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GMC Data Report No. 292
Hydrocarbon extraction gas chromatograph evaluation from cuttings and core chips (13,760'- 13,820') of Union Oil Company of Cali fomi a Clam Gulch Unit No. 1. ~ ~>',~,',,' ",,; , '~".'. ",' ,¡,.~.~/'"""'''I:\~'':,¡. " :if§¡¡¡:,.'~~ ~9""' ..~~ I C.~9 ~..~ " ~' ... . . ....;# ".. ,~ . Created 25 March 2000. Total of 10 pages in report. Alaska Geologic Materials Center Data Report No. 292 UnocaJ Clam Gulch 1, 13809-20 ft, Pentane Soluble Core Extract C27-C30 Sterane Distribution m/e 217 O:\EDMAN\GCMSDA T A\Aucg8s#1 14.0 - 13.0 - 12.0 - 11.0 - A 10.0 - ('It) 0 0 9.0 + - 11.I ~ '" ...... 8.0 c: cu ~ 7.0 ::J - 0 s::: .e 6.0 -- - cu ...... {!. 5.0 - 4.0 - 3.0 - 2.0 - 1.0 - o.o-~ I 750 800 I LEGEND _ Ò AucG8s0001 B f' \ ~ ~"N '/\ \.v 850 900 950 1000 'I \ 1050 c ¡ j \ Vfi NIl 1100 1150 Scan Number D , ~~ 1200 F G H E ~ f .J ~. 1250 1300 1350 1400 :.1/10/100 16:12:59 ,~ a ~ () tj p) .-+- p) ~ (D "'d o :¡ N \0 N ~ p:¡ {JQ (D o ~ - o Bioplot Windows Applic , Unocal Clam Gulch 1, 13809-20 ft, Pentane Soluble Core Extract C27-C35 Terpane Distribution m/e 191 O:\EDMAN\GCMSDA T A\Aucg8h#2 17.0 - 13 16.0 15.0 - 14.0 - 13.0 - 12.0 - CV) <::) 0 11.0 - + UJ 10 ~ 10.0 -- ......... ..... c: ~ 9.0 - L.;;: ::1 (,) 8.0 - c: 0 7.0 - - - J!! 7 {:. 6.0 - 8 5.0 - 11 14 4.0 - 15 3.0 - :: /vv 11- j OJ L C 00 ~ \.. ~ .J ,^..-/rl.J\ ' , "^ 'vlvu ~ ° wAlJ ~ 700 750 800 I 850 900 I 950 Scan Number \ LEGEND J Ò AUCG8h0002 1000 I 1050 1150 1100 ,~ 3/17/100 13:59:35 Q ~ (') \:1- p:¡ .-+- p:¡ ÏiJ (D "0 o :¡ N \0 N ~ ~ (JQ CD N o Þ-!'-) - o Bioplot Windows AppJic I Unocal Clam Gulch 1, 13809-20 ft, Pentane Soluble Core Extract C20-C35 Terpane Distribution mle 191 O:\EDMAN\GCMSDA TA\Aucg8h#2 17.0 - 16.0 - 15.0 - 14.0 - 13.0 - 12.0 - ('It) 0 0 11.0 - + l1J ~ 10.0 - '" ..... c: ~ 9.0 - ~ ~ (.) 8.0 - c: 0 7.0 - - - cu ..... {:. 6.0 - 1 5.0 - 4.0 - 2 3.0 - 2.0 - 7 8 10 13 11 14 15 1.0 ~#Ø~~W·~V4I~·~~'J,'¡'"~~C"0j\!~Jl_~ 0.0 100 I 200 300 400 \ LEGEND 6 AucG8h0002 I 500 600 Scan Number 700 I 800 900 1000 1100 ,~ 3/17/100 13:43:49 a ~ (') tj ~ p) ~ (D ~ o :4- N \0 N ~ p) {JQ (D VJ , o Þ-+¡ - o Bioplot Windows Applic I Unocal Clam Gulch 1, 13760-90 ft, Pentane Soluble Core Extract C27-C30 Sterane Distribution mle 217 O:\EDMAN\GCMSDA T A\Aucg7s#4 100.0 - 90.0 - 80.0 .- A ~ 70.0 ,- 0 0 + UJ ~ 60.0 - .......... ..... c: e F L.;;: 50.0 ::J - 0 G c: B 0 - H - 40.0 - E ~ {:. 30.0 - C 20.0 - , D ( \ 4\¿ JIt, ~ fA ~'~ ~ ~p o.o~ ~k...J'" I 1íl ) \v' 10.0 - 750 800 850 900 950 1000 1050 1150 1200 1350 1250 1300 1100 Scan Number ,N!) {LEGEND Ò AUCG7s0004 1400 J/1 0/1 00 16:21 :22 a ~ n t:J p) .-+- p) ~ (D "'d o :¡ N \0 N ~ p.) {JQ (D .þ. o Þ-t) - o Bioplot Windows Applic I Unocal Clam Gulch 1, 13760-90 ft, Pentane Soluble Core Extract C27-C35 Terpane Distribution mle 191 O:\EDMAN\GCMSDA TA\Aucg7h#2 17.0 - 16.0 - 15.0 - 14.0 .- 13.0 - 12.0 - CV) <::> 0 11.0 - + UJ ~ 10.0 - ......... ...... s::: ~ 9.0 - ~ ::1 (.) 8.0 - c: 0 7.0 - - - ctJ ..... {2 6.0 - 5.0 7 - 8 4.0 - 3.0 - 13 10 11 14 15 :: ~ ~ \ , . ftw.J~)JJ Jr-J-AY^~.AJ~ 0.0 - 700 I 800 1000 750 850 900 950 Scan Number \ LEGEND I"::. AUCG7h0002 1050 1100 I 1150 r ' M- ,MIUIAIH"~ 3/17/100 13:21:49 o ~ () t::1 p) .-+- p) ~ (D "'d o :¡ N \D N ~ p:¡ {JQ (D VI o I-+¡ ~ o Bioplot Windows Applic r ~) Bioplot Windows Applic ....UHIIII J ¡LEGEND ò AUCG7h0002 Scan Number 3/10/100 13:34:55 . I 1100 1000 I 900 I 800 700 I 600 I 500 400 300 200 100 - o 2.0 . , I 0 1 i~, ~ IfJhft \W ~ " .1 : L 1.0 ~ ,,~Il/.A"'JMJ/rMJ~4W~'\fIiI l...r-JU,¡ ~.¡ \~Lv. ~V¡..W~~ ~.~'Y·'V'·VYf 0.0 ~ p) {JQ (D 0\ o ÞO-t) 7 17.0 - 16.0 - 15.0 - 14.0 - 13.0 - 12.0 - C'") <::) <::) 11.0 - + LIJ ~ 10.0 - ......... ..... r:::: Q) 9.0 - ~ ::1 0 8.0 - r:::: 0 7.0 - ---- - ,f! 6.0 - 0 t- 5.0 - 4.0 - 2 3.0 - 14 15 II 8 10 C) ~ (1 tJ p) .-+- p) ?J (t) "'d o ~ N \0 N 13 Unocal Clam Gulch 1, 13760-90 ft, Pentane Soluble Core Extract C20-C35 Terpane Distribution mle 191 O:\EDMAN\GCMSDA T A\Aucg7h#2 Whole Oil Gas Chromatogram Arab Medium Standard N:\Analytic\GeoChem\AIA_ Data\Ckstd 1 .rax co o <:) + UJ ~ ......... CU o c: ~ s::: :::s ..Q q: CU :> "- ..... (Q - (1) a:: 11.0 - 10.0 - 9.0 - 8.0 - 7.0 - 6.0 - 5.0 - 4.0 '- 3.0 - 2.0 - 1.0 - 0.0 - LEGEND ð. Arat> Med 10 15 20 JI\I,ut~~ I I I I 25 I 2000 2500 o 500 1000 1500 Relative Retention Time (Seconds), J... J_.l )~ ~~ l I 3000 3500 ,~ 4000 3/17/100 14:32:49 a E;:: () t:1 p:¡ .-+- p) ïd (D '"0 o ::¡ N \0 N ~ p:¡ O'Q (1 -...J o I--i-) ~ o Bioplot Windows AppJic I Whole Oil Gas Chromatogram Unocal Clam Gulch 1, 13809-20 ft, Pentane Soluble Core Extract tI:\AnalyliC\GeoChem\AIA _oata\13809-20oraX 0.1 - ~ t) ~ p:I ?; ~ o ~ N \D tv 0.1- 0.1 - eo <:> 0.1 0 - + w T- -- Q) 0.1 - 0 1:: CU "'t:S t: 20 ::s 0.1 - 2S .Q « CU > -- ... 0.0 - CU Q) \ 0:. \ 0.0 ~ 0.0 - I-1j ?' Ph 'I (JQ ð> ~L ..3t~~~~~j ~ (fJ 0.0 - pr 0 H-¡ \.)'" .-- 0 Lh-- 0.0- \ \ \ \ \ 0 500 1000 1500 2000 2500 3000 3500 Relative Retention Time (Seconds) 3/11/100 14:24:59 ~ Bioplol Windows AppliC jpPJØDII LEGEND 6. \,;G 13809-20 Whole Oil Gas Chromatogram Unocal Clam Gulch 1, 13760-90 ft, Pentane Soluble Core Extract N:\AnalytiC\GeoChem\AIA_Oata\ 13760-90.rax 0.1 - 0.1 - 0.1 - 25 0.1 - ()Q <:) 0.1 <:) - + UI ~ 0.0 '" - Q) u c: ctS 0.0 - "'tJ t: ::s ~ 0.0 - c;( OJ > 0.0 - "- ..... ctS - OJ 0::: 0.0 - 0.0 - 0.0 - 0.0 - 0.0 - _~I~ 0.0 - I 0 500 20 30 Pi. ~,N.~~\I. ,AJl~"'\/II,\A-..J...,."¡'~ Pr ./ ' l.~ _ . __"' .....Þ I \ I - 1000 1500 2000 2500 3000 3500 Relative Retention Time (Seconds) \ LEGEND ] ß l;G ~ 3760-90 iN :::..':. } CJ ~ () tJ p) .-+- ~ It' ('D '1:$ o ~ N \0 N ""d p) (JQ (D \D o I-+) Þ-' o 3/171100 14:15:25 Bioplot Windows App\ic \ GMC Data Report 292 Page 10 of 10 Key to Labels on the Saturate Fraction Gas Chromatograms 1 5 n-C 15 alkane Pr Pristane Ph Phytane 20 n-C20 alkane 25 n-C25 alkane 30 n-C30 alkane Key to Labels on the Terpane Mass Chromatograms 1 C23 Tricyclic 2 C24 Tricyclic 3 C25 Tricyclic 4 C26 Tricyclic 5 CZ8 Tricyclics 6 C29 Tricyclics 7 C27 18aH, 21ßH Trisnorhopane (Ts) 8 CZ7 17aH, 21ßH Trisnorhopane (Tm) 9 C28 1 7 aH, 21 ßH Bisnorhopane 1 0 C29 17cxH, 21ßH Norhopane 1 1 C29 18cxH,-30-Norneohopane (C29Ts) 1 2 C30 18 aH Oleanane 1 3 C30 17aH, '21ßH Hopane 14 C31 17aH, 21ßH Homohopane (22S) 1 5 C31 1 7 aH, 21 ßH Homohopane (22R) 1 6 C30 Gammacerane Key to Labels on the Sterane Mass Chromatograms A C27 13ßH, 17aH Diacholestane (20S) B C27 13 ßH, 17 aH Diacholestane (20R) C C27 5aH, 14aH, 17aH Cholestane (20R) o C28 24 methyl-SaH, 14aH, 17aH Cholestane (ZOR) E C29 24 ethyl-5cxH, 14aH, 17cxH Cholestane (205) F C29 24 ethyl-SaH, 14ßH, 17ßH Cholestane (20R) G C29 24 ethyl-SaH, 14ßH, 17ßH Cholestane (20S) H C29 24 ethyl-SaH, 14aH, 17aH Cholestane C20R)
