.430 .-+ PH ~ 8 71.487 HH 0.101 1137134 71.430 71.717 ~ 9 71.853 HH 0.093 3285730 71.717 72.003 ~ 10 73.219 HH 0.112 335059 73.030 73.331 0 11 73.517 IIll 0.091 228325 73.331 73.663 ~ 1'0 12 75.237 PH 0.079 242008 75.086 75.333 00 13 75.850 HH 0.096 274019 75.763 75.945 VI 14 76.397 HH 0.095 435079 76.292 76.544 ~ P' (JQ (þ - .þ.. --...J o ~ 1'0 .þ.. 0\ rbu:::::---·--··-------····----;,=;~- ----~- IOO182~10 {~81~8-Òto 182.'8'0): A990õ01U.D ~-_.--- _.~~~~~-'----'--'--_._-----'~-q ~ Cl d P'¡ s¡ ~ ~I ~ N 00 î 140000 130000 120000 110000 69,10 100000 60000 71.85 ~ Jð¡ (1)¡ ~ ~ <Xf 01 ~ N ..þ. ì 70A6 90000 80000 70000 50000 40000 30000 71137 69.02 2??oo I 71.49 10000 ß7.25 ~ __ 7':S 0", _~ 7"- ~,~ _.- _ 76.40 ¡ ß!~ Q' < ~_2._.. :)/ . o.<::.'~ ì" R~ , O·~ ~".~I..¥'~r,y'r~l \^r,'r~.'~~~~~fl ._f?_~:.~_º,ßX:ºº_~._5.Q..§!!:.().º._~.º~~º,...§.ª_~ºº,_~~§º_?'9ß0 .Iº:.50 71·.º9 71_.,§,º__Z.~00:..?2.50 ~3.00 73.50 74.0!L?4.50 ?'?...:Q9_75.50 76.00 I.t?:.?O 77.00 Z!:?º,..Zª.:º--º--.~·5()__.?9.00 7f!:~.Q,_,_.....J ¡ frime--> IOD'231.?0 (230.90 to 231.90): A9900010.D 98R00397 ARO Peak# Ret Time Type Width Area Start Time End Time 1 90.489 PH 0.058 225541 90.354 90.800 2 91.948 HH 0.072 258864 ..9.1_823 92.0-1-4 C) 3 92.064 HH 0.057 116115 92.014 92.185 ~ 4 92.456 HH 0.084 925786 92.361 92.539 0 5 92.599 HH 0.060 209646 92.539 92.638 d 6 92.722 HH 0.082 243969 92.638 92.777 P' 7 93.069 PH 0.095 936647 92.876 93.177 .-+ P' 8 93.278 HH 0.094 204287 . 93.177 93.380 ~ 9 93 . 620 PH 0.062 105125 93.533 93.672 (1) '"0 10 93.713 HH 0.075 144593 93.672 93.865 0 11 94.133 PH 0.066 148391 94.004 94.213 :4- 1'0 12 94.435 HH 0.066 314957 94.367 94.522 00 13 94.952 HH 0.091 279824 94.777 95.093 v-. 14 95.180 HH 0.069 116168 95.093 95.214 15 95.311 HH 0.083 394352 95.214 95.450 16 95.602 HH 0.096 264401 95.450 95.713 17 95.764 lIB 0.081 223657 95.713 95.872 18 96.015 HH 0.085 478206 95.872 96.107 19 96.392 HH 0.079 398272 96.255 96.476 20 96.968 HH 0.095 224265 96.865 97.040 ~ 21 97.102 HH 0.059 130295 97.040 97.135 P' (JQ 22 97.211 HH 0.070 284799 97.135 97.282 CD 23 97.792 HH 0.072 256613 97.650 97.827 I--' .þ. 24 98.452 HH 0.088 284886 98.380 98.600 \0 25 98.774 HH 0.078 421447 98.682 98.922 0 26 99.468 HH 0.134 301450 99.352 99.627 I-t) 1'0 27 105.671 HH 0.069 115108 105.614 .105.789 .þ.. 28 106.335 PH 0.079 108559 106.202 106.467 0\ .------'--~.,..-..-..-..-..--..-.--.-'-..-'--'-'-------: Îuñ--:231~Q123õ~:go..to-æ=r~90}:A99Uooío.n" ,_..'~~~='~~~- 9:L46 93J}7 .__~.__"_~=~-=...;.o;...~_~~___:........;.:...:.:~::..::::_:-~::...:-_..-=---:_~ ~\ nj ~I .-+ : P') þj¡ CD¡ >ö¡ o¡ ~j ~¡ Chi 18000 17000 16000 15000 14000 13000 12000 9000 Gô.û2 98.77 ~¡ p,¡ (JQ ¡ 01 ...... ¡ u-.¡ 0) o¡ ........ ¡ tv! .f;ò..j ~I 11000 10000 8000 94.43 95~31 ~6~39 90.49 7000 97.21 91.~-i..5 3000 g:~.e~} (;]1 ¡?'. ~ . - 'A~&~" CJ5. '?(9it ')7 v~.~ --- .. q. - q 1· ('n° 1(. I '"......{~L _~"):""") ..=;_4.. ~ -'1 ~-:>-c~Û;-~ ~'3~; 9511, .. ! 97]9 98.'''-5 6000 5000 4000 99.47 I 105.67 j 06~33 ~ ~ 1000 ~lh~,JI hi I~ I I, ,III! ».111 II II ' ,~Il \¡¡¡ "116, - J JL L t 'A· J' J~' *"ij( ¡J~J.J fJktl ~ £Ù)·J Jill JI~1 o ~ J 'I 11. ~~þ~ - · III . .. . I ,," .." I .. .. I ".. .... I ... .1.. I " .. I 1 "" J I!. In, ..1, ~í.~r.j?,~.~.?:.... . Jf?:ºº. ._J.!l-=ºº__.ºº~º-q.._...º?:.o.º-_..ª~.:9-º-......J!§.:ººu_.-ª8.00 __ 90.00 __,!g.:ºº___~1:º,º-__, 96·9..9 98.00 100.00 102·o.9_!.Q1·00 1 06.QQ,...1ºª:ºº,_!J.~QQ_:!1~.ºº_..! 14.QQ.,..!.16.QQ...J 18:-º9..._____.J ..-... .0:-..-"'-. -~-.-7~"" 'I." ,," ..;. ..--. ...... ". .n 230.20 (229.90 to 230.90): A99000l0.D 98R00397 ARO !ak# Ret Time ~ 8~,101 Type BH Width 0.088 Area 309155 Start Time 80.952 End Time 8l.223 ~ n d :I) .-+ :I) :::0 CD ÞOt:j o ::4- tv 00 U. ~ p:¡ (JQ CD ....... VI o H) 1'0 .þ. 0\ I , I I I L i jl I ! q ¡ ¡ i ¡ ¡ ¡ ¡ ¡ 1 ¡ / ¡ ¡ ¡ I f ... r 1 I i-r-1 t I j I I . I 1 I I , I I I I I I I I , I J I I I . I'" I I I r I ¡ I 1 I I C I I I I r , I I 'I,. I I I I a I r .., t ' I r r J . I I I E ??:ºº_____..!!:~,º__Xª~º()___J,ª_:?()_.,__Z!!~9. 79.50 _ 80.00 ~~º--___ª_1·Q9_,__ 81.50 _Æ·OO _!J2.50 __--ª3.00_-ªª.:~O 84.º-º--~.5º--_ª--~ºº,..__..ª~ßO _..,..__J ____u_____·__··___··~. _..._....._.. ríme--> 76.50 o I " þ ~ I 500 1000 1500 2000 4000 3500 ~ P' (Jq CD ....... 3000 v-. 1'0 0 ~ 1'0 .þ.. 2500 0\ . Cl ~ Q d P' .-+ PJ ~ CD '"0 o ::4- tv 00 v-. 4500 5000 5500 6000 --:---.~---... }i.ïñ(tËir~CB-" ---....... ..-.......,.- ,.....'..'-....-----..-.... ·....·....--'..-....·'..'..'-----....'---'-·---·----·--·Îon 230.20· (2.29.90 to 230:-9'0): A9900010.0 - BL1û r~:=:---···__·m_-.-......------------------~------ . T!ëÕA9900õ1'EO=-9:RO=ARO------- ---_.._.-..--- =-::.:._c.;...:.c;'_-'--__',..,.__Q ~ (1 tÞ ~ ~ ~ :;þ (þ ~ o ~ tÞ QO ! 2800000 2600000 2400000 2200000 2000000 1:; pp ~ q> Þ-!-> VI tp Ó '"tf1 tU .þ. ,... 'II I ' 4??oo0 20??oo ~~.dJ~,,\l,) ,Jj J ¡~ J. ~ t I ¡t,IJ~¡;¡..,1~ O· I , 1 . I y-r-, I I ' , . I I I I I I I I I I I I I I I I I I I , . I I I I I I I I I I I I I I r t I I I I I I I I I I I I I I I I . I . I I I I I I I I I I I I I I I I I I I I I I I I '. I I I I J f I I . . I . I I I j ª tD!'Q?.-_-,~.__._.._._._...~?__ºº .;!Q:9.Q ..__ª,?~º_(L....1º:9_º~~0_º_._~·9_O'.._,~~·00 _f?_0.00 _ 65.00 __?O.OO _Z~º-º___...._ª9·0Q.__l!5.Q.Q__ª_0.00 _..Q§j)Q...JQQ,:f>-º__!'Q§:90 ..11 0.00 _!.1..~~Q9_....!.~.Q.~º!L,!.25·_ºº___1 1800000 1600000 1400000 1200000 1000000 800000 6??oo0 IQQ 156~10 (155.80 to 156.80): A9900011.D 98R00398 ARO Peak# 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 Ret Time 55.164 55.326 56.935 57.690 58.047 58.346 59.371 59.595 60.514 63.578 65.235 65.776 66.411 66.856 67.415 67.676 68.817 Type PV VV PV VV VV VV W VV PV PV VV W PV W VV PV VV width 0.117 0.112 0.154 0.120 0.110 0.108 0.093 0.135 0.115 0.104 0.100 0.098 0.130 0.095 0.087 0.081 0.100 Area 1282603 '1-1.2344 31417462 14585815 13490626 21170915 1859482 11310490 1926071 483351 1385953 1479702 1020954 1143395 730907 356348 587866 Start Time 54.945 , -55-..-£,0 56.643 57.496 57.863 58.177 59.113 59.426 60.315 63.443 65.109 65.639 66.265 66.707 67.298 67.561 68.690 End Time 55.270 . - -S-S-:65-4- 57.157 57.863 58.177 58.656 59.426 59.895 60.724 63.691 65.533 65.946 66.608 67.126 67.561 67.804 68.969 Q ~ n t:1 P' .-+ P' ~ CD '1:S o ::¡ N 00 v-. ~ p.:I (JQ CD ~ v-. .þ.. o ~ N .þ. 0\ Ál)tir,ctar;G8-·'-·--_·__··,--_.._·_...._·_~,·,·_..__·_..---....'..........-...---~-... 56..94 280000 260000 240000 220000 200000 180000 160000 140000 120000 100000 80000 60000 4??oo 20000 55.16 Å>,,33 o~r~-T~·i -r-I"'i') I IW !!:!fIi~~__:~':~~.~ºº. .. §?~ºº. .. .....,§~~ºº. ....~:rº-º_... 5Et35 --1ŒrrÚ~(f.'it)Ti55Jmlo'156.BO): A9900Õ11~Ö..-'==--===::- 5~7~69 5B.O!-~ 59.60 , 5\~7 6051 . ~r.' I LLL_1~~ I I I r I I I I I I I I I I 't. I I I I [ --. I ...h..,~~Qº....,......,_§~ºº-,_.._~_:9_<2.,.._,___ª~ .00 _~.._62:..Q!L 63.00 -----'··'·'..·----·--··---..'·-'--'..---'-'---··-'--..0 ~ Q ê1 p.:¡ r1'- P:¡ ?Þ .g d ~ Ñ ob i Þ-b ~ (Jq q ~ ch ~ Q I-h Ñ ~ i 6S2J~ 66.416685 1 I I ,____,~1:.Q-º--._~}lº___.._ß6.00 __""._, 67:Qº_,_,_.~&º-, ¡§ ......._@.:.9.Q....___j IQn 16g.10 (167.80 to 168.80): A9900011.D 98R00398 ARO Peak# 1 2 3 Ret 'l'ime 62.180 63.063 64.763 Type BV BV PV width 0.103 0.101 0.112 Area 16898980 _6459238 2464061 Start Time 61.921 6,2 ;'8-"7'1: - 64.558 End Time 62_486 ô3~-2'43' 64.974 a ~ n d P' .-+ PJ ~ (1) '"0 o ~ 1'0 00 v-. Þ-c:J P' (JQ (1) ÞO-' v-. 0\ o ~ 1'0 .þ.. 0\ rb:~::::-.-.-- -.--.----- 220000 2??oo0 180000 160000 140000 120000 100000 80000 60000 40000 20000 e_i.~T~~=~?:. ..-_.__._---._..__......_-~-_._-------- -----!m:1 6ß.-:-",o.~-67 .80 to:16a.-B6): A99OOO11.U- ,. œtH3 b ~ (1 b þ 1-1-- P' po (D "ö o F4- N 00 í to þ) {JQ FD ï-- U. ~ Þ ~ tv ¡.þ. P' . - ----------...------ 63.06 64.76 O~'I'" 'ì~~·I"'..·í"'lIll ('¡ .,..,{, , "I'" 'I' ""I' " 'I' "1'11"""1' "1' "" ,.~"..p'Í' 1"1' 1'" T~~~î~"i'1í¡ __,§º:.?º,~O':1.-ºß9ߺ.§.9.~º_.<.>J_~º_Q..()J:?.Q~!::'!9_~-=,~~§J .80,_62.00 _62.~0 ~2.40_~2.6º 62:80 63.00 6ª~Q-ª-3.4Q.,~ª-:.® 6.ª-.80 {}4·º~L~·20M~º~.J>-º-§1:ª-ºJ)~:º-Q..65.gg 65:!º__I?§~ªº-§~ª-º-,_J Ion 178'.-10 (177.80 to 178.80): A9900011.D 98R00398 ARO Peak# 1 2 Ret Time 78.406 78.630 'l'ype PV VV Width 0.089 0.118 Area 47213426 4'7005-6 Start Time 78.214 ,'HJ;;-6~ End Time 78.609 '-ï-S~853 C1 ~ o d P' .-+ p:¡ ~ CD '"0 o ~ 1'0 00 v-. I-d P' (JQ CD ~ v-. 00 o ~ 1'0 .þ.. 0\ - __n_. _ _..n._ ...___.____._.._._______.__ ...____._.__·_n --.---------.--------..---..--.------ 1<m-tTR-16i'1=rT:801uÎ78:8O)~99OOÖTID' ..- 7~~.4 i --·-----'----'---0 ~ (þ tj ~ ri p:.¡ ~ (IF. '1::1 Q ~ Ñ 00 ~ 750000 700000 650000 600000 550000 500000 4??oo0 ~ P'i (JQj CD! ~ tA \Cf O¡ Hi¡ N ~ 1 450000 350000 300000 250000 200000 150000 100000 5??oo o "., r I , . rfPi . , I I I , f I I . 1 ) I ' I , 1 ~ ,"I. (11 I 'i? ,"I I f'I"-' 'Î ~ I I I I . i , . ( I I . , I I I I , I I " I ' , , 'I . . , , I . 1 , . I . . -. , I . . ., "" I ' 1 ~. . , I I . I , . I ' , , '1 r I , I . . , . I ,--,;-;-1 ITíme-->_.__... __,Z.f?:.?Q..If?_:1º1~.__()_<!1f)·.80 Tl..:.ººTJ..:.?:º_.??.:4!JIl·60 J..Z~_ªº..z!!"go 7~~0 TIJ_:'!O ~ª=~.º..?8.8º-?.~.OO ?9.2-º_?-ª-:,!º..Z~.:§'() 7R-ªº. 80.00 80.20 8~~9 80.6Q. 80--ªºJ1~..:.º-º-ª.!:gº_lD.::.~ 81.()Qß1.80__.J Iqn 192..10 (191.80 to 192.80) : A9900011.D 98R00398 ARO Peak# Ret '1' ime Type Width Area Start Time End Time 1 82.721 PH 0.090 17700568 82.344 82.937 2 83.131 HH 0.092 21839355 -ª-~. 937 83.480 3 83.800 HH 0.092 --2217' 4 7 ~i9 83 . 637 83.883 4 83.981 HH 0.081 17092931 83.883 84.130 "0" ~ (1 tJ P' .-+ P' ~ CD '"0 o ::¡ 1'0 00 v-. ~ P' (JQ (1) ~ 0\ o o ~ 1'0 .þ. 0\ 380000 360000 340000 320000 300000 280000 260000 240000 220000 200000 180000 160000 140000 120000 1??oo0 80000 40000 20000 60000 ¡ 0 1Tlrr!~=~~_¡J 1.0-º_ J3..1.~?9.._ª).:4..º.u ..-_.__.-._--._--_._---~------- 81.60 J~JA!O ---Jëft'H~~1-o-ttit ß0101'921JO}:-AffiJooõ1ï]J-- n ,. 83.13 Ba.8û ------.-------- -------------------~---~- - --·-'-----'---'----Ö ~ o tj ~ .-1> P'¡ ~ (DE "ö o ~ N 00 Î 33.98 62,"?2 'ï:; ~ (Jqj ~ ~ d. '"'i' oj ~ to ~ ~ ) ~ \ I 1 . Î"'I. '1'-'''"'1 [,', [/" I"" '" I I" [, I'~' II I' II. 1" ,JJ!!.<!.<l.. -ª-~·.?9 ,_ f!?~Q_ _¡J~&º-- _ 82.~Q_83.0Q._~3.20 _-ª-~40 .. 83~~-º-...!!.~80 _.._ª.1~QO , I . I I I I I I I I I I I I . t I I I I I I I . I I.' I I J I I I I I I I I I I I I f'ï¡ ~ 84.20 _ 84.40 _~§'º_..84·ªQh--ª~-:.9_Q..., 85.20 --~~~-()-,-EJ.~-ªº-_~~-ªº____.l Ion 182.'10 (181.80 to 182.80): A9900011.D 98R00398 ARO Peak# Ret Time rl'ype Width Area Start Time End Time 1 67.246 PH 0.085 479173 67.159 67 .349 2 68.330 PH 0.lQ2 ' _,~5_46.138- ---6-S-.-1G-3- - -6-8-;-4-8-6' -- u ' .- ------------.-..------- ----.-- -_._--,--- _____Un_ _"._. __~_______ 3 '69.098 PH 0.084 4388645 68.893 69.253 a 4 69.811 HH 0.074 903478 69.702 70.038 ~ 5 70.452 PH 0.088 5426392 70.168 70.715 n 6 71.361 PH 0.090 1455544 71.192 71.423 tJ P' 7 71.481 HH 0.081 1200324 71.423 71.711 .-+ P' 8 71.850 PH 0.091 3493198 71.711 72.018 ¡o 9 73.206 PH 0.060 122332 73.018 73.352 CD '"0 10 75.247 HH 0.070 178183 75.166 75.393 0 11 75.833 HB 0.100 240202 75.730 75~948 ::¡ 12 76.403 HH 0.087 359182 76.286 76.612 1'0 00 v-. ~ P' (JQ CD ~ 0\ 1'0 o ~ tv .þ.. 0\ "':"1.48 ¡ 2??oo 69.81 r I ¡ 1??oo 67,i.25 '" _.... ." I i~4v g I T{ 2-1 75.25 75.83 ¡ o·v, , r"f"'" "'''''',' 1"',...". ~,,':'-:-¡~~'~"1~.-.-¡~~<'<'''*''~~~~~~! ~í!!1~~:':>'n_. .._ ,._~!1_·§_Q...~?:ºº...~3}...:?-º...~.EJ.:ºº....~-ª:~º_~~:9J>_ 69.50 _ZQ~º-?9.5o. 71.QQ-71.50 72.00 _Z?50 ~.0<L?.3.5º,.z±=º-0_?4.50 _.z~:º0 75.50 .z~.00 76.50,lZ:!!º Jl.-É_º 78.ºº-:n~~~_,z~~OO ,}9.50 .J _'~"'_~O~'~_~~=_ -=- -- '----- --0 2t: Q t:Þ ~ rl- ~ ïÞ (!¡ ~ o ::+ ~ I 'i;1 ~ (Jq ~ ~ Q\ up d ~ N> -ß. OÏ\ 71.36 3??oo 4??oo 50000 6??oo 71.85 70000 69.10 80000 90000 ïOA5 100000 110000 120000 130000 ..-·-·-'--..,-----------..------------------=:'km--1&2:::+õ{+&t.-BtTtö--.:t82~OO):-Å990bOfï'D- ====~~~ 68.33 . ~bür;:-d~oC'i3-'-'- -..,---.... ¡ 140000 -_.------"---.--_. Ion 231'.20 (230.90 to 231.90): A9900011.D 98R00398 ARO Peak# Ret Time Type Width Area Start Time End Time 1 90.481 PH 0.051 144520 90.367 90.569 __ _u__" __._n_ ,_ _ ___~ 2 91.939 HH Q _. 068. ,. . . 2.4.5Ji-9-8. ' - u_ -9-±- ~'-f-&Ð- - - - ---------~---~-- -~ - --.---------- ---n-:-tìfJ9' um _u Q 3 92.460 HH 0.081 888371 92.349 92.544 s: 4 92.644 lIB 0.112 276479 92.544 92.703 n 5 93.048 PH 0.122 860329 92.921 93.202 t:1 6 93.281 HH 0.106 208860 93.202 93.540 p:¡ 7 93.718 HH 0.089 177914 93.646 93.932 .-+ p:¡ 8 94.145 HH 0.086 160804 93.932 94.210 ::=0 9 94.433 HH 0.080 510649 94.333 94.598 (1) 'ì:1 10 94.917 HB 0.109 346225 94.780 95.049 0 11 95.171 HH 0.109 197154 95.049 95.234 ::¡ 12 95.305 HB 0.113 353879 95.234 95.490 tv 00 13 95.603 HB 0.089 217075 95.490 95.700 Ut 14 95.767 HH 0.089 215102 95.700 95.881 15 95.993 BB 0.114 434446 95.881 96.140 16 96.385 HB 0.079 290895 96.281 96.453 17 96.959 HB 0.106 308113 96.834 97.059 18 97.115 lIB 0.075 141448 97.059 97.151 19 97.197 HH 0.135 565332 97.151 97.627 20 97.755 HH 0.127 379607 97.627 97.878 ~ 21 97.961 HB 0.085 212349 97.878 98.037 P' (Jq 22 98.100 lIB 0.106 181894 98.037 98.218 CD 23 98.462 HH 0.087 382148 98.368 98.608 0\ 24 98.776 HH 0.079 361660 98.677 98.856 .þ.. 25 99.437 HH 0.067 139903 99.371 99.486 0 26 99.518 lIH 0.088 174391 99.486 99~619 "'""t) 1'0 27 105.662 lIH 0.075 121290 105.606 105.729 .þ. 28 106.338 lIH 0.075 147196 106.213 106~445 0\ ; 2000 I ¡ I' ¡¡~ " ~ ; ~ . 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Q--:' 1" á'li £4 ~ I ;rt. ~\ "oJ , g3.~ .4 ~.,.. g.;; 1- 4000 .93.72. 9~.fj 1 5000 90.48 9~ªé19 6000 91.9l 97.20 9fL~·6 7000 98.73 8000 ~ p:¡¡ ~I ~ 0'\ o o¡ ~ N ~ Oi 9000 10000 94.43 11 000 93.05 12000 13000 --------,·,----'---a ~ C1 tJ ~¡ s¡ ~ j N 00 tA 14000 15000 16000 17000 ---..-,..--------..-----·------~fl:'231_.20(236:001Ó-231~90}~11;990ÖtJ1f])-~-~~---- 92.46 . f\btj"ñ'danc·i-----..-·-- --,--.....-... ~on 230.20 (229.90 to 230.90): A9900011.D 98R00398 ARO Peak# Ret Time 1 81.104 Type PH Width 0.080 Area 293503 Start Time 80.802 End Time 81.205 Q ~ n d P' .-+ P' ~ CD '1:S o ::¡ 1'0 00 v-. ~ ~ P' (JQ CD ~ 0\ 0\ o ~ 1'0 .þ.. 0\ · ' \ 5500 5000 4500 4000 3500 3000 2500 2000 1500 1000 , 500 hlrr,-e~-::::.n ._._----~---_.._----------- ----~----~..-.......~-_.- Ion 230.20 (229.90 to 230.90): A9900011 ~D 8i ;tD - O----rõ T. J, . - ,. I . 1 I I' I. I I 1 7~~!?º. __"...?l:9-º___....rr:~.9.,_ ..Iª-=-º_!L_,_1:ª~~º,__J_9.00 I I I .1...,,,.1' ?~50 -----ª.Q.OO --ª-º=?-º-... 81.00 _ª 1.50 __~._._.__.._.__.___..._'_o..-.&..~_..,-._."..."",,____.,,~__..__._~___.~ jQ ¡~ jn I~ 'r+- p þo rD' '1::j D þ: hJ 00 r ~ Pi> (JQ q ~ d\ '~ d ~ N> .,J::¡.. , . ) . . . . I I I ,I T. I I . . " I . . . I 't . I j . T I ~ 'r---'t- . ¡ 82.00__~_50 ____83.qº.___,ª~®___._ 84.º9_,_.84.5-º--_~§.:ºº__ ...._ª~_50 __, ¡ · . ......- ...__.~ ...." -~ ...-.... .h. ....._....__._.~..._.h_..._......___.._....__._._......____n.---....--- T1C:A99oooI2.D~· --- -----_._-_.-.._--~._._. ~-~~~b ~ (J b ~ ~ IoQ b .þ. tv Do T í:::: 98R00399 ARO 2400000 2200000 2000000 1400000 h:1 ~ (tQ p ~ !O\ þO b ~ !tv ¡.þ.. 1800000 1600000 1200000 1000000 800000 600000 400000 I 200000.~ ~~'¡''¡f w,t).,< . . J r ~ n, Jt I~, (~¡. M~ t..11 '. iU,~.1k J I.. ..., ~ 1\ ~'Y'~ \~~ ~j~ !II IF'" -"~I o , . , , ( , . I r ( , . I I I ' . I r I ' I I I I I I I . I I , . I I I I I I I I I . r , . 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OAI.AA,rt'4~A-f'~1xv0~~,.lI.¡,I.111 '1"11 "'1-' '1' 'I' I'I'I"I""J_II"'I"" 'II'I~I 1D!~~~~.::..._.._. .._f3.ª~5ºJ~.?:ºº_.p!_.§º_§ª.:ºº_._~~~-º.._6_!!:Qº- 69..:~-º_1º...:..~Q_Z<1..~..L1·00 _I.1Þ.<L 72~-º-_Z.~~0 73.OQ. 73:.5..Q-Z 4·Q!L 7 4_~º--75.º-<L!.~50 76.00 '!'~§Q_..ZZ~º-º_~~50 _~..:ºº--?~.?O ..?J!:_º,º--?~:~,º___.., J Ion 231.20 (230.90 to 231.90): A9900012.D 98R00399 ARO Peak# Ret Time 'l'ype Width Area Start Time End Time 1 91.939 PH 0.089 127152 91~838 92.022 2 92.455 HH 0.096 306290 92 . 3.5.2 ~ ~_.-9-2--.~9- a 3 92.707 illI 0.132 ' -r:r225-~f" 92.599 92.767 ~ 4 93.078 HB 0.107 320617 92.935 93.148 n 5 93.267 HH 0.116 138729 93.211 93.424 0 6 94.148 HB 0.092 111147 94.010 94.204 P' 7 94.286 HH 0.096 127175 94.204 94.350 .-+ P' 8 94.442 HH 0.103 329873 94.350 94.582 ~ 9 94.955 HH 0.117 248483 94.837 95.099 CD '"0 10 95.304 HH 0.113 321199 95.188 95.493 0 11 95.600 HH 0.082 198250 95.493 95.669 :4- 1'0 12 95.770 HH 0.110 195950 95.669 95.859 00 13 95.956 HH 0.134 403458 95.859 96.155 v-. 14 96.369 HH 0.065 127569 96.322 96.434 15 96.731 HH 0.071 106640 96.689 96.792 16 96.949 HH 0.112 235192 96.792 97.013 17 97.194 HH 0.156 457297 97.013 97.332 18 97.410 HH 0.074 200647 97.332 97.469 19 97.498 HH 0.127 189392 97.469 97.620 20 97.759 HH 0.066 188331 97.712 97.813 ~ 21 97.842 HH 0.085 168643 97.813 97.917 p:¡ (JQ 22 97.954 HH 0.076 180249 97.917 98.033 CD 23 98.122 HH 0.095 287220 98.033 98.192 ~ --.J 24 98.453 HH 0.135 558690 98.285 98.583 \0 25 98.765 HH 0.091 392744 98.689 98.918 0 ~ 26 99.038 HH 0.101 496784 98.918 99.141 1'0 27 99.306 HH 0.143 310720 99.141 99.365 .þ.. 0\ 28 99.457 HH 0.097 195398 99.365 99.501 29 99.529 HH 0.090 167380 99.501 99.616 30 101.236 HH 0.105 159870 101.190 101.389 31 101.536 lIH 0.086 264920 101.466 101.659 32 102.107 HH 0.102 166793 102.029 102.166 33 102.940 HH 0.151 191491 102.784 103.036 34 103.097 HH 0.161 202856 103.036 103.274 35 104.454 HH 0.107 173099 104.399 104.669 36 104.914 HH 0.105 112794 104.793 104.999 37 105.172 HH 0.140 165274 105.104 105.366 38 105.644 HH 0.092 135434 i05'.583 105.731 39 106.319 flH 0.130 161487 106.253 106.462 40 106.802 HH 0.119 166863 106.718 107.018 41 109.055 HH 0.120 130485 109.023 109.272 42 110.439 HH 0.146 122873 110.232 110.509 rbUr:::, ... .--....- _.... ..-.... - ......... -.- '.' ..__._....__...._....__...._..--_..._.____.o____________. .~---_._-------------~- ~~~~~-=='-",=,-.::::::-=-.._--_._- ~1 n¡ ~¡ M-: P'¡ ~¡ (Pi "01 01 ~¡ ~¡ P'1 (Jq 1 CDj ~i 001 01 gJ Ni ~ _lon23.1..2O-{2-30-9(}..t~GT:--A99000l2jT-- 99:.04 88..:-6 6000 98ßti 5500 5000· 92.45 94.44 95.96 101,54 4500 ..93JJ8 9~lç2( 97..1:1 4000 95..3{ 97. - .3 %.t¥0-37 ~;9A6 3500 .0 c!5t.:?ö3 3000 l4.~~J (1)6. Þ ,ô.l:'i .~ 1 02.11 94 ¿~. 9 L27 'I lOi . ~4 2500 91.~ 104.4WQ&.32 1 C:2.94 fOB.eo 'Ok10 W5.17 :1:: I ¡lll,' ,:i!:: ¡ ilL I ï ¡.. , ¡, '.~:! ..::1 ,!!;:i:.' .:.i':.! :.¡:~ ;' " "I d: lltuJ !~]J II lu~ L 109.05 1 ' 2000 Qi} ;It , ~..,._., . 94.- 5 1 1 ,}~.; ~ 110.44 1500 " I ~1, JL~,_J,Ji, I-n;."~ ....ª?.:.ºº__... 84:ºº-_,~6.Q9__...88.0Q_,J!Q-=-()Q.. 92.0~:ºº_.._l!..6.:00 ..',t "1""1""1""."" ""I' " ,/'\, f 98.0L100.00 102.00 ....1Q!:!1º 1~.OO 10!!:ºº-~10.0,º- 112.00 11.~:,QO_J16.00 118:ºº-.._, .. ,l . l : . I ~. .. .. : _ T -,4 ! ','. ~.~t'·1,~' - j ;;, , , 1. 1 j ~J' l: . 1000 . . I I I I tr!!2?~..::?:....,_._ _..?~:.ºº.._..z.f!:,()_º,..__!!º .00.. 'Ion 230.20 (229.90 to 230.90): A9900012.D 98R00399 ARO Peak# Ret Time 1 81.105 'l'ype PH Width 0.079 Area 251768 Start Time 80.787 End Time 81.223 --- .---------- ------, - __ _______ _ _ n 'C') ~ () d P' .-+ ~ ~ (1) '1:S o ::¡ N 00 v-. 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End Time 72.894 ____~_________._ _____ _____.___________u____ __________.___.__n_..·.__._·____u ._ u_ __"_ _ ____u.__._ ,--0- - ~ n d PJ .-+ PJ ~ CD '"0 o ., .-+ N 00 V'I ~ P' (JQ (1) tv ~ ~ o I-+) 1'0 .þ.. 0\ AG-üñ'd'anGe-------'-'-.-----..-.--..'..------'--'--'...---_u___ I ::: _1-º11.2.l12.Q...(2i6_jml0_2.rr.9..01:~S9..9,o!lQi2.Du__ , 12ø55 --- ---------- ------ ------ - .--- --=-=---:-~=:-::~~'=-~~-=~-=-'--:=----et--u- ~! n¡ O¡ p'1 .-+ ¡ P'¡ ~¡ CD§ '"0 1 01 ::t¡ N¡ 001 Chi 1400 1300 1200 I ~¡ P'1 ~I N¡ ~§ N¡ 01 ~¡ N¡ .þ..1 800 700 600 500 400 300 200 100 . 0 y-rr-' r I I I I . I I I ( . I I I I I 1 I 1 I I I r I I I I I I I I I ' I I I I I I I J I I I 1 I I 1 . I I I I I I . I I I . I I I I . I I I I I , I I I I , I I I I I I ' I I . I I I I I I I I I I I I I I I , I I I t I J I I . I I . I . I I I . 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I I I I J J I' I I I J I 1'1 I I I I J I ~ I f I j ITi~Tie-.:~> 70.00 70.20 70.40 70.?º..'?"Q:ªg...71.()0. ...?J..:gg, ..?J_:.4Q_...?'J..&().._Z.!,&º..,_?g,·Q.Q'mJ2.~º_?~i9..,...zg.:~º_..?2.80.._?~:9_(L"?"'~:?'Q....?ª:,~.9__?.?..:~º._,..Z~~ªº.....?~:.Q.º....Z.4:gº.....!4.:~º,_,?4.~~º ?:i:,ªº_...._.....Æ 500 400 300 200 100 Ion 217.20 (216.90 to 217.90): S9900014.D 98R00391 SAT Peak# Ret Time Type Width 1 83.171 W 0.149 .2 84.069 W ,0.-170 . 3 84.520 PV 0.221 4 85.057 W 0.150 Area 7343 - --.g.{)4á--.- 6299 6022 Start Time 82.963 ., -- -------.fH.-9-1-1--,,- 84.390 84.922 End Time ,83.300 84.263- 84.748 85.306 - - --- ---- ~-~------------------ _____ ______0_____ __u ____ ____ ______ - - - ----- -- ---------- ------G-- ~ n d P' .-t- PJ ~ (t) '1:S o ::¡ 1'0 00 v-. ~ P' (JQ (1) 1'0 ~ \0 o ~ 1'0 .þ.. 0\ · AbundiÙ1ce"...----... ,.........-.........................-.-.......----'-.-..---. ¡ 600 550 500 450 400 J 350 300 250 200 150 100 50 \ ¡lIV l \ .-, -:-ì6n=-217.2&:(£16.90-10217-:-90): S9000011.o------- ,---------==--=-===-=-=--==-=-=:- '.. -===-...:.-==='~.:--=--:=--===-==-=o..-- st (þ d ~ ~ ïÞ .g ô ::t Ñ ob i' _______4___ - _._---~~_. r ) tit' \V tv, 83..17 ~"I'_'- .>~,"-,-I~j '>A~" D'~..~.c: M ~ 85..05 Ñ N) q> Q ""t> Ñ -#>. rr~rr~e·-:~' ....... _.....4......· O-rï . 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Peak# Ret '1.' ime '1.'ype Width Area Start Time End Time 1 83.177 BV 0.223 14750 82.731 83.323 2 83.702 VV 0.100 4847 83.604 83.790 3 83 .89 6 VV 0.112 'BT12 ' '·ST. 790- Hall. 034 4 84.519 vv 0.076 3882 84.447 84.610 5 85.105 PV 0.316 20908 84.610 85.283 -G ~ (') d P' .-+ PJ ~ CD '"0 o 1-1 .-+ 1'0 00 VI ~ P' (JQ CD 1'0 W .þ.. o ~ 1'0 .þ.. 0\ Ion 217.20 (216.90 to 217.90): S9900020.D 98R00397 SAT peak# Ret Time Type Width Area Start Time End Time 1 83.682 M 0.071 4479 83.597 83.783 2 83.879 M 0,0~7 . "B3~J5 , . ._ J13_._7.81 __8A_._O_~5 ---- --- -._-~---------~ 3 84.088 M 0.138 6147 84.022 84.218 4 85.080 M 0.084 6761 85.033 85.226 ---Q-- ~ n d P' .-I-- P' ~ (1) '"0 o ::4- 1'0 00 v-. ~ PJ (JQ (1) 1'0 VJ v-. o ~ 1'0 .þ.. 0\ 750 700 650 600 550 t 500 4501 11 400 350 300 250 200 150 100 50 -.-...--------------..---.......-.---- ___~~~_~!.~~_~!~.~~~~__~J!-=~~~_~~~~~~Q:~___ ___ \ \ !,J ), VV N ~ J -_._-~-- --- J 83.18 tv \ 83.9Q -----~---.. u'u ., ,.s-- ~ C1 d P'i .-+; P'i ~ .g¡ ~ N ~ ì ~ ~t N ~ 85.11 8:3.7( 84.52 01 H} N ..þ.¡ O"~I' I I , I r-1 I , I I I 1 , I I I I I I I 1 1 I I 1 . . I I I I I I I I I I I I I . I I I . I I I I I I J I I I . I I I J .. . I I 1 I I I I I I I I l 1_ I I I I I I 1 1 I I I I I f I I I I , I I . 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