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GMC Data Report No. 298
Geochemical analysis of Tenneco OCS Y-0943-1 (Aurora No.1) well cuttings (3,570' - 3,600', and 4,080' - 4,110'), Amoco OCS Y-0917-1 (Belcher No. 1) well cuttings (2,200', 3,160', and 3,970'), and Mobil Oil Corporation Mikkelsen Bay State 13-09-19 well core (11,608', 11,613', 11,626', and 11,655'). ~ \ \. ; ;t..~;·'~u-¡":·<~ð~.~~:.'·' ,1 .]::t::'......~ " ~.'\~::: ::i \'.'~." ", . . ¡ I.", ,.,.~io.·I"" ~ . l' ¡~~~. '.~"I'" ~~~~~.:, -£~:;:,~:.:(.,. ø....¡· "':. ~~. ~/.'ftl,( ~'~~7'- ~"Y"'Gt.. . ~ ""'.. ':.,.'. .. .;.. ..L ·1 ........ · '~".'...",....-'" .. c;;" Received 7 November 2001 Total of 33 pages in report Alaska Geologic Materials Center Data Report No. 298 GMC Data Report 298 ,. ~~'1 ~6 ~~~~}~¡~..,~~"S I Page 1 of 33 GEOCHEMICAL ANALYSIS OF Aurora-1 Prepared For: BP Peñormed By: Baseline DGSI Project: 01-458·A September 2001 BASELINE DGSI, U.S.A. BASELINE DGSI, Braslt 8701 New Trails Drive, The Woodlands. Texas 77381-4241, Tel: 281.681.2200. Fax: 281-681-0326 E-mail: info@baselinedqsi.com. Rua Benjamin Batista 55(301. Jardim Botanica, 22461·120 Rio de Janeiro (RJ) - Brasil Tel/Fax: +55-21-537-7893 E-mail: ssp@solintec.com.br Web: ht1p:IfW'N'N.baselinedqsi.com -D-G-S-I -- ---- - __..:............--:.1-...:-.;.__: _.;._::..-..;...._..;....-..:...=-: ~ - ..._.n_.__. a ~ (') d P' .-t- P' ~ (I) I-Q o =:¡ N \0 00 MPLC DATA Project #: 01-458-A f,f~~t~~~rf(~r; :ªS~l:' AURORA 3570-3600 AURORA 4080-4110 19.3 52.7 5.9 15.6 1.6 8.4 7.4 19.8 1.7 4.0 30.6 29.6 8.3 15.9 38.3 37.6 8.8 7.6 16.3 46.3 14.8 7.4 16.6 47.8 86.0 90.7 (" '\ l Composition 1 80.0 60.0 -.: 40.0 -- 20.0 -: 0.0 -- Ie -':"':-'-'-·1 1~'¥"~i'Jß?':,'c, I AURORA 3570-3600 AURORA 4080-4110 \. ¡_Sat (%) flAm (%) IINSO (%) DAsph (%) ~ ~ P' (JQ (I) N o Þ-+) UJ UJ Sat=saturate hydrocarbons; Aro=aromatic hydrocarbons; NSO=nitrogen, sulfur and oxygen compounds (resins); Asph=asphaltenes (pentane insoluble) Sample Qrig Wt=sample weight in mg of the material used for the liquid chromatography procedure Total Recovery (mg)=total combined weight of the saturate, aromatic, NSQ and asphaltene fractions Deasphaltene weight=weight of the sample minus the asphaltene weight Baseline DGSI - USA 8701 New Trails Ofive. The Woodlonds. TX 77381-4241 Telephone: 281-681-2200 Facsirnile: 281-.68 1-0326 E-mail: iofo@baselinedgsi.com Web Site: hllp:/Iwww_boselinedgsLcom 8as~lne DGSI - 8ra1.l1 Rua Benjamin Batista 55 /301 Jordim Botóruco. 22461-120 Rio de Joneiro (RJ) - Brazil Tel/Fox: +- 55.21 /5377893 E-moil: ssp@solintec.com.br Page 3 of33 . ANALYTICAL LABORATORIES CGSI SATURATE GC ANAL YSIS GMC Data Report 298 Company Sample File Name BP AURORA 3570-3600 G1 01 0812.0 Saturate Compositions: 2B:XO 24CCC' Resolved Components(%) Normal Paraffins Isoprenoids Resolved unknowns 10.4 1.9 87.7 Ratios Prlstane/Phytane nC17/Pristane nC18/Phytane nC18/nC19 nC17/nC29 CPI Marz11 0.57 1.28 0.69 1.05 0.87 1.25 ~ N ::J I N U Z U Z I I lEDX ~ u z J..Z:X:X: e:x:x: 4CXX: ... ~e",r- ~ z ~ ~ ~ ~ ~65 ~ CJ :Z:Z:~("t'"' ~ ~ ó1 ~~ ~\J JI. :(I~.\ J,:I) ~?i ~f.¡ ~~"H ' '" ~::: j~ ~ ~ =: ~~ ~ ó1 ~ E ! l \' a ~ 5 1~¡l11 <:> c..... ..... ~ .....wz Ell )WI¡¡ ~ ~ Ô~ c::¡ ~ '" .11 ~ ~ .ZH}~~ ~ 2J.0 40.0 6).0 ~~ ~ 00.0 Page 4 of 33 ----, 100.0 120.0 'Thompson. K.F.M.,1983.GCA:V.47, p.303. 2Mango, F.D.,1994.GCA: V.58, p.895. 3Halpem,H.l., 1995.AAPG Bull.: V.79, p.80l. '1-.1arzi, 1993,OrgG;20, 1301. REQNUM:01-456-A GMC Data Report 298 Page 5 of 33 Company BP Sample AURORA 3570-3600 File Name G1 01 0812.D Abþre'yiation cÞmpquljd ::1' '. T.im,~ Atêl ,HØJ9ht, I Art;!~o/i! fi~i9ht~lg· NC9 Normal Alkane C9 21,013 134 35 " . .¡ 0.00 0,00 NC10 Norma! Alkane C10 26.572 224 53 0,01 0.01 IP11 Isoprenoid C11 27.999 266 67 0.01 0.01 NC11 Normal Alkane C11 31.803 386 101 0.01 0.01 NC12 Normal Alkane C12 36.702 1417 382 0,04 0.04 IP13 Isoprenoid C13 37.445 823 165 0.02 0.02 IP14 Isoprenoid C14 40.193 873 251 0.03 0.03 NC13 Normal Alkane C13 41.289 6025 1879 0.18 0.22 IP15 Isoprenoid C15 44.728 3251 892 0.09 0.10 NC14 Normal Alkane C14 45.606 12249 3762 0.36 0.44 IP16 Isoprenoid C16 48.258 7972 1623 0.23 0.19 NC15 Normal Alkane C 15 49.675 17486 4700 0,51 0.55 NC16 Normal Alkane C 16 53.522 16846 4758 0.49 0,56 IP18 Isoprenoid C18 55.458 10006 2148 0.29 0.25 NC17 Normal Alkane C17 57.168 18584 5017 0.54 0.59 IP19 Isoprenoid C19 (Pristane) 57.530 14487 2502 0.42 0,29 NC18 Normal Alkane C18 60.638 17653 4841 0.51 0,57 IP20 Isoprenoid C20 (Phytane) 61.116 25499 2861 0.74 0.34 NC19 Normal Alkane C19 63.945 16810 4192 0.49 0.49 NC20 Normal Alkane C20 67.098 18373 4527 0.54 0.53 NC21 Normal Alkane C21 70.112 20912 6066 0.61 0.71 NC22 Normal Alkane C22 72.996 27857 7779 0.81 0.92 NC23 Normal Alkane C23 75.756 24686 7171 0.72 0.84 NC24 Normal Alkane C24 78.401 19757 4824 0.58 0.57 NC25 Normal Alkane C25 80.943 18651 4763 0.54 0.56 NC26 Normal Alkane C26 83.399 16589 4452 0.48 0.52 NC27 Normal Alkane C27 85.762 18614 4487 0.54 0.53 NC28 Normal Alkane C28 88.034 11865 2745 0.35 0.32 NC29 Normal Alkane C29 90.247 21395 4309 0.62 0.51 NC30 Normal Alkane C30 92.317 11536 2645 0.34 0.31 NC31 Normal Alkane C31 94.435 14001 2786 0.41 0,33 NC32 Normal Alkane C32 96.407 15425 2743 0.45 0.32 NC33 Normal Alkane C33 98.372 10320 1709 0.30 0.20 NC34 Normal Alkane C34 NC35 Normal Alkane C35 NC36 Normal Alkane C36 NC37 Normal Alkane C37 NC38 Normal Alkane C38 NC39 Normal Alkane C39 NC40 Normal Alkane C40 NC41 Normal Alkane C41 REQN UM:01-458-A a s;: (') t:1 PJ -- PJ ?:1 (j) '"a o ::¡ tv \0 00 Sample: AURORA 3570-3600 28000.-~- - - -- 24000_ 0'1 N U Z O-lN 0: (") 00) (Y) ('. ~ ~ ~ L 0') :z ~ lit ~ .~ ú) N r- U \D N Z N U U Z Z "'" N U Z f") N U Z N N U Z rl N U Z r~r ,W J ,~~ ~ ~ }l C> N o Z ~ ~ PJ (JQ ( ) 0\ o H) VJ VJ ! IVJ!A\ (Y) \D .-I .---I ij~tþl~'~ 120.0 l1å.o loå.o o ----"90· 80.0 70.0 Retention Time (minI 60.0 50'.0 40.0 20000_ 16000_ 12000_ 8000 4000_ 0 0'1 rl U tL Z H ----------- 0_----..-__-- 20.0 30.0 : G1010812.U\FlDl Date , Tilll~""~ lO-Sep-O O;S~;J4 0\ rl U Z <D .---I U Z c C'- D.. r- rl U Z J\ --i )., <D -; rl P.. H \D rl U Z ú) Õ Z <3' r-I U Z GMC Data Report 298 Company Sample File Name Page 7of33 BP AURORA 4080-4110 G1010813.D Saturate Compositions: 40XC 3Xœ , ¡ 'ðXf:J::. J..(XXX Resolved Components(%) Normal Paraffins 12.7 Isoprenoids 3.9 Resolved unknowns 83.4 Ratios Prlstane/Phytane 0.54 nC17/Prlstane 0.82 nC18/Phytane 0.40 nC18/nC1g 1.04 nC17/nC29 0.80 CPI Marz¡1 1.51 ..,.. ..... u :z; ..., ..... u :;:: en N V') ..... U N N :;:: ~ E ~~~ ..... '" þ "" ......;:::j:;:: :;:: ...., ~ ~ E ¡¡ Ë ~ "\I ¡¡ ~III¡¡\·W:J ~J~.~~\:&llb 6 ~ ::: ~ IIMll ßI\.~"~' · ,..;1/ I,IJ~\. ¡ ,#..! ...... ~..,.. ,I ~~~~~~)I~ ffi2 ~ . S l~ ~~~WI ~J..U'MJ.Jll.~ (Ji 2:).0 40.0 SJ.O ~'ID tœi 00.0 1m.0 120.0 'Thompson, K.F.M.,1983.GCA:V.47, p.303. 2Mango, F.D.,1994.GCA: V.58, p.S95, 3Halpem,H.I.,1995.AAPG Bull.: V.79, p.SOl. ~arzi,1993,OrgG;20,130l. REQN UM:01-456-A GMC Data Report 298 Page 8 of 33 Company BP Sample AU RORA 4080-4110 File Name G1 01 0813.0 Abbrevi~tiQn çÞinPþt;jr1~ lime ...A.rØ.~ t:I~1 ght I Ar¢a% H¢Ight% NC9 Normal Alkane C9 NC10 Normal Alkane C1 0 26.626 201 53 0.00 0.00 IP11 Isoprenoid C11 27.911 223 67 0.00 0.01 NC11 Normal Alkane C11 31.852 1932 455 0.04 0.04 NC12 Normal Alkane C12 36.744 8961 2663 0,18 0.23 IP13 Isoprenoid C13 37.488 3879 806 0.08 0.07 IP14 Isoprenoid C14 40.234 3889 1230 0.08 0.11 NC13 Normal Alkane C13 41.336 33775 10562 0.70 0.91 IP15 Isoprenoid C 15 44.772 18881 5423 0.39 0.47 NC14 Normal Alkane C14 45.656 55892 17175 1.15 1.48 IP16 Isoprenoid C15 48.303 29849 5642 0.51 0.49 NC15 Normal Alkane C15 49.721 57477 15028 1.18 1.29 NC16 Normal Alkane C15 53.663 31316 8992 0.64 0.77 IP18 Isoprenoid C18 55.498 27363 5888 0.56 0.51 NC17 Normal Alkane C17 57.211 29542 7813 0.61 0.57 IP19 Isoprenoid C19 (Pristane) 57.577 36237 7449 0.75 0.64 NC18 Normal Alkane C18 60.675 26789 5999 0.55 0.60 IP20 Isoprenoid C20 (Phytane) 61.152 67560 8683 1.39 0.75 NC19 Normal Alkane C19 63.978 25832 6406 0.53 0.55 NC20 Normal Alkane C20 67.023 17873 3685 0.37 0.32 NC21 Normal Alkane C21 70.128 19909 5803 0.41 0.50 NC22 Normal Alkane C22 73.005 17345 5013 0.36 0.43 NC23 Normal Alkane C23 75.765 23924 7137 0.49 0.61 NC24 Normal Alkane C24 78.410 17322 4735 0.36 0.41 NC25 Normal Alkane C25 80.957 32409 8443 0.67 0.73 NC26 Normal Alkane C26 83.412 28877 7468 0.59 0.64 NC27 Normal Alkane C27 85.773 31828 8255 0.66 0.71 NC28 Normal Alkane C28 88.049 16593 3945 0.34 0.34 NC29 Normal Alkane C29 90.261 36884 8596 0.76 0.74 NC30 Normal Alkane C30 92.321 18934 3627 0.39 0.31 NC31 Normal Alkane C31 94.447 20629 4498 0.42 0.39 NC32 Normal Alkane C32 96.428 10744 1960 0.22 0.17 NC33 Normal Alkane C33 98.373 15317 2751 0.32 0.24 NC34 Normal Alkane C34 100.318 10251 2221 0.21 0.19 NC35 Normal Alkane C35 102.098 8901 1494 0.18 0.13 NC36 Normal Alkane C36 104.011 2425 489 0.05 0.04 NC37 Normal Alkane C37 106.212 3293 504 0.07 0.04 NC38 Normal Alkane C38 108.629 3338 491 0.07 0.04 NC39 Normal Alkane C39 111 .453 3270 352 0.07 0.03 NC40 Normal Alkane C40 114.675 2042 249 0.04 0.02 NC41 Normal Alkane C41 118.497 2698 230 0.06 0.02 REQNUM:01-458-A a ~ (") t) PJ t'""t- PJ 10 (1) "'d o ;¡. N \0 00 'ï:t PJ (JQ (1) \0 o Þ--+') VJ VJ r<) r<) "'" N {) r<) (Y) z {) lO Ig,l 1 ~ \1 ~ 'M J~~ z '" N lO 0 r- Z (Y) N N o .0 0 N Z N Z 0 '" ..--f Z {) Z ..--f N ..--f 0 o "" (Y) z z ~ "'" C) 0 0 N =- (Y) Z Z U 0 0 z C'. z ('1 L U :z z I ~w;,~.~.~~JIJv~'~ "'" .... 0 z if) rl U Z C) N a.. (Y) .0 H .... Û ~ ~ u Z z 0 z (X) .... a.. \D H .... if) a.. rl H a.. H ~ LJIIII~i A~~~J \' !Iv ~?am:ele~__ .~~!30RA 4080-4110 40000 120.0 110:0- 106.0 .0 70. o..---.-~o· ~ (min) o ~o---~o 40.0 30000. 20000 10000 o .-< .-1 rl U D. .. LZ-H. 20.0 30' _ 0 : G1010813.IJ\FlOl D.ate '- Tímr-~ JO-Sp.l')-O GMC Data Report 298 [1[.' ~~., 4 BASELINE CGSI .:....fI.:.~~,... ....... -- ...~~;·t,~·~,.. ...:. -~ Page 10 of 33 GEOCHEMICAL ANALYSIS OF Belcher Prepared For: BP Performed By: Baseline DGSI Project: 01-456·A September 2001 BASELINE OGSI, Brasil 8701 New Trails Drive. The Woodlands, Texas 77381-4241, Tel; 281.681.2200, Fax: 281-681-0326 E-mail: info@baselinedosi.cam, Rua Benjamin Batista 55/301, Jardim Bot.ånico. 22461-120 Rio de Janeiro (RJ) - Brasil Tel/Fax: +55-21-537-7893 E-mail: ssp@sollntec.com.br Web: pttp:/('M'ffl.baselinedqsl.com BASELINE DGSI, U.S.A. GMC Data Report 298 ri.tII:.õ._ ". ~·!~·BASEL.INE CGSI ,,. ~.',. ...~_. ...'. -- ....:.... :,.. :.!... ...:., =-.; Page 11 of33 Extracted Whole Oil GC ANALYSIS i¡¡:-~..1I U~<l§ ~~~.~~_'~~~._;9-~.-~1 . a ~ (") tJ p.) .-+ p.) :;0 (1) >-cs o :4- N \0 00 ------- MPLC DATA Project #: 01-456-A BELCHER 2200 BELCHER 3160 BELCHER 3970 63.1 75.3 66.1 20.2 26.5 23.4 8.0 18.8 14.8 29.4 24.5 22.4 4.3 2.6 2.0 32.0 35.2 35.4 12.7 25.0 22.4 46.6 32.5 33.9 6.8 3.5 3.0 58.6 71.9 63.8 10.1 5.6 6.3 61.9 72.4 62.6 98.1 96.2 94.7 (' '\ I Composition I 80.0 60.0 -,~ 1'....··C"c,'".-c ·1 ... .... BELCHER 2200 BELCHER 3160 BELCHER 3970 \-. I_Sat (%) (lAro (%) (lNSO (%) DAsph (%) I ~ ""'0 PJ (fq (1) Sat=saturate hydrocarbons; Aro=aromatic hydrocarbons; NSO=nitrogen. sulfur and oxygen compounds (resins); Asph=asphaltenes (pentane insoluble) Sample Orig Wt=sample weight in mg of the material used for the liquid chromatography procedure Total Recovery (mg)=total combined weight of the saturate, aromatic, NSO and asphaltene fractions Deasphaltene weight=weight of the sample minus the asphaltene weight ~ N o H) l;.) w Baseline OGSI - USA 8701 New Troils Ofive, The Woodlands, 1)( 77381-4241 Telephone: 281-68J-2200 " Focsimile: 281-681-0326 E-moil: info@boselinedgsi.com Web Site: htlp:/JW'W'N.boselinedgsi.com tkJseJlne DGSI - 8raIlI Ruo Benjomïn ß.otísto 551301 Jardim Botöníco, 22461-120 Rio de Janeiro (RJj - &-olll Tel/Fox: + 55,21 /5377893 E-mail: ssp@solintec.com.br Sampl r~-~ e BELCH£: 9000,' -W· ...- 'R 2200 ¡ ¡ ¡ i 80001 I I j ! i 70001 I I J 6000 5000 ¡ ¡ 4000\ I 3000j I ( I i I I ) ! 200oL__J J ~ '-L- 1000, ~ile: GlOl0802,D\ ate, Time: 06~S:¡OI1\.. CH P-Ol. 11:01:Q9 _u ~ - ------- ~¡ : r . f~~~¡~ 1 "J(, M:~.I' ) ~~J'I L\~ \('~ ,~. ~ I f1' ~ ~. ~r io 4'0 6'0 80~ --- lÒO 120 ~ () tj Pi ~ po) ~ I"r:J o ::4- N \0 00 I I 'ï::1 p:¡ (JQ o ,........ W o I'-+) w w ~ample . ¡! -----T- BELCHER _~~ 3 0 I 70001 I 6000, 5000 . : II ~~..~þ 4000 3000 2000,__M. '-'-- ~ 10001 2'0 4'0 6;0 8'0 flL..: G1010R03 Oat.. . Tim..: O~~\FIDLA.<:II S..p-01. 19:24:32 100' 120 ~ (J t::J py rot- py ït1 .g o ::¡ tv \0 00 I ¡ I ¡ ! i i i j i i Þ-t; ~ (JQ (t) Þ--' .J:::.. o I--t) w w Sample BELCHER 2440 :- -----------r-~ 8000; , i 7000; I 6000, 5000, 4000 3000 2000---J.À ~\. . I I I i lOOOL_ ----- 20- File: GlOl0804.0\FIIHI\.CII Dat.e .. Time, 06-Sep-Ol, 21:48:00 ~- "." - ---- --- ,w JflY _.~/ 4'0 6'0 --------------. I~ ~ [ ~,j ~~ , vM\ ...., -----" - -- -- --. ------ 8'0 ~/ ~ ---------- I -~-------- 1ÓO 120 a 2;:: (1 t;;1 ~ rt-- ~ ~ (þ '1:j o ::¡ tv \0 00 ~ ~ (Jq (þ ~ VI o I-t) w w :~a~~le BELCHER , 1'~--- 3160 7000, 6000 5000 4000 3000 2000<__--.M. ~~L i i ! 10001 L- :~::: GlOI0805. O\FIDIA. CH - ;;. TUTI" , 01-Sep-Ol. 00:11:48 io 4'0 , - ' ' ~ ~~M,~I' ~!; tij 6'0 8'0 " ' ~ \ ~ , :~/ -J~ . --y-- 100 ---------.-J 120 ~ n tJ PJ ~ PJ ~ "d o ~ N \0 oc ¡ ¡ I ¡ I I I j I I I¡;j PJ {JQ (D 0\ o ~ w w Sample BELCHER 3610 1------ I 70001 6000 5000 4000 3000, 2000___µ'" ~-~ 1000. file: G1010806,D\FID1A.CH Oa~e , Time: O)-Scp-Ol. 02:35:19 ~- ---- ~- ",,-- ---~. .- -, . -,--- , , f.! '~,I I ,: It-¡.Þ ,,',~, . ,/'~l",~1 ",f.r ''''~ 'J f. "JIII~. I"~ f ,J",+\, ~ b '~I . d~ .'1 , 'l 1·1 ¡ ~ ." ~- ~~ , I 4'0 20 6'0 ~~- 8'0 . '--~---- ---r-- -- - 100 L~O a ~ (1 t1 p:¡ ...,.. ~ ~ "d o ~ N \0 00 ~ ~ (JQ (D ¡......l --..) o I-+) V.J V.J Sample BELCHER 3970 .--------------. -,- 8000 7000 6000 5000 4000, 3000 2000,___ß.. _____~ 1000 2'0 fil..: GIOI0601.0\f'IOlh.CII O.'Le , Tim..: 01-S..p-Ol. 01:56:30 ----- ----~------- ----. I \, /fl~ . t~)~MW~ ~I dl ~ .Irr I µ..)I 4'0 60 8'0 -.~-~-------. a s;: () t:I ~ ~ ït1 (þ '"d o ::¡ N \0 00 ~ ~ (]Q ¡ ([) ~ i 00 i 0 I I--+) V-) .I V-) i f lÒO 120 GMC Data Report 298 r·. 111 ~.~~ BASELINE CGSI ~.~.~.'II.", .11:....'. -- ,.~" :... :..:.111.... :..... Page 190f33 GEOCHEMICAL ANALYSIS OF Mikkelsen Bay Prepared For: BP Performed By: Baseline DGSI Project: 01-457-A September 2001 BASELINE DGSI, U.S.A. 8701 New Trails Drive, The Woodlands, Texas 77381-4241, Tel: 281.681.2200, Fax: 281-681-0326 E-mail: info@baselinedQsi.com. Rua Benjamin Batista 55(301. Jardim Botânica, 22461-120 Rio de Janeiro (RJ) - Brasil Tel/Fax: +55-21-537-7893 E-mail: ssp(ã)solìntec.com,br Web: httD://WoNW,baselinedcsicom BASELINE DGSI. Brasil -CG5J _....:.....,....~. .,-..._...;.-.. _..:._~.-..¡:,_..:...--..;:.., -~ Project #: 01-457-A -- ---- - MPLC DATA a ~ () tJ p:¡ .-t- p:¡ ~ (D '1:j o :4- N \0 00 MIKKELSEN 11608 MIKKELSEN 11613 MIKKELSEN 11626 MIKKELSEN 11655 74.1 59.9 96.4 35.4 16.5 14.2 27.4 8.3 16.0 7.2 18.0 4.4 25.0 21.6 29.7 11.4 12.3 13.5 9.4 6.1 ( l Composition I 80.0 60.0 40.0· . 2~:~~W~1 MIKKELSEN 11608 -- MIKKELSEN 11613 22.3 23.7 28.4 23.5 21.6 12.0 18.7 12.4 33.7 36.1 30.8 32.2 ---.~ ___ ·=:"·C'·::; MIKKELSEN 11626 "- I_Sat (%) IIAro {%)[INSO (%) DAsph (%) I 16.6 22.5 9.8 17.2 61.3 50.3 75.9 30.0 4.1 7.9 6.1 7.6 69.8 56.5 84.5 30.2 Sat=saturate hydrocarbons; Aro=aromatic hydrocarbons; NSO=nitrogén, sulfur and oxygen compounds (resins); Asph=asphaltenes (pentane insoluble) Sample Orig Wt=sample weight in mg of the material used for the liquid chromatography procedure Total Recovery (mg)=total combined weight of the saturate, aromatic, NSO and asphaltene fractions Deasphaltene weight=weight of the sample minus the asphaltene weight Baseline DGSI - USA 8701 New Trails Drive. The Woodlonds. 1)( 77381-4241 Telephone: 281-681-2200 Facsimile: 281-681-0326 E-moil: info@baselinedgsi.com Web Site: http://'N\NW.boselinedgsi.com BoseUne DGSI - 8ro211 Ruo Benjamin Balista 55/301 Jorálm Botðrnco_ 22461-120 Rio de Janeiro (RJ) - Brazil Tel/Fax: +- 55.21 15377893 E-moìl: ssp@solintec.com.br - MIKKELSEN 11655 94.2 94.3 87.7 85.3 '\ ~ ~ p:¡ (JQ (D N o o Þ--t) w w GMC Data Report 298 ,t:. e~~ ~~!~·BASEL-INE DGSI .,. ~.&.. -"'-. ...'. _ ..... :_.,:,,~.. ... t'..~ SATURATE GC ANAL YSIS Page 21 of33 , ., GMC Data Report 298 Page 22 of 33 Company Sample File Name BP MIKKELSEN 11608 G6010594.0 Saturate Compositions: Resolved Components(%} Normal Paraffins 50.0 Isoprenoids 8.6 Resolved unknowns 41.4 Ratios Prlstane/Phytane 0.61 nC17/Pristane 2.57 nC 18/Phytane 1.54 nC18/nC19 1.08 nC17/nC29 6.10 CPI Marzl1 0,98 ~ = '-' ~ "" '-' .r, "" '-' ï;i "" ~ ¡;¡ ~ :::1 ~ :::J ~ - ~ !i ~ ~ .~ = = 1= ~ ð..... ""-¡;;¡co ~6"" . U,wJ¡JJ~JLJll i ~~<iA,^"~...JJ.~"-,,,"~ ~ - <>< - ... .~ 1.0.0 =.0 3:>~'J::II-."""" 40.0 !:!O .0 EO.O ¡Thompson, K.F.M., 1983.GCA:V.47, p.303. 2Mango, F.D,,1994.GCA: V.58, p.895. 3Halpem.H.I.,1995,AAPG Bull.: V.79, p,801. 4Marzi,1993,OrgG;20, 1301. REQNUM:01-457 ·A GMC Data Report 298 Page 23 of 33 Company BP Sample MIKKELSEN 11608 FiI e Name G6010594.0 Abbre,viation CçmþouncJ TJrnØ .A;r~a Heigh~ Area % I Height % NC9 Normal Alkane C9 NC10 Normal Alkane C 10 IP11 Isoprenoid C11 NC11 Normal Alkane C11 7.424 534 247 0.02 0.03 NC12 Normal Alkane C 12 9.902 9045 3801 0.35 0.49 ¡P13 Isoprenoid C13 10.269 2523 922 0.10 0.12 IP14 Isoprenoid C14 11.821 5871 2325 0.22 0.30 NC13 Normal Alkane C13 12.544 40387 15564 1.54 1.99 ¡P15 Isoprenoid C15 14.580 22716 8469 0.87 1.08 NC14 Normal Alkane C14 15.202 85505 29846 3.27 3.81 IP16 Isoprenoid C 16 16.808 35513 9726 1.36 1.24 NC15 Normal Alkane C15 17.780 104983 3~443 4.01 4.27 NC16 Normal Alkane C16 20.255 117245 36415 4.48 4.65 IP18 Isoprenoid C18 21.407 35062 8542 1.34 1.09 NC17 Normal Alkane C17 22.616 119940 37100 4.58 4.74 IP19 Isoprenoid C19 (Prlstane) 22.748 46678 13280 1.78 1.70 NC18 Normal Alkane C 18 24.866 117462 35075 4.49 4.48 IP20 Isoprenoid C20 (Phytane) 25.082 76405 19749 2.92 2.52 NC19 Normal Alkane C19 26.970 108326 34191 4.14 4.36 NC20 Normal Alkane C20 28.907 102303 32626 3.91 4.16 NC21 Normal Alkane C21 30.700 85304 29008 3.26 3.70 NC22 Normal Alkane C22 32.377 74445 25118 2.84 3.21 NC23 Normal Alkane C23 33.956 62408 21938 2.38 2.80 NC24 Normal Alkane C24 35.452 55220 19001 2.11 2.43 NC25 Normal Alkane C25 36.876 45563 15656 1.74 2.00 NC26 Normal Alkane C26 38.241 40749 13695 1.5.6 1.75 NC27 Normal Alkane C27 39.549 29733 10253 1.14 1.31 NC28 Normal Alkane C28 40.805 22798 7735 0.87 0.99 NC29 Normal Alkane C29 42.016 19649 6420 0.75 0.82 NCJO Normal Alkane C30 43.188 15239 5063 0.58 0.65 NC31 Normal Alkane C31 44.320 12703 4081 0.49 0.52 NCJ2 Normal Alkane C32 45.418 9544 3173 0.36 0.41 NC33 Normal, Alkane C33 46.497 7188 2202 0.27 0.28 NC34 Normal Alkane C34 47.637 7861 1775 0.30 0.23 NCS5 Normal Alkane C35 48.891 5089 1076 0.19 0.14 NCJ6 Normal Alkane C36 50.286 3172 657 0.12 0.08 NC37 Normal Alkane C37 51.855 3220 413 0.12 0.05 NCS8 Normal Alkane C38 53.676 1715 261 0.07 0.03 NC39 Normal Alkane C39 55.778 1239 147 0.05 0.02 NC40 Normal Alkane C40 58.230 990 112 0.04 0.01 REQNUM:01-457-A a ~ () tJ $:I) ....... $:I) ïO (1) "0 o ::¡ tv \.0 00 Þ¡:1 ~ (JQ (1) tv .þ.. o ~ w w _§ample: MIKKELSEN 11608 50000 e- .-t I.D U .-t Z U ro Z .-t m U Z .-t U If) Z C> .-t U N Z U Z '<I' .-t .-t U N Z U Z N N U Z ...... N U Z ::J "I :l. "" --< N U Z to ...... N .-t U U Z Z ~ I.D .-t N " U -I Z ("'- to N .-t U n. ill Z If) H .-t .-t n. ill a, H N t-I U m Z N U Z C> M U .-t Z ...... N U N Z M r-I U ...... U Z ...... "" Z '<I' U ...... LL~l.JJ..J ~ t J J I".l J l J ~,1vA, Ju'~~~JIJl..M.~AJJvJ.'.~",,^~ z u If) z ...... u ~ ro Z m 0 U ...... ...... J z u u "" z u ----^----- z z 10'.0 20.0 30~-Õ---- 40.0 50.0 ~<J:() (minI 40000_ 30000_ 20000 10000 : G~O 1 O~94 Dat.c , Time:. 17.-5~p-O GMC Data Report 298 Company Sample File Name BP MIKKELSEN 11613 G6010595.0 Saturate Compositions: Page 25 of 33 Resolved Components(%) Normal Paraffins 51.3 Isoprenoids 8.6 Resolved unknowns 40.1 I ~ S j ~ ~ ~ ~~ ~>J~JL'-~~Á~~~J¡.~lw~~~::~ Ratios Pristane/Phytane nC17/Pristane nC18/Phytane nC18/nC19 nC 17 /nC29 CPI Marzi1 ~ = ,~ = ~ = u 1= ::. ~o.o 0.66 2.41 1.44 1.14 5.29 0.97 ----..-'-1 i §i u !;1 ~ ~ ~ ~ ~ ~ § u ::. '.. ~ =~ 'Dnoo tc!n 40.0 6:).0 =.0 IThompson, K.F.M., 1983.GCA:V.47, p.303. "Mango, F.D" 1994.GCA: V.58. p.895. JHalpern,H.I.,1995,AAPG Bull.: V.79, p.801. ~arzi, 1993,OrgG;20, 1301. REQNUM:01-457-A GMC Data Report 298 Page 26 of 33 Company BP Sample MIKKELSEN 11613 File Name G6010595.D Abbreviation Oompounçt Time "Area Heig ht Area % l Height % NC9 Normal Alkane C9 NC10 Normal Alkane C10 IP11 Isoprenoid C11 NC11 Normal Alkane C11 7.410 256 109 0.01 0.01 NC12 Normal Alkane C12 9.881 6237 2630 0.25 0.36 IP13 Isoprenoid C13 10.249 1706 627 0.07 0.09 IP14 Isoprenoid C14 11.797 4156 1686 0.17 0.23 NC13 Normal Alkane C1~ 12.516 29999 11803 1.23 1.61 IP15 Isoprenoid C15 14.552 16835 6340 0.69 0.86 NC14 Normal Alkane C14 15.169 67128 24101 2.74 3.28 IPi6 Isoprenoid C16 16.778 29067 8260 1.19 1.12 NC15 Normal Alkane C15 17.749 98889 32381 4.04 4.40 NC16 Normal Alkane 016 20.226 120424 37336 4.92 5.08 IP18 Isoprenoid C18 21.377 35822 8744 1.46 1.19 NC17 Normal Alkane 017 22.585 119055 37250 4.86 ' 5.07 IP19 Isoprenoid C19 (Pristane) 22.721 49345 13629 2.02 1.85 N018 Normal Alkane 018 24.833 107089 32673 4.37 4.44 IP20 Isoprenoid C20 (Phytane) 25.053 74556 19461 3.05 2.65 NC19 Normal Alkane C19 26.938 93558 30788 3.82 4.19 NC20 Normal Alkane 020 28.876 89782 2854 7 3.67 3.88 NC21 Normal Alkane C21 30.673 77744 . 26135 3.18 3.56 NC22 Normal Alkane 022 32.353 70706 25166 2.89 3.42 NC23 Normal Alkane C23 33.932 61121 21383 2.50 2.91 NC24 Normal Alkane C24 35.433 56137 19879 2.29 2.70 NC25 Normal Alkane C25 36.858 47053 16201 1.92 2.20 NC26 Normal Alkane C26 38.222 43316 14360 1.77 1.95 NC27 Normal Alkane C27 39.529 32348 11073 1.32 1.51 NC28 Normal Alkane C28 40.785 25159 8675 1.03 1.18 NC29 Normal Alkane C29 41.999 22495 7210 0.92 0.98 NC30 Normal Alkane C30 43.170 17861 6164 0,73 0.84 NC31 Normal Alkane C31 44.304 15182 4898 0.62 0.67 NC32 Normal Alkane, C32 45.402 12170 3972 0.50 0.54 NC33 Normal Alkane C33 46.479 9313 2889 0.38 0.39 NC34 Normal Alkane C34 47.623 9877 2413 0.40 0.33 NC35 Normal Alkane C35 48.873 7328 1532 0.30 0.21 NC36 Normal Alkane C36 50.262 4585 975 0.19 0.13 NC37 Normal Alkane C37 51.834 4023 599 0.16 0,08 NC38 Normal Alkane C38 53.651' 2820 436 0.12 0.06 NC39 Normal Alkane C39 55.744 1796 235 0.07 0.03 NC40 Normal Alkane C40 58.187 1727 200 0.07 0.03 REQNUM:01-457·A a s: () tJ p) .-+- p) ?;J CD "0 o ::4- N \0 00 ~ p) (JQ CD N -..J o H) w w o C> ..,. u z (J\ t"') u z Sample: MIKKELSEN 11613 50000. 40000 <D r-- .-t .-t U U Z Z co .-t ú) U .-t Z U 0'1 Z r-I U Z C> N U 30000 z r-I N U N Z N U '<I" Z r-I U Z (Y) N U => Z '<I' :'I N :l.o U -< z 20000 ú1 N U Z ð\ <D N rf U "" Z rl t"') r-- .-t U N Z U Z ro ro r-I <D a.. N .-t H U 10000 a.. Z 0\ H N ú1 U C> Z (Y) .-t U a.. Z r-I H t"') U N Z C') U (Y) Z (Y) '<I" N U (Y) Z U ú1 rl Z C') Jl~)~ ,1J'JI¡,. 1 J ~ J\:~;JAAtÁ~~.M.JÀJA,AJ)"JJ\~N. u z ~t J .-t U Z ~. 10.0 20.0 30·:Õ.------- --- 40.0 50.0 Imin : (;6010~9~.D\FlDl Dat.c , Time~ 12-Sep-O GMC Data Report 298 Co mpany Sample File Name Saturate Compositions: 2«:0:::: = :1.= = = l u l'~ :z: Page 28 of 33 BP MIKKELSEN 11626 G6010590.0 Resolved Components(%) Normal Paraffins 43.0 Isoprenoids 9.5 Resolved unknowns 47.6 Ratios Pristane/Phytane 0.51 nC17/Pristane 1.46 nC18/Phytane 0.76 nC18/nC19 1.03 nC17/nC29 2.78 ,CPI Marz 1 0.99 j;1 ~ u ~ "" ~ ~ u "" ~ u "" - ---'] I I I I I ~ ~ e ,., - g ~ ~~c:;:. ¡,¡¡~:::::~ ~~~- J' Q~~~ ~ É JII J I, ,II ~I /JA.;,¥!JA1JM.w,\¡JÁ.,Jl.r/vJloM)O'M"""JliuL___ U~J IN~ J~ 'L,.fll u _ = ""' - :1.0.0 =.0 3::>~ 'IInoo ...... 40.0 =.0 W.O IThompson, K.F.M., 1983,GCA:V.47, p.303. 2Mango, F.D.,1994.GCA: V,58, p.895. 3Halpem,H.I.,199S.AAPG Bull.: V.79, p.SOI. 'Marzi,1993,OrgG;20, 1301. REQNUM:01-457-A GMC Data Report 298 Page 29 of 33 Company BP Sample MIKKELSEN 11626 File Name G6010590.0 ÄQQr~,'~:Iªt¡ol'1 L çÞmþQ.µI1ç nrtl~ At~a H~lght Areª% I Heighl% NC9 Normal Alkane C9 . .\ NC10 Normal Alkane C10 IP11 Isoprenoid C11 NC11 Normal Alkane C11 7.420 557 242 0.03 0.05 NC12 Normal Alkane C12 9.892 3834 1594 0.21 0.31 IP13 Isoprenoid C13 10.260 1407 506 0.08 0.10 IP14 Isoprenoid C14 11.808 3136 1250 0.17 0.24 NC13 Normal Alkane C13 12.523 16125 6289 0.89 1.21 IP15 Isoprenoid C15 14.562 13640 5070 0.75 0.98 NC14 Normal Alkane C 14 15.169 39334 14263 2.18 2.75 IP16 Isoprenoid C16 16.783 21590 6225 1.19 1.20 NC15 Normal Alkane C15 17.742 48135 16525 2.66 3.19 NC16 Normal Alkane C 16 20.213 51959 17507 2.88 3.38 IP18 Isoprenoid C18 21,381 24340 6156 1.35 1.19 NC17 Normal Alkane C17 22.575 52913 17631 2.93 3.40 IP19 Isoprenoid C19 (Prlstane) 22.720 36281 10098 2.01 1.95 NC18 Normal Alkane C 18 24.826 53771 17709 2.98 3.41 IP20 Isoprenoid C20 (Phytane) 25.060 70870 18245 3.92 3.52 NC19 Normal Alkane C19 26.933 52266 17856 2.89 3.44 NC20 Normal Alkane C20 28.873 54876 17850 3.04 3.44 NC21 Normal Alkane C21 30.672 48903 17103 2.71 3.30 NC22 Normal Alkane C22 32.355 46866 16793 2.59 3.24 NC23 Normal Alkane C23 33.936 39121 13356 2.17 2.58 NC24 Normal Alkane C24 35.436 36070 12905 2.00 2.49 NC25 Normal Alkane C25 36.863 32271 10686 1.79 2.06 NC26 Normal Alkane C26 38.229 29425 9993 1.63 1.93 NC27 Normal Alkane C27 39.539 22790 7880 1.:26 1.52 NC28 Normal Alkane C28 40.798 19524 6593 1.08 1.27 NC29 Normal Alkane C29 42.011 19041 5594 1.05 1.08 NC30 Normal Alkane C30 43.184 15285 5161 0.85 1.00 NC31 Normal Alkane C31 44.319 14390 4495 0.80 0.87 NC32 Normal Alkane C32 45.418 '12275 4124 0.68 0.80 NC33 Normal Alkane C33 46.495 10993 3432 0.61 0.66 NC34 Normal Alkane C34 47.638 15819 3497 0.88 0.67 NC35 Normal Alkane C35 '¡~48.897 12841 2416 0.71 0.47 NC36 Normal Alkane C36 50.285 7735 1585 0.43 0.31 NC37 Normal Alkane C37 51.863 6908 1048 0.38 0.20 NC38 Normal Alkane C38 53.682 5170 785 0.29 0.15 NC39 Normal Alkane C39 55.781 3418 467 0.19 0.09 NC40 Normal Alkane C40 58.233 3656 421 0.20 0.08 REQNUM:01-457·A CJ ~ () t1 ~ ~ ~ ~ (1) 'U o =:¡ tv \0 00 Þ-O ~ (Jq (1) VJ o o ~ VJ VJ _~§rnpl!!! : MIKKELSEN ll626 24000 20000 C> N 0'\ ~ C> \D r- rl N rl 0 0 rl 0 0 z z u z Z rl Z N N ú) 0 N ...... Z U U Z z 16000 <3' r-I U Z f') N 0 '<r Z N U z 12000, ú) "" N 0 ..-f Z \0 Il. N H 0 Z r- N U Z 8000_ ro f') \D ro N rl rl rl 0 U (l, (l, z (J) Z >-I H N c> ú) o f') rl Z 0 (l, Z rl H Y) N o f') Z U Z Y} '<r f') f') u 0 4000 z z ú) f') U N Z ...... <3' \0 0 ...... f') z (l, U r-I UJJ."J~ J"J ~I¡..l\'~~ ",I~-Å,J'~A~~A',JvtJA~AAM~M]>'~N: ~ û J z -....J I ~ lA..... 10'.0 20.0 30.0 {minI 40_0 50.0 60.0 ll-Sr.p-O Tíme\ Date GMC Data Report 298 Page 31 of 33 Company Sa mple File Name BP MIKKELSEN 11655 G6010596.0 Saturate Compositions: Resolved Components(%) Normal Paraffins 43.5 Isoprenoids 10.5 Resolved unknowns 46.0 , , Ratios Pristane/Phytane 0.65 nC17/Pristane 1.49 nC 18/Phytane 1.02 nC18/nC19 1.08 nC17/nC29 5.36 CPI Marzl1 1.01 ---~---.,._--... '. = g ~ "" ~ g ~ ~ ~ ~ ~ ~ ~ ;:::¡ ~ = u "'" ~ 1= .... ~ ~~ §È~_ = . tl~,Jl\,JL~jJ1WJYÁ~~~","w\¡~JlllJ~ ~ z ~ ~. w z :¡,p.o =.0 ~...... ~ 40.0 00.0 (3:).0 IThompson, K.F.M.,19S3.GCA:V.47, p.303. 2Mango, F.D., 1994.GCA: V.5S, p.S95. ~Halpem.H.I.,1995.AAPG Bull.: V.79, p.80!. ~arzi,1993,OrgG;20,130!. REQNUM:01·457-A GMC Data Report 298 Page 32 of 33 Company BP Sam pie MIKKELSEN 11655 File Name G6010596.D Abbreviation , QQrTlþound Time. Area Height I Area % I Height % NC9 Normal Alkane C9 NC10 Normal Alkane C10 IP11 Isoprenoid C11 NC11 Normal Alkane C11 7.406 367 163 0.02 0.03 NC12 Normal Alkane C12 9.877 4401 1853 0.21 0,31 IP13 Isoprenoid C13 10.244 1790 652 0.09 0.11 IP14 Isoprenoid C14 11.793 3899 1560 0.19 0.26 NC13 Normal Alkane C13 12.508 17123 6716 0.82 1.11 IP15 Isoprenoid C15 14.545 14141 5415 0.67 0.89 NC14 Normal Alkane C14 15.152 36172 13281 1.72 2.19 IP16 Isoprenoid C16 16.768 23662 6728 1.13 1.11 NC15 Normal Alkane C15 17.729 55119 191~6 2.63 3.16 NC16 Normal Alkane C16 20.206 72962 23998 3.48 3.96 IP18 Isoprenoid C18 21.370 31467 7962 1.50 1.31 NC17 Normal Alkane C17 22.570 85398 27647 4.07 4.56 IP19 Isoprenoid C19 (Pristane) 22.713 57302 15840 2.73 2.61 NC18 Normal Alkane C18 24.824 89361 28297 4.26 4.66 IP20 Isoprenoid C20 (Phytane) 25.052 87690 22263 4.18 3.67 NC19 Normal Alkane C19 26.932 82915 27834 3.95 4.59 NC20 Normal Alkane C20 28.869 77426 25125 3.69 4.14 NC21 Normal Alkane C21 30.665 62017 21909 2.96 3.61 NC22 Normal Alkane C22 32.345 54905 19483 2.62 3.21 NC23 Normal Alkane C23 33.924 44883 16213 2.14 2.67 NC24 ' Normal Alkane C24 35.424 42099 15062 2.01 2.48 NC25 Normal Alkane C25 36.850 37181 12619 1.77 2.08 NC26 Normal Alkane C26 38.215 31 064 10467 1.48 1.73 NC2? Normal Alkane C27 39.523 22680 7872 1.08 1.30 NC28 Normal Alkane C28 40.779 15846 5230 0.76 0.86 NC29 Normal Alkane C29 41.992 15932 4145 0.76 0.68 NC30 Normal Alkane C30 43.164 9313 2975 0.44 0.49 NC31 Normal Alkane C31 44.302 8736 2454 0.42 0.40 NC32 Nonnal Alkane C32 45.469 7273 1933 0.35 0.32 NC33 Normal Alkane C33 46.473 4609 1275 0.22 0.21 NC34 Normal Alkane C34 47.618 12181 2036 0.58 0.34 NC35 Normal Alkane C35 48.940 11714 1600 0.56 0.26 NC36 Normal Alkane C36 50.256 1888 400 0.09 0.07 NC37 Normal Alkane C37 51.799 3429 395 0.16 0.07 NC38 Normal Alkane C38 53.644 2100 281 0.10 0.05 NC39 Nonnal Alkane C39 55.738 1397 170 0.07 0.03 NC40 Normal Alkane C40 58.180 1330 150 0.06 0.02 REQNUM:01-457·A o ~ (J t;1 ~ ~ ~ 10 (t) '1:j o ::4- ·N \0 00 Þ¡: ~ (JQ (þ W W o I--f) w w 60.0 C> Õ z (J'\ (") u z _~_ampl e : MIKKELSEN 11655 m .-t (J'\ 30000 r- U .-t .-t Z U U Z Z CI N U Z \0 .-t U Z => :"I .-t ::to N ..... U Z N N \l) U .-t Z u 20000. z CI\ (") N ..-i U '" Z "'" H N U Z "'" .-t \l) U N Z U Z W N U z 10000. m r- .-t 0.. N H U W Z (") rl rl U 0.. Z H en If) .-t N 0.. U H Z (J'\ N U Z CI (") rl U (Y) Z U rl 1 ~ >;J~.JtJ J,"^ l J ~ llJ,"t,J ~J!A~A~J/Jw~JÞ.~'^M: .-t u Z - "-- 10'.0 20.0 30.0 ---- ---- 40".0 t€ {min : G('OlO~9(,.D\FlDl Dat.e " Time"': 12-Sep-O ¡. 50.0
