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Home My WebLink AboutGMC Data Report No. 270 Saturated Gas Chromatography, Saturated Gas· Chromatography /Mass Spectrometry 191, 217,218, and 259 fragmentograms, and Aromatic Gas Chromatography/Total Ion Current and 231 fragmentograms of extracts from the following NPRA well materials: Husky NPR Operations (D.S.G.S.) Drew Point No.1 core (6,977' - 6,981.6'), Husky NPR Operations (U.S.G.S.) East Simpson T.W. No.2 cuttings (7,150' - 7,180'), Husky NPR Operations (U.S.G.S.)Inigok T.W. No.1 core (10,304'), Husky NPR Operations (U.S.G.S.) J. W. Dalton T. W. No.1 cuttings (7,960' - 7,990'), Husky NPR Operations (U.S.G.S.) Kugrua T. W. No.1 cuttings (8,710' - 8,730'), Husky NPR Operations (U.S.G.S.) Kuyanak T. W. No. ·1 core (composite from 5,096', 5,100', 5,108', 5110', 5,145'), Husky NPR Operations (D.S.G.S.) North Inigok T. W. No.1 cuttings (8,330' - 8,340'), Husky NPR Operations (U .S.G.S.) West Dease No.1 core (3,717') and cuttings (3,360' - 3,380'), ~~ GE~O.(Q '~ ~ :j/ ~ 0 ~~~~. . ~¡4LS ..?tf.. ,.~. .,", ,.." .- "" . U. S. Navy East Ournalik No.1 core and cuttings (composite from 1,620' - 1,710', and 2,230' - 2,250'), U. S. Navy (Husky Oil) East Teshekpuk No.1 cuttings (7,100' - 7,130', and 7,230' - 7,250') , U. S. Navy Kaolak No.1 core (composite from 4,804' - 4,805' and 4,824' - 4,825'), U. S. Navy Knifeblade No.1 cuttings (1,425' - 1,475'), U. S. Navy Simpson T.W. No.1 core (composite from 388', 6,182', 6,185', and 6,239'), . U. S. Navy South Harrison Bay No.1 cuttings (7,170' - 7,210'), U. S. Navy Titaluk No. 1 core (3,421' - 3,429'), U. S. Navy (Husky Oil) W. T. Foran No.1 cuttings (7,510' - 7,540', and 7,730' - 7,750') and core (8,256'). Received 2 July 1996 Total of 222 pages in report Alaska Geologic Materials Center Data Report No. 270 -----------.--- NPRA Extract DataV4.1.GMC Sample Well Depth I Sample ( 95r2116 W T Foran 7510-40 Ictgs 95r2117 W T Foran 7730-50 ctgs 95r2118 W T Foran 8256 oil in fracs 95r2120 Drew Pt 6977-81.6 core 95r2122 Simpson 1 388 core 9520005} Simpson 1 6182 core 9520005 eo~f';"f(~jsimpson 1 6185 core 9520005 Simpson 1 6239 core 95r2128 E Simpson 2 7150-80 ctgs 9520004"" Kuyanak 5096 core 95Z0004 Kuyanak 5100 core 9520004 ~e()"'fo?;tJ Kuyanak 5108 core 95Z0004 Kuyanak 5110 core 95Z0004.J Kuyanak 5145 core 95r2145 E T eshekpuk 7100-30 ctgs 95r2148 E Teshekpuk 7230-50 ctgs 95r2176 Inigok 1 10304 core 95r2189 Kugrua 8710-30 ctgs 95r2192 N Inigok 8330-40 ctgs 95r2208 S Harrison Bay 7170-7210 ctgs 95r2209 Titaluk 1 3421-3429 core 95Z0007} .¡ E Oumalik 1 1620-1710 core/ctgs . , ( 9520007 comp(JcjdG E Oumalik 1 2230-2250 core/ctgs 95Z0006} J Kaoiak 4804-5 core/~ 95 Z 0 00 6 C/JMfo~/~ Kaolak' 4824-25 core 95r2220 Wolf Ck 3 2662 core . , ~ , 95r2223 W Dease 3717 core II .... 95 r2227 W Dease 3360-80 ctgs . . 95r2228 J W Dalton 7960-90 ctgs 95r2230 Knifeblade 1- \ 1425-1475 ctgs ¡' \....,. GMC Data Report No. 270 Page 1 1/222 This data report contains the following: Saturate GC Saturate GC/MS 191, 217, 218, 259 fragmentograms Aromatic GC/MS TIC and 231 fragmentograms GC = Gas Chromatography MS = Mass Spectrometry TIC = Total Ion Current GMC Data Report No. 270 2/222 " Co) 2- o Ã I ... I I GMC Data Report No. 270 3/222 0002 0004 0006 0.006 0010 0.012 0014 0016 0.016 ,0020 0022 -Û.024 0026 0.026 ,0.030 0032 0.034 ·0036 0038 O~O 0~2 -- -----0.044 oJ - - .~~~~ 1u~ 0iLWiJ.v.ßI. ~ ~JJ\LAJok \VvJ.¡~ JJ"v\t J vJ\ ~JI~)IIÅ}I1'","~A.J . ~ . è '--L'.A...- 25 .' . -'--.... Minutes 5ü- ("' , j () () IJ'\ '-0 ~ N -~-- 995 15:21:39 0.004 .þ. - N ~2 N 0,006 0.008, 0,010 0.012, 0,014 0.016 0,018 0,020 0.022 0.024 0.026 0.028 0.030 0~2 (') reO ~ ~ ~6 (t) þoO o o."ã36 Z o Oß" -.J o 0.032, O.044,Aquired VI t::J N N N ........ o Q ~ (') t:1 JlJ ..... ~ ~ ~ o ::J. & Abundance Ion 191 1 95Z0006- R . 0 amu from m29556501065' d · un at 12: 36 AM COT on Sat . Jun 24, 1995 140000- 120000- 100000- 80000 -- 60000 - 40000 -- 20000 -- - -~. ~ o ~~'-'-~~L),JJJJLjk¡" ~M,,ItJJvþ.J 50 60 . rime (min.) 90 I 90 I SFï I 80 Time (min.) I 75 I 70 o =~ L J .uJvjtf .J ~ JAAA./v ) AL ~ ~ ~ µ."U 1995 Ion 191.10 amu from m29556501065.d 95z0006; Run at 12: 36 AM cor on Sat Jun 24. 20000 - 40000- 60000 - 80000- 100000- 120000- 140000- Abundance 0\ - N N N C) ~ () tJ t:\) ,..,. ~ þd (t) Þ'C) o ~ Z o N -.) o CI ~ n t1 ~ ~ ~ ~ (t) "CS o :4. Z o tv -J o -J -- tv N N Ion 217.20 amu from m29556501065.d 95z0006: Run at 12: 36 AM COT on Sat Jun 24 . Abundance 30000- 20000- 10000 - \ .' , ' =~Jv~ t.o/#JJIlÁ.~~~fNJ.¡I.o'¡ 1(\ \ o I 50 I 55 I I 60 65 Time (min.) 1995 I 70 N , I ~ \ I ,~V~ I 75 Q ~ () tJ ~ ~ ~ (t) >0 o :4- Z o N 30000- -1 o Abundance 20000- 10000 - -~ 0- 64 00 -- N N N Ion 217.20 amu from m29556501065.d 95z0006; Run at 12: 36 AM COT on Sat 0un 24. 1995 AfJVl VJ)I r\,' \. \ I J,r J 'J\ '\ \!\ J ~ V I 66 I 68 I 70 I 72 I 74 Time (min.) I 76 I - Q ~ n t1 ~ ~ ~ ~ ~ o ::\. ~ N ......) o \0 - N N N Ion 218.20 amu from m29556501065.d 95z0006; Run at 12: 36 AM COT on Sat Jun 24, 1995 Abundance 30000- 20000- 10000- - I ~~~WJ~ ~ Jll.vN vJ'J ~JV~~ o 64 I 66 I 68 I 70 I 72 I 74 I 76 Time (min.) Q ~ n t1 ~ r-t- ~ ~ (D to o :4 Z o Ion 259.20 amu from m29556501065.d 95z0006: Run at 12:36 AM COT on Sat .Jun 24. 1995 Abundance N è5 18000- 15000 - 14000~ 12000-- 10000-- 8000 -- 6000 - 4000 - = AkA W , ~ 2000 =N~ ~ ",\flY/\." : AI I\fv) I. lit '/ I I lVI JVI¡' 'l}W'J~I~ ~ /VvVV JvJwAVy 0- I I I I - 64 66 I I I 0 68 70 72 - 74 76 N N N Time (m in. ) C) ~ o tj ~ ~ ~ (t) I'd o :4 Z o N -1 o ...- ...- - N N N " TIC of'm29560301003.d 95z0005; Run at 03: 31 PM COT on Wed ~un 28, =,.. ""'_.~~"."'~.I\l...Jw.\..t.1r,!~~1~~~ ~·~.lnl.~~~tI 0- Abundance 200000- 150000- 100000- 50000- I 40 I 50 I 80 I 100 I 120 Time (min.) 1995 I 140 V'I'' .1 ,_~ ~ I 160 I 180 Q ~ () tj P' -- D) :;d (t) '"C:S o :4 Z o tv -..J o Abundance 6000 - 5000 - 4000 - 3000 - 2000 - , 1000- ~- , 0- ........ tv - tv tv tv I 140 Ion 231.20 amu from m29560301003.d 95z0006: Run at 03: 31 PM COT on Wed Llun 28, 1995 1 I '+1, ft'\'V.MWwW~V~~~ l'I\Þf·'~4 '~V- I 150 I 160 Time (min.) m\ . o s:: 3 æ.. ~ I ..¡, GMC Data Report No. 270 13/222 001 0.02 0.03 '--C\ V\ O.OS N Q 0 () ~ 0.04 0.06 - -- - ----~ Minutes --50 . -------. -- 2'5 -- ---L_~....J..~~~ ~I JJJuJAoJ",¡,ffi.J#J. 4k, ~ ~t w~JuJl ~ w-.~_~_~ ~-- - ------------- ---------- ~4.001 - Channel A '.-r Sgc :995 09:47:21 z:\gcwor1<\ara -~- - ~ -- N N N 0.01 0,02 0,03 0,04 ~ ~ () t; :!,) ...,. :!,) ~ (t) to o ~ ~5 o N -J o .' Sample 10 Acquil'ed C) s:: n t:1 ~ p) ~ (1) "0 o ::¡ Z o N -.J o I-" U\ - N N N 20000-11.... . _ .. J j)Þ"~"--- = ~ ~ J.J....J.,..... vJ.,l.,.,~+ ~ "\'--,' ~,_, ,¡..,..¡.,);jJ t,J. \ l""" ,IV ..J .,., · 0- I I I I 50 ¡,' Ion 191.10 amu from m29556601066.d 95z0007; Run at 02" 24 AM COT . on Sat 0un 24, 1995 Abundance 120000- 100000- 80000- 60000- 40000- I 60 I 70· Time (min.) I 80 I 90 C) ~ () tj ~ ~ :;d ~ o ::1- ~ tv -J o ........ 0\ - tv N N =~-.~ '"'WW~ ~ JJ ~JW .rl}l' J, ÎJ,'~ JJ J tw JÅJ...J...,.JI»'-- 0- Abundance 120000- 100000- 80000- 60000- 40000- 20000- Ion 191 10 95z0007' R . amu from m29556601066 d . un at 02: 24 AM . COT on Sat 0 - un 24. 1995 I 70 I 75 ì I 80 Time (min.) I 85 I 90 C) s:: (") tJ p) t'"1- ~ ?d (1) ~ o ::¡ Z o tv -... o - -... - tv tv tv Ion 217.20 amu from m29556601066.d 95z0007; Run at 02: 24 AM COT on Sat tJun 24, 1995 Abundance 40000- 30000- 20000- \ . ~~N~ I~J A~'~\~~~~Jj~~, 10000- o r 60 I 65 I 50 I 55 Time (min.) ~ ~~ , ì I . 70 I 1 ~ J ~ N¡ ~~ I 75 C) ~ () tJ p) ..... ~ ~ ~ o ~ Z o N -1 o Ion 217.20 amu from m29556601066.d 95z0007: Run at 02: 24 AM COT on Sat Jun 24, 1995 Abundance 40000- - 30000- 20000- 10000 - , r I I r =~ \rw \j\. V\ I 1\ rI\ ì/ ~ ~.~ \. \ - ~ ~ 0 . I r I I· I I . I I r I--" 64 66 68 70 72 74 76 00 -- N Time (m in. ) N N C) ~ () t1 ~ þJ :::0 ~ o ~ Z o N -J o - \D Ñ N N Ion 218.20 amu from m29556601066.d 95z0007; Run at 02: 24 AM COT on Sat ~un 24, 1995 Abundance 25000- 20000- 15000- 10000- 5000 =~ r ^ W\V) 0- 64 I 66 \ ~ I 68 .~ ~"I¡ I I I 70 72 Time (min.) 1\/,\/ ~~U~ I 74 I 76 C) ~ () tJ ~ ~ ~ ~ (I) "0 o ::¡ Z o N -1 o N o - N N N Ion 259.20 amu from m29556601066.d 95z0007: Run at 02: 24 AM COT on Sat 0un 24. 1995 Abundance 20000- 15000- 10000- J 5000 =~.A ~ ;J^^- ^ o 64 I 66 I 68 v( 1 1 II v^ ~".1\ if\A,~ ^~ .. ~, . . JWV'VJV~ ~J V~ I I 70 72 I 74 I 76 Time (min.) Q ~ () t:1 Š :;d (t) Þ'Cj o :4 Z o tv -.) o TIC of m29560401004.d 95z0007; Run at 06:50 PM COT on Wed Jun 28. 1995 Abundance 300000- 200000- 100000- I ... ~ Jl~' -.~,.,u .-Å'~.." v,...._~--LJ.llJ ,~;~ .~ ~~ M.. .~"I"~~~J.. . _.. I -- ,... :: 0 I I I I I I I I I 40 60 80 100 120 140 160 180 tv ...... - Time (m in. ) tv tv N Q ~ () tj ~ ~ ~ (t) Þö o ::t. Z o t:-.) -.} o t:-.) t:-.) - t:-.) t:-.) t:-.) Abundance 12000- 10000- 8000 - 6000 - 4000 - 2000 - o fi ~ I 140 _:.r---....... Ion 231.20 amu from m29560401004.d 95z0007; Run at 06:~50 PM COT on Wed 0un 28, 1995 \ \ - I - ,~ V'J J YtW' 1/ - ~ fit v~ I 150 Time (min.) I~ ~ I\. ~ )v1,.,J ~~ I 160 1- 'I:E :.; "'T1 o , "'" " §. , ."\ I I i I \ I i \ GMC Data Report No. 270 23/222 ~-, ----- z:\gcwork\arCl· .', "'-001 - Channel A ·~Dage 2 of 3 Sample ID : Acquired : --- . Sgc 395 14:39:08 o.@ ~ n o~, ~ ~ o~ ~ o :4 o.~. o N o.~ ---~ '^- ~ f0 0.028 '- -..... f'. 0.026 0.024 0.022 0.020 0018 0.016, 0.014 0,012 0.010 0.008 0,006 o§' .J,,rJMuJftW.~~,J~ ^" \ )v)...1 V· j~·lJ ~ Il J.Jl ~~AA~LJJ~~~~Jj1. µJ M\}J/h.v.., '~J~ 0002. --J____~___n~. --~- 2'5 50----- -.. Minutes 0038 0036 0034 0.032 0.030 0.028 0026 0024 0022 0020 0.018 0.016 0.014 0.012 0010 0.008 0006 0004 0002 C) ~ n t1 ~ þJ ~ (1) "'d o ::¡ Z o .....---'- Abundance ~ 300000- o tv U\ - N tv tv 200000- 100000- o !. I ~ \: (' .4 Ion 191.10 amu from m29553001030.d 9 5r 2116: Ru n at 04: ',22 AM COT 0 n We d 0U n 21, 1995 I 50 l A ~l-t~ ---,-,~~J~ ..)¡... \ v...I' L~ ~",....". ... r I I I I I I I I I I I I I I I 60 70. 80 90 . Time (min.) ---""""" o ~ (} t1 ~ f"'1- ~ :;:0 ~ o ::t. Z o .. r: . Ion 191 10 am f 95r2116" R . .u rom m29553001030.d . un at 04: 22 AM COT on Wed 0un 21. 1995 Abundance tv ð 300000- 200000 - 100000- -, o~~.J¡~ JJvÞv.. Îf~~ JjJLNJ~..-J.Alu--",~kr~ I I ! 1 I I I ' 70 r I I I I . I 75 80 I 85 I 90 N 0\ Ñ N N· Time (m in. ) a ~ n t1 ~ ~ ~ CD '"d o ;::¡ Z o N -.l o N -.l - N N N =~~.~\~~.J.J;\v"~ 0- I I ,I 1 50 55 60 65 r----·· ~ Abundance 120000- 100000- 80000 - 60000 - 40000- 20000- Ion 217.20 amu from m29553001030.d 95r2116; Run at 04: 22 AM COT on Wed Juri 21. 1995 \ J ! , . ~ I J I \ J \ ~ J -v~ I 70 75 Time (min.) C) ~ n tJ ~ ~ ~ þd (þ "0 o ::t. Z o N -1 o Ion 217.20 amu from m29553001030.d 95r2116; Run at 04:22 AM cor on Wed Jun 21. 1995 Abundance 120000- 100000- 80000- 60000 -, 40000 - =vltvu ~ ~ ~ .IV , r \~ J IJ } J ~ . ~dìv~~~~ 20000- , , þ "\ 0 I I I· I I . I I I N 64 66 68 70 72 74 76 00 - N .. Time (m in. ) N N C) s:: () t1 ~ ~ :;0 (I) '"CS o ::¡ Z o N -J o N \0 - N tv N Abundance 70000- 60000- 50000- 40000- 30000- 20000- 10000- Ion 218.20 amu from m29553001030.d 95r2116; Run at 04: 22 AM COT on Wed 0un 21. 1995 =~JvvM) o ...- 64 I 66 "\ ~ , , ~ o J, I I . I I 68 70 72 Time (m in. ) I \ jI, J ~ "Ij~\)~ I 74 I 76 Q ~ () t1 ~ r-t- ~ ~ CD '"CJ o ~ Z o tv .......:¡ o w o - N tv N ~_.- Ion 259.20 amu from m29553001030.d 95r2116: Run at 04: 22 AM COT on Wed Jun 21, 1995 Abundance 60000 -, 50000~ 40000- 30000- 20000- 10000-" ~ f ~~,~Jw/' ~ IV o -- 64 I 66 I 68 \ ~' ~^;V'r ~ rvv \rwvv~~'N'~ I I 70 72 I 74 I 76 Time (min.) C) ~ () tj ~ ~ ~ ~ ~ o ~ Z o N -1 o (..) - -- N N N TIC of m29557901079.d 95r2116; Run at 07: 46 AM COT on Sun tJun 25, 1995 Abundance 250000- 200000- 150000- 100000- )J'l'" " ..."'. 50000 ~ J j JJi.JY = ~~~_ ._~JJ..M I ~~~~.~J.J~J!A~~ o I 140 I 160 I. I 180 I 40 r I 100 120 I 60 I 80 Time (min.) Q ~ n t:1 ~ ~ ~ ~ o ::¡ Z o Abundance N 140000- -.J o W N - N N N 120000- 100000- 80000- 60000 - 40000- 20000- Ion 231.20 amu from m29557901079.d 95r2116: Run at 07: 46 AM COT on Sun 0un 25, 1995 o I 140 I 150 Time (m in. ) ~-vJ<\ 4~LL- I I 160 GMC Data Report No. 270 33/222 'I=E ~ ." o '""'I Q) :;, . "",- ,- Sample 10 Acquired .. Sgc ~995 16:15:43 0.012, (;) ~ () Ö Š ~ ~ o :4- ~O N -.J o 0.008 0.006 0.004 ~ _ ~I t §2~~~)W' . I ..~ I ~ ~~ 1~1 2'5 z:\gcwork\ar( "I ~ -"'5.001 - Channel A , ~I Minutes ~ f ¡.j , ~ ~ ql. II , \ ~ '-:::J- - ~- 0.012 -..f.\ '^ ,)j N 0.010 '- "'-.J 0006 0.006 ~. ~~~ "'" ~ ~ ·50-- ,0.004 ,0002 C) ~ n t1 ~ ~ :;d ~ o ::\. Z o N -.) o (;) IJ\ -- N N N Ion 191 10 amu f 95r2117; Run ~t 03-.. rom m2955400 1040 . d .28 AM COT on Thu Jun 22. 1995 Abundance 250000- 200000- 150000- 100000- 50000- o - ~ ~~~....L ...LkJl. ~,lÁ~~~ .AI ,J A/.", · \<Iv. It';" .¡~JJJllJ~ I I I I I . . 50 .1 I . I I I 60 I I I I I I 70 80 I 90 rime (m in. ) C1 ~ () t1 ~ .-+ ~ ~ (t) ~ o :4- Z ~ tv -..) o w 0\ - tv tv tv /-----.., 95 Ion 191.10 amu from m29554001040.d r2117, Run at 03° 28 AM COT . on Thu Jun 22, 1995 Abundance 250000- 20000ú- 150000- 100000- 50000- ="'.JV J ~..) 'IWJ ~ ft. \. ~ ~ _ JV.- ~ J ^ ~ L MJ J ,.mJv .,J ~ J NA..) 0 ~.Å--A o I 70 I 75 I ' I 80 Time (min.) I 85 I 90 Q ~ n t1 ~ ..... ~ ?d ~ o ~ Z o N --1 o w --1 --. N N N ,---- - Ion 217.20 amu from m29554001040.d 95r2117: Run at 03: 28 AM COT on Thu Jun 22. Abundance 50000- 40000 _. 30000- 20000- 10000 - - l ., =~NNv..1 "'.w V\,\IJu~J ..JJw1J.I~J\^ 0} 0- I 50 I 55 I I 60 65 Time (min.) 1995 -' '\- I 70 I d I~V~~ 75 Q ~ () t:1 ~ ...... ~ ::0 ~ o ::¡ Z o N -l o Ion 217.20 amu from m29554001040.d 95r2117: Run at 03: '28 AM COT on Thu tJun 22. 1995 Abundance 40000- 30000- r 20000- 10000- "' it} ="IA'viV f ^ J\ V V JI - \ r , ~ ~ v ~A\'~ v~~ II o- J I I I I J I 64 66 68 70 72 74 76 ~ 00 - Time (min. ) N N N Q ~ () t1 ~ £ ~ CÐ >0 o ;:¡ Z o N .........t o v,) \0 - N N N ,,,-. Ion 218.20 amu from m29554001040.d 95r2117; Run at 03:28 AM COT on Thu Jun 22. 1995 Abundance 40000~ 30000- 20000~ 10000- . ~ =~rJj\r~)\\\\/~\ ~ AV~ ~ '\AJ~~~J~ 0- 64 I I 70 72 I 74 I 76 I 66 I 68 Time (min.) :------. C) &:: () tj š ~ .g o ::\. Z o N 20000- -1 o Abundance 18000- 16000- 14000- 12000 - 10000- 8000 - Ion 259.20 amu from m29554001040.d 95r2117; Run at 03: 28 AM COT on Thu 0un 22, 1995 6000 - .. A ) I 4000 =J.vfl.V^ VV ~ 2000 - ~ o - N N N 0- 64 I 66 ~ I, Af A I 68 \ ( I Wt IV/I .\\, '\l)~v\ i h'M 1\/ Ïj~ I I 70 72 I 74 I 76 Time (min.) I 180 ~ I 160 Time (min.) I 140 I 120 I 100 I 80 I 60 I 40 o -. ~. 10000 _ ~1'II.r-- 1 I , II, ! h. . luL., , 1 II ....11 J I~ .~. /,¡¡, LLIIN. _ . . -'~"'hLt-...-~ ~AJA~ ,'IJfIJ\W ~ Þ ~ ""'I".~' 'fI" 'l' "'"! I 1995 TIC ofm295580010BO.d Run at 11: 05 AM COT on Sun 0un 25, ~ ~5r2117; - 20000- - 30000- - 40000 - -, 50000- - 60000 -= - 70000-' - 80000- - 90000 - - 100000- Abundance / ~ Þ-" - N N N Q s:: () t:1 fI,) ~ fI,) ~ (t) "0 o ::+ z o N -.1 o .~.....- C) ~ n t:1 þ:) r-t- þ:) ~ ~ o :4 Z o Ton 231.20 amu from m2955B0010BO.d 95r2117: Run at 11: 05 AM COT on Sun 0un 25. 1995 Abundance !j 40000- o 30000- 20000- 10000- .p.. N - N N N I 140 ~~w I 150 A.M.'W\J-j~~~ 0- I 160 Time (min.) Ii ·1 GMC Data Report No. 270 43/222 ,. 0.006 ~ ~nl~ij ~ W,ß I I ~w J 0.008 '\ I I ¡ 0.004 \ ! J\, 0.006 'w t \~ - I~~/ N N N~ '""""^ 0.004 ~ - Minutes - - - ~ .' SO' 0.008 '-..(' , 0012 ~ ~ N -...... ........ ~ 0.010 0.010 C) ~ n t1 ~ fJ ~ ~2 o ::1- Z o N -.) o ':'d.~t:: ¿ UL ~ ~1.001 - Channel A z:\gcwork\arcc' , Sgc 995 17:31:47 Sample ID Acquired . . Q ~ n t1 ~ ..... ~ ~ ~ o ~ Z o N -l o ~ Ut - N N N ,/----, -- Ion 191 10 amu f 95r211S- R· rom m29554101041.d . un at 05: 16 AM COT on Thu Llun 22. 1995 Abundance 300000- 200000- 100000- o ~~~~~...L--L~Jl. ~,l.ih..AJ ,.,J" ,JAJ.J4. ,I~ t~.¡kvJ.,\J~ I I I I I I I - 50 I I I 60 I I I I I 70 I I I 80 I 90 Time (m in. ) ~'-- ----- .r"-- -- C) s:: (j t:1 ~ r-+ fI,) ~ ~ o ;:¡ ~ Ion 191.10 amu from m29554101041.d 95r2118; Run at 05: 16 AM COT on Thu 0un 22, 1995 Abundance N -.....1 <::> 300000- 200000- 100000- - _~ ,A...J\) ~ 'vJvu ~ h \, ~ I \,J" ~.M.- J A ~ ,} W J ~..,J kJ ,.ÞAtÅ.J 0 ~ 0 I 70 I I I ~ 75 80 I -- 85 N 90 N N Time (m in. ) C) s;:: n tJ ~ .... ~ ~ ~ o ::¡ ~ ~ Ñ N N Ion 217.20 amu from m29554101041.d 95r2118; Run at 05" 16 AM COT Th . on u Jun 22, 1995 Abundance N --..) o 70000- 60000- 50000- 40000- 30000- - ¡ 20000- 10000-=: _ _ I ] I =~~J~<lJ ~Jj..~ ~.JI%~)'1'A} 0- I 50 I 55 .1 I I 60 65 Time (min.) l'V V J I 70 - ---... r "~~ ~\ ~~ I 75 C) ~ () t1 ~ þ) ~ .g o ::4- Z o N .....,J o .þ. 00 - N N N -~'. Ion 217.20 amu from m29554101041.d 95r2118; Run at 05: '16 AM COT on Thu Jun 22, 1995 Abundance 30000- 20000- 10000-, 0' =\.vl~/~11 }I o I 66 64 ~ J , r ~ I J \. I 68 I I '70 72 Time (min.) 'f\ \ I~ ~ I 74 I I 76 --....-. o ~ () tj ~ :;0 (t) ro o :::¡. Z o tv -.I o Ion 218.20 amu from m29554101041.d 95r2118; Run at 05: 16 AM COT on Thu Jun 22. 1995 Abundance 30000- 20000- \ 10000 - ~ L P I rVV · VI I~ ~ JJ. IrJJ~ r ~ . \ ) \' ~. "- =~I'ýV~ \ 0- I I I I . I I I 64 66 68 70 72 74 76 ~ 1.0 - tv Time (m in. ) tv tv C) g: (j t1 þ) ..... !:\) ::0 (þ þO o :¡ Z ? 95r211:onR 259.20 amu from m29554101041.d , . un at 05:,16 AM COT on Thu 0un 22, 1995 Abundance !j 18000- o u. o - N N N 16000- 14000- 12000 - 10000- 8000 -. 6000 - 4000 ~ \ ~ J V f ~ J / V'v 2000 - 0- 64 I 66 Î I v ~ I J ~ 'V ~ \r "~ ~ ~J.~ J\ \ ' Fir I 68 I 70 I 72 I 74 Time (min.) 'i'Vf~fl I 76 I . Q s:: n t1 þ) ...,. ~ ~ ~ o ::¡ ~ N -J o Ut to-' - N N N Abundance 140000- 120000- 100000- - 80000- - 60000- - 40000- - 20000- o -~ ¿ , , ,,,.., I 40 _ ~ 'iIII'" .... 95 2 TIC Of r 118; Run m2955810 at 02: 24 PM 1081.d COT on S un " . ..~_w~1¿~~ "J.~ JA ~~ ,J-, ~ I I I 60 'It.. -. I 80 I 100 Time Jun 25, I 120 (m in. ) 1995 , JI I 140 I 160 I 180 VI tv - tv N tv C) ~ () t:1 S :::0 ~ o ~ Z o N -1 o Abundance 60000- 50000- .40000 - 30000 - 20000- 10000- ~, Ton 231.20 amu from m29558101081.d 95r2118: Run at 02: 24 PM COT on Sun Jun 25, 1995 o I 140 ~~~ I 150. Time (min.) u ~.^ ~,~ ~~ I 160 o -.: en ~ ""C ~ GMC Data Report No. 270 53/222 "i:JUlpttt IU ~ ~~ired ~ O.~ ~ n O''e' ~ ~ O.ð!m ~ o O,a. z o o.~ o 0.030 0.028 0.026 0.024 0.022 .0.020 0.018 0.016 0.014 0.012 0,010, 0.008 0.006 Ut O.¡lO4 Ñ N N 0,002 ~gc 195 18:58:07 .l .G}L L-..L~..J".w~..... ' --,--~- z:\gcwork\arcc' -·:....001 - Channel A ~-'·t)age 2 of 3 ------ --- --- 0.040 .0.038 0.036 -..i) 0034 '^ ~. .0,032 'tv '- . ,0030 }v 0 0.028 0.026 ,0.024 0.022 0.020 0.018 0.016 .0.014 0.012 0010 0008 '.J MIll t~ . ~~ß,~ ~h~~ÅuÀdAM~YÀ.M.Jw~~~\O~ '. ---------.A.. . 0.004 -----'^---. 0.002 2'5 ---s<).--.--... - Minutes C) ~ () t1 ~ ..-+ ~ :;d ~ o ;¡ ~ tv -t o Ut Ut - tv tv tv Ion 191 95r2120' R .10 amu from m2 . un at 01: 07 9555201052 AM COT . d on Fr i Llun 23, 1995 Abundance - 160000- 140000- 120000- . 100000- -, 80000- - 60000- -- 40000- o _~~~~~~~.~.~~~~ ,,,,r.Ll~J. ~/ 1."J.¡)~,jM¡.--~ I I I 50 I I I 60 -, 20000 - I 70 I 80 I 90 Time (m in. ) Q s:: () tj ~ .-+ ~ ~ CD "0 o ~ Z o tv ......,J o lit 0'\ - tv N tv Abundance 160000- 140000- 120000- . 100000- 80000- 60000- 40000- Ion 191 10 . amu f 95r2120: Run at 01. rom m29555201052.d . 07 AM COT . on Fr 1 ,"",un 23, 1995 _. 20000 =W"~"J~~,,JlJV'\fivi. ))..,fM ;JN~ ~ J. ^J.J~ \^,,~J~J~ 0- I 70 I 75 I 80 -Time (min.) I 85 I 90 Ç) ~ () t:1 ~ ~ :;d (t) ~ o ::¡ Z o tv .......) o VI -.I - tv tv tv Ion 217.20 amu from m29555201052.d 95r2120; Run at 01: 07 AM COT on Fr i 0un 23, 1995 Abundance 70000- 60000- ~ 50000- 40000- 30000- 20000- . 1 10000- ; , =~~NJ~.J~~~~~~JvNÀJ¡1 \\ o I 50 I 55 I 60 I 65 Time (min.) , ~ I I ~ I ~i! ~V~ II 70 I I 75 C) ~ (1 tj ~ ~ ~ ~ o ::t. Z o Abundance tv è5 50000- 40000- 30000- 20000- Ion 217.20 amu from m29555201052.d 95r2120; Run at 01· 07 AM COT . . on Fr 1 Jun 23, 1995 10000 =N ~ Jvtl .A A ' Ut 00 - tv tv tv o 64 I 66 I \ ' \ \ I 68 --... \ I j \', "\~ V .~ \Y\y~ 'I I I 70 72 Time (min.) I I 74 I 76 Q ~ n t1 ~ p) ~ .g o :4- Z o N -I o U. \D - N N N Abundance 40000- 30000- 20000- 10000- =~ o 64 ~ Ion 218.20 amu from m29555201052.d 95r2120; Run at 01: 07 AM COT on Fr i Jun 23. 1995 r, r JJV ,",^'jl, J NJ\ ~ \II \;~ J), V I 66 I 68 I 70 I 72 Time (min.) I ~Vv ~~ I 74 I 76 Q g: n tJ ~ ~ ~ ~ (t) "'0 o :4 Z o tv -.J o 0\ o - N N N Ion 259.20 amu from m29555201052.d 95r2120: Run at 01: 07 AM COT on Fri Jun 23, 1995 Abundance 25000- 20000- 15000 - 10000- 5000 ~Á¡ "~\ fw ¡ ) ~ I o 64 I 66 J ~ ^ ~ I r' A i I 68 J ~ ) ~~ ----- ,'~fvIJ) ~~'~~ I I 70 72 I 74 Time (min.) I 76 Q ~ () tj ~ ~ ~ ~ o :¡ ~ N -.] o 0\ ...... N N N Abundance 100000- 80000- 60000- 40000- 20000- I 40 95r2120; I 60 TIC 0 f 2 - R m 955820 un at 05: 44 PM 1082.d COT on S un Llun 25, - -;. - ¡ I 80 I . 100 ~ "I'~..... '*"'n~."J..,~1.~J~ ~\ ~ ~..~, ~~ I o Time (m in. ) 1995 I, ,~~þþÞ AI - I 120 I 140 I 160 I 180 C) s:: o t1 ~ r"1" p) :;d (Ð '"0 o ::1- Z o tv -..J o 0'\ tv - tv tv tv .-., Abundance 25000- 20000- 15000- 10000- 5000 - I 140 Ton 231.20 amu from m29558201082.d 95r2120; Run at 05: L14 PM COT on Sun 0un 25, 1995 1 I- I 150 I =-.M...)~~~N 0- Time (m in. ) w ~ ¡J ~ IWur ~~ I 160 j I I I GMC Data Report No. 270 63/222 0002 -0.003 --50-- --- ~._------- Minutes 2'5 0.002 ~ §~, 0.003 0.005 J . VI 0.005 t ~ \. 0.004 0.004 0006 0007 N ~ 0.008 '- ,0.009 '-!.\ "--" }so N ,0010 ---. ------~----~---- ~Jage :¿ or 3 -I ~ ~I ~¡ 11\ -: ~.001 - Channel A 0.006, '" 0.007 ¥ · !IJ I~r °ao ~ (') t1 ~ ~ @J9 o ::4- Z o N -J o 0,008 z:\gcwork\arct - ;jgc 995 20:24:22 ;jSmpl9 IU : Acquired :' --- C') ~ () t1 ~ ~ ~ ~ o ::\. ~ .Ion 191.10 amu 95r212~ Run t .. from m29554301043.d a . 08. 53 AM COT on Thu 0un 22. 1995 Abundance !:j 120000- o 100000- '. 80000- 60000- 40000- 20000 = .. . ... .. 11~ _~~~~.......~~L,:.r..J1JM.¡....-%. \ 1*., L.JJ o I 50 I 60 I 70 I 80 I 90 G\ U¡ - N N N Time (min.) Q ~ () t1 ~ ~ ~ ~ ~ o :::¡ Z o N -J o 120000- Ion 191.10 amu 95r2122; Run at 08; 53 from m29554301043 d AM COT on Thu Jun' 22. i 995 Abundance 100000- 80000- 60000- 40000- 20000-- = ~ L '" ~.J; JJLlNv J J\f^HWiA.. 'v A ~ J! "LA W ~w o - - I 70 I 75 I 80 Time (min.) I 85 I 90 ~ - N N N Q ~ () t; ~ s ~ (D toO o :4 Z o N -J o ---------- Ion 217.20 amu from m29554301043.d 95r2122; Run at 08: 53 AM COT on Thu Jun 22. 1995 Abundance 30000- 20000- 10000- =~A}NJ~~, ^~IM~~J\IA)·\¡/¡}4 j I ~ \ J I ¡ I \Î ., ~ ~ \y~ 0- I I I r I I I 0'\ 50 55 60 65 70 75 -J - Time N (m in. ) N N Q ~ () t:1 ~ ~ ~ ~ ~ o :4- Z o N -J o 0'\ 00 - N N N /---- Abundance 30000- 20000- 10000- -/---=--........ Ion 217.20 amu from m29554301043.d 95r2122; Run at 08: 53 AM COT on Thu 0un 22. 1995 ~J,~Jwv J~ 0- 64 I 66 ,~I \ \. I 68 ,_ j t / \J . \ J\ V ~ V~'~ I I 70 72 I 74 Time (min.) I 7G o- J I I I I I I I I I I I J J J I I I I I I 1 I I I I _ 0\ 64 66 68 70 72 74 76 \D - N TiP.ïe (m in. ) N N I '\ J"''¡ ~ ~~~ . _ I ' 5000- ~ ~.', ~ - ' ( , . ~ _~ ~ )V'v V\) " ~ ~ \ ~ !\ \ 10000- 15000- 20000~ 25000- Q ~ () t:1 ~ ~ ~ ~ .g o :4- Z o N -J o Abundance Ion 218.20 amu from m29554301043.d 95r2122; Run at 08: 53 AM COT on Thu 0un 22. 1995 ~- .~--- Q ~- () o ~ ~ ~ ~ ~ o :::¡ Z o N -J o -J o - N N N ...,/---~. Ion 259.20 amu from m29554301043.d 95r2122; Run at 08: 53 AM COT on Thu 0un 22. 1995 Abundance 18000 - 16000 - 14000- 12000- 10000 - 80Q()- ~ ::::~i~~J/~ r~ J^ ¡I; in I"'\'\A~~~~~ 2000 - 0- 64 I 66 I 68 I I 70 72 I 74 I 76 Time (min.) /~--- Q ~ () t; ~ ~ ~ (D toO o :4- Z o N ð 200000- Abundance 150000- 100000- 50000- -I- .. o -J - - N N N , ,,_, j l , _ I 40 ~-"'-.. TIC of m29560701007.d 95r2122; Run at 04: 47 AM COT on Thu Juri 29. 1995 ':.~< -.-- 1 ~' '~~I ~~, l;'~ '. ,)# . ~.~ ,,~. \,),HM~"'~ .~. -"'- I 60 I 80 I 100 I 120 Time (min.) I 140 I 160 I 180 Q ~ () t1 ~ ~ ~ ~ (I) ~ o :4- Z o N -J o 95r212~onR 231 .20 amu from m2956070 1007 . d . un at 04: 47 AM COT on Thu Jun 29. 1995 Abundance 30000- 20000-- 10000 - _ ,~'\. ,\~\;~,IJ.~~~'\^N.W ~~.·~A·~~\\~ -~~ \\ o I 140 I - I 150 I 160 Time (m in. ) -J N - N N N 73/222 GMC Data Report No. 270 rn If -=**= f\) Sample 10 : ' Sgc ~~uire~~ 99521:50:33 C) o.~ t; ~ S o.~ (t) toO o :4- O.~ o N -J 0~4 0022. 0.020. 0.018 -a.~<= ¿ u'- z:\gcwork\arCt 1.001 - Channel A ---~ - --~ --- ~-------_. 0.030 0.026 ---..0 \J\ '- .0"026 rV N ........ 0024 N '\ 0022 0.020 0.018 0.016. 0.016 0.014 0.014 0.012 0.012 0.010 .0.010 0.008 0.006 8,Q04. ~ - N N N 0.002 . ..1 I }~I~ ¡JJ 1~v..J1.A"~J.'J"W..1' '1"\' 0.008 I~ : ^ hi I~ \~ ~.M\" ~ ~I.I .' \h.~.I!h ,I ~ . . I~~~ ~~\~'V f~\lnM~IIJ~\I. Jl . . v~ ~J '* \\ . M.J. ~ ~ 0.004 ~----"-----^-_._--- 0.006 0002 ------- - --so- i5 Minutes Q ~ () tJ ~ ~ ~ ~ (D to o :4-' Z o N -J o -J V- - N N N .v. ~ '.. . I I I ~~I "-'-'~~<'~M,,,,^-J.ÞJlJ.Jrjll.Jt.)...Jw~J,r..J"""'J~ I I I 50 ' 60 Ion 191 10 . 95r2128; Run ~t 1;:m~1 from m29554401044 d AM COT on Thu 0un" 22. 1995 Abundance 300000- 200000- 100000- o I 70 Time (m in. ) I 80 I 90 Q ~ n t; ~ ~ ~ (t) toO o ~ Z o N -J o -J 0\ - N N N . . Abundance 300000- 200000- 100000- Ion 191.10 amu from 2955 m 4401044.d 95r2128; Run at 10: 41 AM COT on Thu 0un 22. 1995 -~_~I."w-J~^þ~C Ii';"'^"\ \J~ d A-vJwMJ!0l~~v/~--J'~ 0- I 70 I 75 I 80 Time (min.) I 85 . I I 90 Q ~ n ö þJ ~ ~ ~ ~ o :4- Z o N -J o -J '-J Ñ N N ./-". Ion 217.20 amu from m29554401044.d 95r2128; . Run at 10: 41 AM COT on Thu 0un 22. Abundance 40000 - :.... 30000- 20000-' 10000 - ~.J Jv '" \ . ~ w.;JI '^ ~ J ~J/lJJ...J \J fiw,/w ,iAl ~ ~,. I . \ o -- I 50 I 55 I I 60 65 Time (min.) 1995 I t II 70 Í I ~~~~ I 75 I 76 I 74 I ~ t \ r . 1\.1\ \ .~ \; ~ ~ Time (min.) I I I I I :70 72 ¡\ I ) I) \ \ I I 68 0- 64 I 66 ~U~ ~ Jv~ 10000 - 20000- 30000- 40000- Abundance Ion 217.20 amu from m29554401044.d 95r2128: Run at 10: 41 AM COT on Thu 0un 22, 1995 -J 00 - N N N Q ~ () t1 ~ ~ r:u ~ (1) toO o ::t. Z o N -J o C) ~ () t; ~ ~ ~ ~ (1 toO o :4- Z o N -J o -J \D - N N N Ion 218.20 amu from m29554401044.d 95r2128: Run at 10: 41 AM COT on Thu 0un 22. 1995 Abundance 40000- 30000- 20000- 10000 - t I . =~ vf'^ \Ai}.' .J ~ 1\ Af\ v.. '\j ~ 0- 64 I 66 I 68 I 70 Time (min.) ,. 1 '" ) I . ~ \. · \. ^ \ 'vi U'v..j\ VV IJv-.,J Iv ~ I 72 I 76 I 74 Q ~ (j t:1 ~ ~ ~ CD toO o ~ Z o N -J o 00 o - tv N tv ~~-~ Abundance 25000 -. 20000- 15000- 10000- 5000 -. ~jV~1 V' N o -- 64 Ion 259.20 amu from m29554401044.d 95r2128; Run at 10: L11 AM COT on Thu 0un 22. 1995 , Jvv ) J ~ Â V' ~ ~ ~) r I 66 I 68 I 70 \ \ ~, Time (min.) ,\ \/1\/ '1M¡ ~Ai ì~ 72 I 74 I 76 C) ~ (1 t1 ~ ~ :;d (t) toO o :4- Z o ,""_.... 95r2128; TIC of m29558401084.d Run at 12: 22 AM COT on Mon Jun 26. Abundance !j 500000- o 00 ~ - N N N '.ß.,. o ~~U'''-J\J~~l.~t~.".tAI~~H~tAwJ, .J~ ~.~l~~V I J I I I I 40 60 400000- 300000- 200000- 100000- I'" I 80 > I I 100 Time (m in. ) I 120 1995 ,- --,. I 140 I 180 I 160 Q ~ (") t:1 ~ ~ ~ ~ (t) '"0 o ;:¡ Z o N -J o 00 N - N N N Abundance 40000- 30000-' 20000- 10000- . \ " t r J ~ \¡VA, I o I 140 ------- Ion 231.20 amu from m29558401084.d 95r2128; Run at 12: 22 AM COT on Mon L1un 26. 1995 I i ~ , . ~ \ ~~j ^~~ I ·150 . Time (min.) ~~} ,i!{I¡) ~~ I 160 'Iii , (t) " r:: -~ ,"'" GMC Data Report No. 270 83/222 0002 0004 0.006 0.008 0.010 0.012 0014 ...J:\ 0018 \.'\ ~ N "- 0016 ~ ~ 0020 ?age 2 of 3 50---. Minutes ,II ,I!, fk'~ ~ «M ~~~\.\ ~ . I., ~ \j\I ~ VV· oj ",JI , ~~AJJ~~.~I\~~W" "~ -~.... z:\gcwork\arcc . "i.001 - Channel A is 00 ~ ~OO2 ~JJ~ ..~ ,) l ~ ;.j µI N \.¡ ,j ~ I. .VlII 0.004· 0.006 0.008 0.010. 0.012 0.014 Q o~o. () t:1 p:I S ~ (D Dg18 ~ Z o N -J o 0.016 .~ Sgc 995 23:16:42 Sample ID Acquired C) s:: () tJ þ.) S ~ .g o :4. ~ :r---- . Abundance N -J o 200000- 150000- 100000- 50000- O· 00 V\ - tv N N ,~. Ion 191 95r2145' R .10 amu from . un at 12; 29 PM m2~554501045.d COT: .f) n Th ~ U 0un 22. 1995 ...-..........., I "-'-~LL.,.~c....v\ "" 4.· .JlJJ~ ~ J., j t;.; .¡Jw.,~¡;"'w ~ I J . 60 I I I I I . 70 I I I T· Ime (min.) I all 90 r'-,·. .~_....\. Q ~ () t:1 ~ S ~ .g o :4- Z o N -J o 10n 191.10 amu from 95r2145; Run at 12: 29 PM m2955450 1045. d COT_on Thu Jun 22, 1995 Abundance 200000- 150000- 100000- 50000- I 00 70 I I 0\ I - 75 N 80 I N I N· 85 Time (m in. ) 90 =~ v~" ~ ~ JJ J)l JJ-wvf\' Nt ""^' }V Nu J ~ -J~.J;vJv.-/ J ~ 0- C) ~ () ö £ ~ (D "0 o :::¡ Z o N -.I o 00 -.I - N N N ~- 0"'--" Ion 217.20 amu from m29554501045.d 95r2145; Run at 12: 29 PM CO~ 'on Thu 0un 22. 1995 Abundance 50000- 40000- 30000- 20000- .- . 10000 - =~~~J~JJJ~~I~M~\lo' ~, o I 50 I 55 I 60 I 65 Time (min.) I .~ I 70 ~ ~Jlv~ I 75 C) ~ (") t:J ~ ~ ~ ?d ~ o :4 ~ tv -J o 00 00 - tv N N --'~" Ion 217.20 amu from m29554501045.d 95r2145; Run at 12: 29 PM c~T:on Thu 0un 22. 1995 Abundance 50000- 40000- 30000 - 20000- 10000 - =JNJ'~ Af\^ 'j, ~ " . 0- 64 I 66 ( ! '\ ~ I 68 \JI {I N \ I I 70 72 rime (min.) \ '^ J ~ ~lv'~~ I 74 I 76 o- J J I I I I I I I I I I I I J I I I J I I I J I 64 66 68 70 72 74 76 00 \D - Time (mi n . ) N N N \M ~ A.-~ ~ j '\ A v r ~. \A~\l ~jJl\, - I =~IAfÂW L 10000 - 20000- 30000- 40000- 50000- Abundance Q ~ (j tJ ~ S þrj ~ o ~ Z o tv -J o Ion '218.20 amu from m29554501045.d 95r2145; Run at 12: 29 PM COT "'on Thu Juri 22. 1995 ,.;. --... ..----........... .'~> ,~-" Tire (min.) I 76 I I I I I .70 72 I 68 I 66 0- 54 I 74 ~ . ~ 5000 ~ "v\v J ~ ,^ ~ i' j '^ It', ,~\ f^v\'ifll tJN ¡ An -Jl ~. 4/' '" / . 0\,. jV'\ ~ 10000 - 15000- 200GO- 25000- Abundarce Ion 259.20 amu from m29554501045.d 95r2145; Run at 12: 29 PM COT ~on Thu 0un 22. 1995 . .. \0 o - N N N C) s:: () t; ~ ..... ~ ~ ~ o :::¡ Z o N -J o C) ~ n Ö tI) ..... tI) ~ (t) '"0 o :::¡ Z o N -J o \0 - - N N N Abundance 20000 - 15000- 10000- . 5000 - ~ =.~' ~~ ~ o I 140 Ion 231.20 amu from m29558501085.d 95r2145: Run at 03: :40 AM Co}.on Mon 0un 26. 1995 ~ ~ J o \YAJ\J ~~ I 150· Time (min.) . ~ ~ 'W) \.~!IJ'Vl~ I 160 Q ~ (') t;;I ~ ..... ~ ~ (11 "1::j o ~ Z o N -.1 o \0 N - N N N ,..---. . . ---------. TIC of m295585010B5.d 95r2145; Run at 03: 40 AM CD_T..on Man Jun 26. 1995 Abundance 200000- 15000G- ., 100000- 50000- . I' I! = ~l~"úJh~"." ¡J ..J.1j LJ ~~ . o I 40 I 60 - . - ~~J~ \i~~'.J~ ,I..~~ .~ !..:..:~. f 80 I r I 100 120 I 140 Time (min.) ---, I 160 I 180 93/222 GMC Data Report No. 270 0002 -- 0004 0006 0008 0.010 0.012 0014 0.016 0.018 0.020 0022 .0024 0.026 0028 "-~'.Page 2 ot 3 Minutes 50 - I ~ ,~W\ ~\~N~~~( ,JI ,I, P~\tV'" '.,\. J. ~~i~~ '~~~ ~~. .A ""- <><\' ......... t-J ~ \}".: ~ 25 0.004 \0 .... . [2~J1JUJl N.~,'l~IM~'J~, 1 \.¡i J ~ 'J! ~\ \~ JrJJJt~ I 0.006 0.008 0.010 0.012. 0.014 0.016 0.018 0.020 0.022 C) ~ CØ18 t1 ~ -- ~ ~6. toO o ~ ~4. N --....1 o .~. z:\gcwork\arc- :-'i001 - Channel A ~-. . 'I Sgc 1995 00:42:46 Sample ID Acquired Q ~ () t:J ~ ~ ~ ~ ~ o ~ Z o N -J o \.0 Ut - N N N ( Abundance 200000- 150000- 100000- 50000- o -, Ion 191 95r214S' R .10 amu from . un at 02; 17 PM m29554601046 COT 0 n Th . d U 0un 22. I 50 .' ~. 1995 --...... .J-~~,.~,~\~,"..,JJ.JJ~ ..IV\; tk.~",»À<J~ I I I 60 I I I 70 Time (m in. ) I ·80 I 90 Q ~ () t1 ~ ~ ~ (1) I'd o :4- ~ Ion 191.10 amu from 95r2148; Run at 02;17 PM m29554601046. d CD} ~on Thu 0un 22. ~' 1995 Abundance N -J o 200000- 150000- 100000- 50000- \0 I 0\ 70 I '1 - I N 75 N I N 80 I 85 Time (m in. ) 90 =~ J -M '. ~ -w,J J ~~ J),V"W., I J tAA. . j J A,JJ ~ cJ JiMN v)VIÀ./ J ~ 0- Q ~ () t:1 ~ S ~ (1) '"d o ::1- Z o N -J o \D -J - N N N· ./ Ion 218.20 amu from m29554601046.d 95r2148; Run at 02: 17 PM COT ~on Thu 0un 22. 1995 ,,: .. Abundance 60000 - 50000- 40000- 30000- 20000- 10000- =~vJVJlJv) o~ 64 I 66 v" ~ I f JJ\'\ ~ \A~~ I 68 I I 70 72 Time (min.) ( ,ill./' ~~J~ I 74 I 76 Q ~ n t1 ~ ~ ~ ~ ro I'd o ~ Z o N -J o \0 00 N N N Iün 217.20 amu from m29554601046.d 95r2148: Run at 02: 17 PM COT on Thu Jun 22. 1995 .' Abundance 60000- 50000-:- .-- 40000- 30000- 20000- .. 10000 - ~~JA.L.~LJw.J\)JJt,.JÀ ~V~·~ fIA 0- . \ I 70 I 50 I 55 I 60 I 65 Time (min.) } " ~ \ } / ~ V~~ I 75 Q ~ () t1 C) ~ ~ ~ (Ð ~ o ~ Z o N -J o \D \0 - N N N Ion 217.20 amu from m29554601046.d 95r2148: Run at 02: 17 PM COT -Dn Thu uun 22. 1995 Abundance 60000- <, 50000- 40000- 30000- 20000- 10000 - ' =A~~ ~ ~^^ \, o 64 I 66 i I 1\ I "'¡. I 68 If -' . " ~ ~ \ ·\lv~~~~ I I 7Q 72 Time (min.) I 74 I . I 76 Q ~ (") t1 P' !J ~ (t) '0 o ~ Z o N -J o - 8 - N N N Abundance 30000-' 20000- Ion 259.20 amu from m29554601046.d 95r2148; Run at 02: 17 PM COT on Thu 0un 22, 1995 \ - )1 ~ =;^vJJJ^ ~ V\ 10000- o~ 64 I 65 I 58 -' ..;. V t ~ N J ~ \{J' I ·\NrM'j"JI..~ rvM~ I '1 70 72 Time (min.) I 74 I 76 '.. Q s:: () tj ~ r-t- ~ ~ (t) "CI o ;:t Z o TIC of m29558601086.d 95r2148; Run at 06: 59 AM COT 'on Mon Jun 26. 1995 .. .' Abundance ~ 300000- o 200000- 100000- - o - - N N N II - .... . ..' ~¡. - -J~'lw.~.1~~¡"~LljlJ1'M~ ¡:':~'~I,~JJ.J.J,.,þI.,"¡ t~(~ 0- I I I I I I I 40 60 80 100 120 140 160 I 180 Tim e (m in'. ) Cl ~ n t:1 ~ ~ ~ ~ ~ o ;:¡. Z o N -J o - o N - N N N ~~, Abundance 20000- :.... 15000- 10000- In 5000 - r =I\; ~ o \ I 140 . Ion 231.20 amu from m29558601086.d 95r2148; Run at 06: 59 AM COT "on Man 0un 26. 1995 -... ~' ..; ~ ~ ,v~J )~~rl!J~~~~I~~ ~ ~ '\~~~ I 150 I 160 Time (min.) 5' I! . ~ GMC Data Report No. 270 103/222 ---------- ------~- 0.01 0.02 0.03 0.04 005 '-"J?age 2 of 3 Minutes 50---- . - w J II~i~t~~,,\'~~A~~~JJ~JA.JlivMM~.___ '-...¡ f.' ~; \.,~ ~ N ------- z:\gcwork\arcl ":·7.001 - Channel A 25 Þ--'- ~ § ~.wJJ.\~\' ¡¡Jiil" \A 'V~I.J ~ 1ft M ! i ~, 0.01. 0.02 0.03 G) ~ Q5 t:1 ~ ~ ~ ~ ~ o :4- Z o N -.] ~ ----- Sample 10:: '.", Sgc Acquired 1995 19:18:29 - ~ Ñ N N ,~. o ~ n tJ ~ ..... ~ ~ .g o ::¡ ~ N -....J o Abundance 25000 -. 20000 _. 15000 - 10000 =;~~ fir ~ ~ ~: ~ -, 5000 --. 0- 40 .'~ Ton 191 95r2176- .10 amu f . Run t rom m295 . a 0~08 PM COT o~1101011.d Thu Jun 29, ., f 50 I 60 I 70 'Time (min.) 1995 ~ I 80 f 90 C1 ~ () t1 ~ fJ ~ ~ o :4- Z ? tv -.I o - ~ - tv tv N .-. ,'~" Ion 191 95r2176' .10 amu f , Run t rom m2956 a 02: 08 PM 1101011 COT 0 n . d Thu Jun 29, At'urdar ce .. 20000 - =tt~~~ JAJ^' ..t\¡J~w~1 10000- 1"11" ~ '11'· 150UO- ~oou - ú- I 70 I 75 ì i we 1995 I BC 8') I 90 (win. I Q ~ () t.1 Š ~ ~ o ::\. Z o ----- /'----..,-. ------. Ion 217.20 amu from m29561101011.d 95r2176; Run at 02: 08 PM COT on Thu 0un 29. 1995 Ahundance ~ 80000- - o .......¡ - N N N 70000- 60000- 50000- 40000- 30000- 20000- 10000~~~~ 0- I 50 I 55 I 60 Tif11e (min.) I 65 I ,70 75 Q s:: () tj ~ ~ p:I :;d ~ a :::¡ Z o N -1 o Abundance 10000 -. 8000 - 6000 - 400a - 2000 - \~~~ ~~, Ion 217.20 amu from m29561101011.d 95r2175; . Run at 02: 08 PM COT on Thu 0un 29. 1995 ~-.. tjJ~j^,~\ ~\~~I'~~.N~ 0 I 1 I I I I I ~ 64 56 68 70 72 74 7G 0 00 - Time (rrif1.) tv tv tv Q ~ n Ö ~ ~ ~ ::0 ~ o :4- Z o N -J o - ~ - N N N !~'. ,.r----., . ---..... Ion 218.20 amu from m29561101011.d 95r2176; Run at 02: 08 PM COT on Thu Jun 29. 1995 Ahundance 5000 - 4000 - . , I MiA"Ll.IAII. II .\ ~i w.W ~I V 3000 -j II "VI 1/11"'" Y"~ V ',. " 2000 - 1000 - 0- 64 1 66 d~ $\ ~~ I 68 .~ ~ (t ~ Mr'ÞV . .' WV'\\ '\I 1 ~~~/ ~'if1fVtr ¡'I I 70 72 I I 74 I 76 Time (rrin.) 0- I I I I I I I I I J I I I J I I I I 1 J I I I - 64 66 68 70 72 74 76 - 0 - Time (m i Po . ) N N N 10 rJ fj - 2000 - 3000-' Ii ~w~'IJ ~ ~\fi,;, ~~/' V~\~N\J~t~V'^~J t~~~ " . . .' .. -LIh- j ~ 4000.=.-r \~ 500() - Ahurdarce G1 ~ () ö ~ t'"'t- ~ ~ ~ o ::+ z o N -I o Ion 259.20 amu from m29561101011.d 95r2176; Run at 02:08 PM COT on Thu 0un 29. 1995 ,~-- ,-----.,. Q ~ () t1 ~ - ~ ~ ~ o :4- Z o N -.J o - - - - N N N ,.r---- . .~--... TIC of m29558701087.d 9 5r 2 176; Ru n at 10: 18 AM COT 0 n Mo n 0U n 26, 1995 Abundance 400000-' { : 300000- .- .' . 200000- , 100000- ~~~~~.~.uA.~~,~~~~\ ~~.w..~, 1 o I 60 I 80 f r 100 120 I 40 Time (min.) ~.. \, '., .- I I I 140 160 180 Q ~ n t:1 ~ ~ ~ ~ o ::4. Z o N -..l o ~ ~ N - N N N ,..-- - Abundance 14000- 12000- 10000- 8000 - 6000 - 4000 - 2000 -= l -J'V\ o \ I 140 ------ Ion 231.20 amu from m29558701087.d 95r2176; Run at 10: 18 AM COT on Man Jun 26. 1995 ~ .~ ~i~~\!vy¡ M\ ,1 ¡!~ ~ II 150 Time (min.) I 160 GMC Data Report No. 270 113/222 ,0002 0004 0.006 '0.008 0.010 --,0.012 5õ ~~ V\\ \: -........!':. '- ....J) v\ 2b ~ -~'Page 2 of 3 J~ ¡\~ J 1 ~. Minutes - \i, ~ j \ ¡ : -~ z:\gCWork\arC('·r -':,7.001 - Channel A J i I j 2'5 t l2~~JJ~.WJllj4J~ {' I· I ,--------, ... Sgc 1995 02:08:49 0.004 0.006 0.008 Q ~ n tj ~ ~ ~ þd ~ o ~ O~ o N -..l o - Sample 10 O.012Acquired CJ s:: () t1 ~ ~ ~ ~ ~ o ~ ~ N -.1 o ~ ~ V- - N tv N ..---.... , /----., Ion 191 10 amu f 95r2189' R . , rom m29554801048.d -. . un at 05: 54 PM COT on Thu Jun 22. 1995 -, -¡.. , o ~~~~,_~,_j,.~J~-'Á~1l~~~,Atj4 "LA~)...-'~Y~ I r r II J r 50 60 Abundance 200000- 150000- 100000- 50000- ,I.. I 70 'Time (min.) ---, I 80 I 90 ,~" /- C) ~ n t:1 ~ S ~ ~ o ::\. Z o N -..l o Ion 191.10 amu from m29554801048.d 95r2189: Run at 05: 54 PM COT on Thu Jun 22. 1995 Abundance 200000- 150000- 100000- 50000 - =~D~-wJ~ JJ-J. ~~ JJ NwJ~,",,~-'~~ 0 I ~ I I ~ 70 I 0'\ 75 t:3 80 85 - I N 90 N Time (m in. ) ",r--, , ,---.... a ~ n t:1 ~ ~ :;d ~ o ~ Z o N ë3 40000- Ion 217.20 amu from m29554801048.d 95r2189; Run at 05: 54 PM COT on Thu Jun 22, 1995 Abundance 30000 - , , , , 20000- .' . i i --:: . 10000- f =~MjJ^, IA.¡J JvJJv.,,"J~~.wJMJJ 0- I I 60 65 I 55 I 70 I 50 ~ ~ -.1 - N N N Time (min.) ¡ ~\~~ I 75 ---- - o ~ n t:1 ~ ~ ~ ~ o :¡ ~ ~ 40000- o Abundance 30000 - 20000- 10000- ~--;,- i ~.""----- . " Ion 217.20 amu from m29554801048.d 95r21S9: Run at 05: 54 PM COT on Thu .Jun 22, 1995 =M JWIJ rJìA \JV ~ ' ~ ~ 00 - N N N o 64 I 66 [ V J \ \ ; I \ "\ I 68 I I 70 72 Time (min.) \v/t ~ \r~~ I 74 I 76 /"-" ,..-----..",.. Q ~ () t:1 ~ ~ ~ :;d ~ o ::4- Z o N ~ 40000- Ion 218.20 amu from m29554801048.d 95r2189: Run at 05: 54 PM COT on Thu Jun 22, 1995 Abundance 30000 - 20000- 10000-' \ f 1 ,^'V'f. '\ J\ \. ~ v' /V V ~ "'u ~.~ I =~JJ0vJ}l\ J~ ~ ~ \D - N N N o 64 I 66 I 68 I I 70 72 I 74 I 76 Time (min.) '~-" o ~ n t:1 ~ S ~ ~ o ::¡ Z o N -..l o Abundance 20000- 15000 - 10000- 5000 =^\N\J J ~ ~ ~ , Ion 259.20 amu from m29554801048.d 95r2189: Run at 05: 54 PM COT on Thu 0un 22. 1995 ., lJ )IN\ AJA'J' J ~I' 'AA ~))uJ~'~ ~~ 0 I I I ' I I I I ~ 64 66 68 70 72 74 76 N 0 - Time (m in. ) N N, N - N - ~ tv tv C1 ~ n t:; þ.) .-t- þ.) >:1 ~ o ;:¡, ~ N -...J o ,~. '---.. Abundance 95 TIC of r2189; , Run m295588010 at 01: 37 PM 88.d COT on M on Jun 26, 1995 100000- 80000- 60000- 40000- \, I :' . . .;..., [ I .. <. 20000- - - . -' ' ,~ , -- '1 ,.~:.. " ',~~ J' o - "/I!.,, ""'" " -fl.....! ~. "01 .A~" W I' 1JAI ~tf ' J~' W,( ,~~ 40 80 100 Time (min.) 120 140 160 180 o s;:: n t:J ~ ~ ~ ~ o :4. Z o N -..l o ~ N N - N N N .'~'" ........~'.. ....--.,., Ion 231.20 amu from m29558801088.d 95r2189; Run at 01: 37 PM COT on Mon Jun 26. 1995 Abundance 12000 - 10000"- 8000 - 6000 - 4000 - 2000 =A\J ~ I ~ ~~ H ~ ~ ~ o I 140 I 150 Time (min.) i Å J WJvJl~. ~V1 ~~ I 160 z . GMC Data Report No. 270 123/222 ~ ~' ~ ~' Ñ t-, ~ è,Q4 ~ ~. Sample ID ; \ ., Sgc AcqU~~'_ 995 20:44:30 C ¡,05 ( t ~ E, ~ (I, ~\ C Þ- .. ' ./...r--~-_._ z:\gcwork\ar ' -Il,001 - Channel A J?age 2 of 3 ---- --~------ 0,05 0,04 --0 V\ ::0 )-.J '-- ~. 0,03 I 0,03 Nt' ---t.~ ~t ~ t- rv 0,02 0,01, . ¡ . .1 ¡ ,I. \.¡ I þ~~ ~LJ¡11J.~ II) "¡.II #' . , ' . ' ' J/~II'J ~'IA t\ ~ \L\~~^~~~J.~iJVUN\AJIlwJk~~~~~~ 2's Minutes -- - ---5õ--- -- -,- ,- 0,02 0,01 ---'-------- -~ C) ~ (j tj ~ ..... þ,) ~ ~ o ;:¡ ~ N -..J o ,,,"---~ ,. Ion 191 ' 95r2192' R .10 amu from m29 . un at 03: 56 PM COT 561201012,d on Thu Jun 29. Abunciance 3000f,) - 1995 . ~ h~~ 10000 :~Vt fW¡~~Mt~~W1ft"'Å~ ~'^J\11rJ ~\ 20000- o I 5J ~ N v- -- tv N N I 60 I 70 rime (min.) I ELl ..... N ~ N N tv ..-- Q ~ t:1 ~ ...,.. ~ ~ {î o :::¡ ~ N ~ Ion 19 95r2192- 1.10 a . . Run at mu from ' 03: 56 m29561 PM CDT 201012 on T . d hu J Un 29, 1995 Ahund <lance 30000- 20000 - 1000,)~~J~w)k~/j o .. ~~ j)/~j~J~) 75 80 7ime (min.) 8!:i G) a:: n tJ ~ S ~ (1) '"0 o ::¡ Z o N -.1 o ~ N -l - N N N ,,r---., Ahu£ìdance 60000- 50000- 400r)fj- 30000- é.OOOO - 1000f) - =~~, o I 50 Ion 217.20 amu from m29561201012.d 95r2192: Run at 03:56 PM COT on Thu Jun 29, 1995 ~~)JÂtJvì~~~ I 55 I I 60 65 I 75 I 70 Time (min.) C) ~ n tj ~ ~ ~ ~ ~ o :4 Z o N -.1 o ....... tv 00 - N tv tv .---' , ' 95r219:.onR 217't20 amu from m29561201012.d J un a 03: 56 PM COT on Thu ,Jun 29, 1995 Abundance 1GOOO- 14000- 1201.JO - 10000- 800') -, 6000~~ JH·V M 4000- 2000 -, (j 64 I 6,- o r f\ I 68 \\, ~ ~\'~J/\~v III I 70 Time (mil'.) I 72 J ~ I 74 I 76 ---- Q ~ n Ö Š ~ CD '"0 o :4- Z o tv -..l o Ion 218.20 amu from m29561201012.d 95r2192: Run at 03:56 PM COT on Thu 0un 29, 1995 Abundurtce ~()Of)-' 8000 - 7000 - 6000 - 5000 -= I 4000 ; ) ' .\~ ~ ~ ' 'J 3000~~ V~ JJ 200') - 1'JOO -= ~ N "-0 - N tv N 0- 64 I 66 I 68 ~ A. ' 1 ~. V' , I ' I I 70 72 Tirre (min.) ! ~ \ I) t ~ ~'iV A~ ~ I 74 I 75 ,,----. , ,.---., c;} ~ n tj ~ ~ :;d ~ o ~ Z o N -..l o Ion 259.20 amu from m29561201012.d 95r2192: Run at 03: 56 PM COT on Thu Jun 29, 1995 Abunci0nce 10000- 8 0 0 I') .-;- = ¡/J ^If\ .tI! N \J 400')- A'I~ R . ! ~ '\ ~ rA ~!. .\J\Jij\V~Vv1~~ 6000 - 2000- 0- I I I I I I ~ 54 Elf) 68 ' 70 72 74 76 w 0 - Time (win.) N N N C) ~ (j t1 ~ ~ þd .g o ::¡ Z o N -..l o ~ W ~ - N N N /----...... Abundance 300000- 200000- 100000- 95r2192: ~~-----... TIC of m29558901089.d Run at 05: 09 PM COT on Mon Jun 26, r 1995 = ~~j JJI~ì I~ ~~~ (~J'~.JJ ~ ~,~ .l W"4~~~J·""~W- o J I 40 I 60 I 80 I 100 I 120 Tiwe (m in. ) I 140 I 160 I 180 ,,....--' , G) ~ n t:1 ~ ~ ~ ~ ~ o ::¡ Z o Abundance ~ 12000- 10000- 8000 - 6000 - 4000 - 2000 - ' -I ~ o ~ w N - N N N I 140 Ion 231.20 amu from m29558901089.d 95r2192; Run at 05: 09 PM COT on Mon Jun 26, 1995 ~ '~~;\,~hJill~ h}\ ~J~~~ 1~~ I 150 I 160 Ii me (m in. ) ~' II "t]J s:u '< GMC Data Report No. 270 133/222 0,002 -------- 0,004 0,006 ,0,008 0,010 ,0,012 ,0,014 0,016 0,018 0,020 0,022 0,032 --0 \J>. )J ,0,030 >-v N 0,028 0 CJ\ì 0.026 0,024 0,034 ,0,036 '. Page 2 of 3 Minutes ,I L ~ I ..I I ~. I II ,1\,\1 J~ '.¡I \\'~ ..~~ JV,,~\'\!J\lA~~Wu~I' ,II j L.,.....J).).lU,J....MIII. .J..wl ,J \JIJ' }j . Vi 1.\ ,Nij M Þ/\ % Þ'IÀ.!. . ... . \~~ 25 ~ 50----' ~ z:\gcwork\arc-' , "001 - Channel A <;gc 195 02:28:21 ,/- Oµll4, V) ~ - N oþg2 0,006 0,008 0,010 0,012, 0,014 0,016 0,018, 0,020 0,022 0,024 0,026, 0,036 C) ~ o,Q tJ ~ ~ o.r~ ~ o o,6!o, z o O,~ o Sample ID Acquired C> ~ n t:j ~ ~ ~ ~ o ::\. ~ N -..l o ....... W U¡ - N N tv ~---. ~ ...-!"--.....- Ion 191 95r220S- .10 amu f . Run t rom m2955 a 04>43 AM CDT 5401054.d on Fri 0 un 23, 1995 Abundance 250000- 200000- 150000- 100000- 50000 - J- o . , ' . ; , ~~,"'JMJA!Û Jk \ \ ~.I ~"k"J!Àv-''µ~ I 60 I I I I I 70 Time (m in. ) I SO I 90 CJ ~ () tJ ~ .-t- ~ ~ ~ o :4 Z o tv -..l o 95r220~onR191.10 amu from m29555401054.d . ,un at 04: 43 AM COT on Fr i Jun23, 1995 Abundance 250000- 200000- 150000- 100000- 50000- I I - 70 I 'I w 75 0'\ I - 80 I N 85 N N Time 90 (m in. ) =~<\AJJJl.-A~ J~ VÑWJJ"JvvJ~-A.)W.J-~~ 0- C} ~ () tj ~ ~ ~ ~ o ::\. ~ N -..l o ~ W --1 - tv N N r--'" Ion 217.20 amu from m29555401054.d 95r2208; Run at 04:43 AM COT on Fr i tJun 23, 1995 Abundance 50000- 40000- 30000- 20000- 10000 -= I - . II IA I I~ .! IIL W A '" - ~ J,}.]I) .....' ¡ },.IM '^' JVW I.~ \ vJ .AJ.tv It.'; y~ J ¡l.Jù.W I\..¡' 'VI~ o I 55 I I 60 65 I 50 Time (min.) ~ \ J I ~ \ ~~~ I 70 I 75 Q 3:: n tj Š ~ ~ o ::4- Z o t-.) -..l o ~ lÞ.) 00 - N t-.) t-.) ,---- , ".r--., Ion 217.20 amu from m29555401054.d 95r2208; Run at 04: :43 AM COT on Fr i Jun 23, 1995 Abunc1c:¡nce 50000- 40000- 30000- 20000- 10000- =Aw) fVVIv J Iw \) J\ 0- 64 I 66 " \' \ 68 ^ ) ( VI ~ I I I 70 72 Time (min.) I ! . \/1 V ~ \Jrw~ I 74 I 76 ~." G1 s:: (j tJ ~ ~ ~ .g o ::¡ ~ - ~ Ion 218.20 amu from m29555401054.d 95r2208: Run at 04: 43 AM COT on Fr i Jun 23, 1995 Abundance N -.J o 40000- 30000- 20000- 10000- =~vJVv~J \ < JI \ ìYì , \¡IvJ f \ I \\!,J\! ^"^ \v J~ 0- I I I I I I I I--'- 64 66 68 70 72 74 76 w \0 - Time (m in. ) N N N .----.' ,~, Q ~ () tJ ~ r-t- ~ ~ ~ o ~ Z o N -.1 o Ion 259.20 amu from m29555401054.d 95r2208: Run at 04: '43 AM COT on Fr i Jun 23, 1995 Abundance 30000- 20000- - =j\'W\~ A ) 1V J ~ , \ \ ,I \ I AJ V! V^ ~I \,yvvA¡JJ~~Avk~ 10000 - 0- I I I I I I I--' 64 66 68 70 72 74 76 ~ - Time (m in. ) N tv tv - .¡:. - t::3 N N ----- '. Q ~ t1 ~ ...... ~ J;d ~ o ~ ~ N ~ o Abundance 180000- 95 TIC of m2955 r2208; Run at 09:,...37 9401094. d AM COT on Tue Jun 27, 1995 i - I. ' l' · J,1/4 20000::' I tJIII'r< ' o =~J.t~~.j.LL."tdþ,~t ;'J;M~~~:,,~,J ^4~~' - 160000- -, 140000- :120000- - 100000- - 80000 - - 60000 - - 40000- 60 80 .100 Time (min.) 120 . 180 /"--., -------. Q ~ n Ö ~ ~ ~ ~ o ~ Z o Ion 231.20 'amu from m29559401094.d 95r2208: Run at 09: 37 AM COT on Tue Jun 27, 1995 Abundance !j 30000- o 20000- 10000- -~,'fj ~ \fJ / II tvlWiý' ~~ ~ \fA. J \ ~ ,~N~'vv' 0 I I I ~ 140 150 ~ N - N Time (m in. ) N N I 160 -f =: æ.. c: ;I\' ; I I i I I i ; I I GMC Data Report No. 270 143/222 Sample ID . :---, Acquired Sgc . ' 995 03:54:18 0,038 o ~ O.Q t:1 ~ ~ O'9èf' ~ o 0,Q12 Z o O,~ -..l o 0,028 0,026 0,024 0,022, 0,020. 0,018 0,016 0,014, 0,012 0,010 0,008 0,006 (}:Ø04 t - N ~2 ~ ,.... '....'" " 1, ~~~JI!.-JLJ· Z:\gcwork~CC"-----"""'':\ " .001 - Channel A ~ ~\~~ ,~JvlAk~JÀJJdk}JlM lM\~k,~Jl~ is '50--"-" Minutes .. '0 age 2 of 3 ---û V\ "- _U }J ¡\.) o ~ 0,038 0036 ,0,034 ,0,032 0.030 0,028 0,026 0,024 0,022 , .0,020 0,018 0,016 0,014 .0,012 0,010 ,0,008 0,006 ,0,004 - 0.002 ~, Q ~ () tJ ~ ~ ~ (t) '"0 o ~ Z o Abundance !:j 250000- o 200000- 150000- 100000- 50000- o - .þ. v- - N N N .-".,.----~ - , : ~'J Ion 191.10 amu from m29555501055.d 95r2209; Run at 06:31 AM COT on Fr i Jun 23, 1995 I 50 " . ~ " " k.. 'J...J¡ .;'4\ U!,.."N.,.J.,.",JANv ---'--~ ~\Jf\+"JM'.wW.lt I ï I I I 60 70 80 90 Time (min.) I 90 ~~"",,~~vwA J./iwh. "J^~)JAv~~c.-~,j 0- I 85 I 80 'Time (min.) I 75 Ion 191.10 amu from m29555501055.d 95r2209; Run at 06:'31 AM COT on Fr i Jun 23, 1995 I 70 50000 - 100000- 150000- 200000- 250000- Abundance ~. ~ ð\ - N N N C) ~ () t:1 ~ ~ ~ ~ o ~ Z o N -..l o C) ~ () tJ ~ ~ ~ ~ o ~ Z o tv -1 o ~ .þ. -1 - N N N /---. Ion 217.20 amu from m29555501055 d 95r2209: Run at 06: 31 AM COT . . on Fr l Jun 23, 1995 Abundance 40000-- 30000- 20000- 10000- I j ~J~",v0 "",,~J~JPwJJWJ~rM^.. \ \ 0- I 60 I 65 I 50 I 55 Time (min.) I 70 f ~v~~ I I 75 C) ~ n tJ ~ ~ ~ (t) ~ o ~ Z o N -..l o 40000- Abundance 30000- 20000- Ion 217.20 amu from m29555501055.d 95r2209; Run at 06: 31 AM COT on Fr i Jun 23, 1995 10000 ~ J# v\~.. ,\ \ .jl¡\, ,'\vhJ ~\¡ ~ .þ. 00 - N N N 0---, 64 I 66 I 68 I I 70 72 I 74 Time (min.) I 76 .r/--' Q ~ n tj Š ~ .g o ::\. Z o N -J o Abundance 40000- 30000- 20000- Ion 218.20 amu from m29555501055.d 95r2209; Run at 06: 31 AM COT on Fri Jun 23 1995 10000-::: ( j =~~~hJJ¡,(J\~ lJ\ j\~~' ( ~ f '~V'¡J~'0~~ 0- I I I I I ' I I ~ 64 66 68 70 72 74 76 ~ \0 - N Time (m in. ) N N, .r-- C) ~ () ö ~ þ) ~ ~ o :4- Z o N ~ 25000- Abundance 20000- 15000 - 10000 - 5000 - I = JIÂJv . -Á JYw ~ v- o - N N N o 64 I 66 Ion 259.20 amu from m29555501055.d 95r2209: Run at 06:31 AM COT on Fri Jun 23, 1995 J )"'~J A \~ 'Ir~'v ~ \ \~Mfv)JWì# J\JV AJ~~ ~"^ I 68 I I 70 72 I 74 I 76 Time (min.) ./~---- Q ~ n t:1 ~ ~ ~ ~ o :¡ Z ? N -..l o 95r2209; TIC 0 f m2955 . Run at 12: 56 P 9501095.d M COT on Tue Jun 27, Abundance 90000 -= 80000 -= 70000 -= 60000 -= 50000-= 40000 ::... 30000-=' ~ v- ~ - N N N 20000 -= o = v..,.~,...."',_.L~llJ...,.~, ~..Á1...~ÀI- ~þ .' Û¡J I I 40 I 60 I 80 I 100 I 120 Time (m in. ) 1995 I 140 I I 160 I 180 Q ~ n t:1 ~ ~ ~ (t) Þ-O o ~ Z o Ion 231.20 amu from m29559501095 d 95r2209; Run at 12: 56 PM COT . on Tue Jun 27, 1995 Abundance !:j 25000- C> ~ lit N - N N N 20000- 15000 - 10000- 5000 - =V\..J/ P ~ \t /1f ~ ~ o I 140 ~ . I \ ' w\Jr~,~þ~ I 150 I 160 rime (min.) "\, ,:E o ::;: C") ""I: CD CD "" GMC Data Report No, 270 153/222 Sample 10 .--- lJ~r~~ n o,i4 ~ ~ ~ 04]2 o :4 o,~ N -..l o,Q 0,026 0,024 0,022 0,020 ,0,018 0,016 0,014 0,012, 0,010 0,008 0,006 (µX)4 U\ ~ - N 4fþ2, --' ·"...sgc . 995 08:11:59 z:\gcwork\arCi'" -------- ". "UJ01 - Chamel A ~ ~ ~ Jl ~~~jl~~J.~ JA ~ ~¡i~~.U, .\tN\JJ\~.rJ..~ _J . ~~ . 2~ .'y"'--Ll~ ------1L _ so' Minutes ?age 2 of 3 _0 \i'\ .Ji N N }0 () ~ _J'- 0,036 0,034 0,032 0,030 0,028 0,026 0,024 0,022 ,0,020 0,018 0,016 0,014 0,012 0,010 0,008 0,006 0004 0,002 Q ~ (') tj þ) ...... ~ ~ ~ o ::t. Z o tv -1 o - u. u. - tv tv tv Abundance 100000- 80000- 60000- 40000- 20000- o Ion 191.10 amu from m29556701067.d 95r2220; Run at 04: 12 AM COT on Sat Jun 24. 1995 ~~ I 50 I 60 Time (min.) »~ ~J JJ...;Ju )\. \ \ V" p, ~. J.t.. I 70 . I 80 I 90 I 90 I 85 I 80 Time (min.) I 75 I 70 0- 20000 - =~~J\~ ,if-\M. 'VA ~j)~~J.v."'~ 1995 Ion 191.10 amu from m29556701067.d 95r2220; Run at 04: 12 AM COT on Sat Jun 24, -_""""-0.- 40000- 60000- 80000- 100000- Abundance . - - U. 0'\ - tv tv tv o a=: () t1 ~ ...... ~ ~ ~ o ::t. Z o tv -1 o o ~ () t1 ~ ~ :;d ~ o ::t. ~ tv -1 o - U. -1 - tv tv N . ,r--- Ion 217 20 amu f 95r2220' R' rom m2955670 1067 . d , . un at 04: 12 AM COT on Sat Jun 24, 1995 Abundance 60000- 50000- 40000- 30000- 20000- 10000- I ' ~~~~~~~~MtAo\l~\~J jJ '\,t)~~~ o J 50 I 55 I 60 I 65 I 70 I 75 Time (min.) Q ~ () tj ~ ...... ~ :;d (tI "'Ö o ::t. Z o N -1 o - u. 00 - N N N Abundance 30000-- 20000- Ion 217.20 amu from m29556701067.d 95r2220; Run at 04: 12 AM COT on Sat Jun 24, 1995 1 V \. 10000 =4"1A/l,¡ ~ J... '^ I . '\ 0- 64 I 66 I 68 .. r'\J \ \ }. I I 70 72 Time (min.) ( / '\ J! \ ~Vy~ I 74 I 76 I· ..--. C) s: (') tj š ~ ~ o ::t. Z o N ð 30000- Ion 218.20 amu from m29556701057.d 95r2220; Run at 04:12AM COT on Sat Jun 24, 1995 Abundance 20000 - 10000- -~ tJ0IJv} - U. \0 - N tv N o 64 I 56 ( \ ~ '\ ~ \ I 68 ~ V\' ~ \J ~ ~ t \ '\~,J~Vv~~ I I 70 72 I 74 Time (min.) I 76 I. o a:: (') t:1 ~ þ) ~ ~ o ::t. Z ~ tv -1 o Ion 259.20 amu from m29556701067.d 95r2220; Run at 04:12 AM COT on Sat Jun 24, 1995 Abundance 2000') - - 1500') - 10000- 'l/ - J W¡fÁj 5000 ~~ ~ ~~ ~! ¡ ~ I \r rf \ r\Jl~~~~~ 0 I I I I I I - 64 66 68 70 72 74 7Cl ~ - Time (m in. ) tv N N G ~ () t1 ~ ~ ~ ~ o ::t. Z ? tv -1 o - 0'\ - - tv tv tv Abundance 100000-= 90000 -= BOOOO-=' 70000 -= 60000-= 50000-=' 40000 -= 30000 .=. 95r2220; TIC of m295 Run at 0~34 p59701097.d M COT on Tue Jun 27, 1000:~,_c.uc~"_..h~~~~r~ Ji m~W' I I 40 20000 -= I 60 I 80 I 100 Time (m in. ) I 120 1995 I 140 .~ I 160 I 180 C) s=: () tj þ) ...... ~ ~ (tI "'Ö o ::t. Z o tv -1 o Ion 231 20 amu f 95r2220' R' rom m29559701097 d , . un at 07:34 PM COT . on Tue Jun 27, 1995 Abundance 14000- 12000- - 10000- 8000 - 6000 - 4000 - 2000 ~~II' t \,'" ¡PÅ f~INvJfw'J~~'W~' \~~~~(~;~~~~ 0- I 140 I 150 . I I 160 - 0'\ N - N tv tv rime (min.) Ii GMC Data,Report No. 270 163/222 Sample 10 Acquired 0.020 - Q ~ () t1 o.m-a ~ ~ o ::t. Z 0.~6 tv -1 o 0,014 0.012. . 0.010 0.008 0.006 0.004 - ~ - N ~2. - ...---- . .. Sgc 395 22:10:33 .. ~ I I ¥' ~ JjW) _L-J~~llr . 2'5 z:\gcwork\arco··-----~· -."'\ 001 Ch , . - BMeI A l ~ ) l 'r ¡ Minutes tJ ¡ I., \ \ ,\~ II, !i¡\ ~ i~, ~ ~ ~ \ \ -so---~. Page 2 of 3 -·0.020 0018 ---0 v--. '- 0.016 -'--' }V tv tv LN 0.014 0.012 0.010 0.008 0.006 .0.004 0.002 Q s: n tj ~ ~ :;d ~ o ::t. r: tv -1 o ....... 0'\ U. - N N N Abundance 40000- 30000- 20000- .......-"-.... Ion 191 95r2223' .10 amu f . Run t rom m295 . a 12: 20 PM COT on61001010,d Thu Jun 29, 1995 ¡ =~~w~~M~~~~'.~~¡~ .~~ ¡)II 10000- o I 50 I 60 I 70 I Time (m in. ) .Á~~'úl \\~}'}~~ I 80 I 90 Q ~ () t1 þ) ..... ~ ~ (t) "0 o ::t. Z ? N -1 o - ~ - N tv tv ..~...~ Abund ance 40000- 30000- . . Ion 191 95r2223' .10 amu f . Run t rom m295 a 12: 20 PM COT 61001010,d on Thu Jun 29, 1995 10000~~J~ ~w4VJ~JwVV\ j¡-JM \}N'vIJ\ \ I'~.NU~ '4Þ~ 20000- o I 70 I 75 I 80 (m in. ) Time ~ I 85 I 90 '~.". Q ~ n t1 þ) ...... þ) ~ (tI "'Ö o ::t. Z o Ion 217.20 amu from m29561001010.d 95r2223; Run at 12: 20 PM COT on Thu Jun 29, 1995 Abundance !:j 40000- o 30000- 20000 -. 10000 ~ =~J~J ~,~~~~~I~\' r)v~~v ~~ 0 I I I" I I I I - 50 55 60 65 70 75 0'\ -1 - Time (m in. ) tv tv tv ~. Q ~ (') t1 ~ þ) :;0 (tI "'Ö o ~ Z o N -1 o ------ Ion 217.20 amu from m29561001010.d 95r2223; Run at 12: 20 PM COT on Thu Jun 29, 1995 Abundance 18000- 16000 -. 14000 - 12000- 10000 - 8000 - 6000 ~VWv ~ ~ ~ 4000 - 2000- ~ I ,1~ \ ! ~ ~ \ J f/ I, \ J/'v ~ ~~. ' \- 'W ~~ to 0- I I I . I I I I - 64 66 68 70 72 74 76 0'\ 00 - Tirre (m in. ) N tv tv .~"'. .---....... C1 ~ () t1 ~ þ) ~ (tI "'Ö o ::t. Z o Ion 218.20 amu from m29561001010.d 95r2223; Run at 12: 20 PM COT on Thu Jun 29, 1995 Abunciance !j 12000- o 10000- 8000 - 6000- 4000 - ~ ..i'ì.' ^ =~# '1\V ~ ~ ~ \1 I~. ^ .' ~ ¡'\II ' ~ J'~ J ~ \ .~~ 2000 - - 0'\ \0 - N tv N 0- 6-1 I 66 I 68 I I 70 72 I 74 I 76 Time (min.) .,,--- ~- C} ~ () t1 þ) ...... ~ ~ (tI "'Ö o ::t. Z o tv -1 o Ion 259.20 amu from m29561001010.d 95r2223; Run at 12: 20 PM COT on Thu Jun 29, 1995 Abundance 10000 -, 8000- 6000- 4000 ~Jw^ ~ ïN ¡\l' ¡V\ J^ '\¡ ~ \/w ~ 2000 - ¥ ~ o -- I I I I I I - 64 66 68 70 72 74 76 -1 0 - Time (m in. ) N tv N C) ~ () t:1 þ) ...... ~ ~ ~ o ::¡ t N --1 o ..- -1 ..- - N N N 20000 ~ :""~ ~"JJ'~VH.~~~~~.J..~_~~MLJlM)~t~ ~~I~ ~ ~I~~' ~I~I o - ---- 95r2223" R , un TIC ¡ of: m29559 at 10· 5' 3 B01098.d . ,. PM C , OT on T ue 0un 27, Abundance 100000- 80000- 60000- 40000- I 40 I 60 I 80 I 100 I 120 Time (min.) 1995 I 140 I 160 I 180 ,----. C) ~ () tj þ) ...... þ) ~ ~ o ::t. Z o Abundance !i 7000- o 6000 - 5000- 4000 - 3000 - 2000 - - 1000.:) ~, ' o - -1 N - tv tv N to- Ion 231.20 amu 95r2223; Run at 10:53 from m29559801098 , d PM COT on Tue Jun 27. 1995 ". !' ~ I V J 140 ~'/'~~/' I t'~ ,W+,~~~ldWr ~.~~ 1~'~lr~ I 150 I 160 rime (min.) Ii '\. .,..-. GMC Data ,Report No. 270 173/222 Sample 10 Acquired ."----- . Sgc 395 09:37:49 o.~. () t1 ~ O.~ ~ o ::¡ 0.á1 tv -1 o 0.018 0.016. 0.014. . 0.012. 0.010 0.008 ..----- z:\gcwork\arcr' .~, 7.001 - Channel A l 1.3 ,.~ I j¡ \'~' ~ Jtl .~IU~ o~~J¡¡\) lt~\ 1 "" ·VV~,.",'-J J'WlJlJhvJJd. 0.006 0.004 2'5 Minutes . \) ~ I i ·-~!)age 2 of 3 - 0024 0022 -0 1..1"1 ~ ]v N ~ \1 0.020 0.018 0.016 0.014 0.012 0.010 0.008 II: I 1\ 0.006 .~~ ~~ . ~~~~,- 0.004 0002 -~5õ o ~ () tJ ~ S ìd ~ o ::t. Z o N -1 o - -1 U. - tv tv tv ----. ,-----... Ion 191.10 amu from m29556101061.d 95r2227: Run at 05:' 22 PM COT on Fr i Jun 23, 1995. Abundance 400000- 300000- 200000- 100000- o ... _,H ~~.....L~...N.-.~vM..''''\\r}vM ,JA,tIo,J """J"v~"'~ r I I I I I I I I I I I I I I I I I I I I I I I I 50 60 70 80 90 Time (min.) -~-.. ""......-.......- ',\ .---., Q ~ (') t:1 $:\) ~ $:\) þd ~ o ~ Z o N -1 o Ion 191.10 amu from m29556101061.d 95r2227: Run at 05:: 22 PM COT on Fr i Jun 23, 1995 , Abundance 400000- 300000- 200000- 100000- ~J~",^wv-J~~# ~ ,,), JvJ. JI-vJ L ~rw.J~"" 0 I I . I I I I - 70 75 80 85 90 -1 0'\ - ·Time (m in. ) tv tv tv c¡) ~ () tj ~ ~ ~ ~ o ::t. Z o tv -1 o - -1 -1 - N tv N ...--. ./--\ Ion 217.20 amu from m29556101061.d 95r2227; Run at 05:22 PM COT on Fr i Jun 23, 1995 Abundance 250000- 200000- 150000- 100000- 50000- - : \ =~~.~~J)lU)NII>.' f o 1 I 1 I 1 1 I 1 1 1 1 I 1 I I I I 1 I 50 55 60 65 Time (min.) t ~ J J I 70 í ,!~ ~ V ~~ I I I. 75 ~--- .....--...... C) ~ (') t1 ~ þ) ~ (tI "'Ö o ::t. Z o N -J o 250000- Ion 217.20 amu from m29556101061.d 95r2227: Run at 05: '22 PM COT on Fr i Jun 23, 1995 Abundance 20000.0- 150000- 100000- =~ A l1 ~ j ~ tq ^ ^' vl·V M, ~~ 50000- \ ~ - -1 00 - tv tv N 0- 64 I 66 I 68 I I 70 72 I 74 I 76 Time (min.) '- a ~ () t1 ~ þ) ~ (tI "'Ö o ::+ z o N -1 o - -1 \0 - tv N tv ~ Abundance 180000- 160000- 140000- 120000- 100000- 80000- 60000- 40000- 20000 -= J -~t o 64 - ". - ~. .'~-.. Ion 218.20 amu from m29556101061.d 95r 2227: Run at 05: 22 PM COT on Fr i 0un 23, 1995 /I. WfI L ¡J' , I 66 ~ \ ^ ~I\¡ I 68 I: i I I 70 72 Time (min.) ,\(11 ~~J~ I 74 I 76 ,~-- C1 ~ (') tj ~ þ) ~ ~ o ::t. Z o tv ð 100000- -..---.... ..-:. ----..... Ion 259.20 amu from m29556101061.d 95r2227; Run at 05: ;22 PM COT on Fr i 0un 23. 1995 Abundance 80000- 60000- 40000- J , , ~ ~;Jvv, -J~ ~ ;' 20000- }W If ~ ~ \ I (! ¡ \l' AA' , 11\j~,~ Þ/J~ 0 I I I I I I I 1 - 64 66 68 70 72 74 76 00 0 - Time (m in. ) tv tv N Q ~ () t:1 þ) ...... Po) ~ ~ o ::t. ~ ~- ---- 95r22 TIC of.m29 . 27- R 5599 . un at 02: ;12 AM 01099. d cor on Wed Jun 28, 1995 Abundance tv -...¡ o 300000- 200000- 100000~ o ~ 00 - - N N N ... .J ~. .. I II I , "A~' ,. ~" -.J..IUI"" JlJ~". ' I~; L, .J' , . #'~;~ ' ' I I I I I _~,.¡.w.L~~¡]~AI#Î' I I .~ "~ W"'~ 40 I I I .w~", 1- \- 6 I I ~,~ o J I ,- 80 I ~OO _1 1 I 120 I 140 1 I 160 I 180 Time (min.) /" ----- '. Q ~ () t) ~ þ) ~ ~ 0 ::t. Abundance Z ? tv 200000- -1 0 180000- - 160000- 140000- - 120000- 100000- - 80000- 60000- - 40000- - 20000 - - 0 I ..- 140 00 N - N tv N /~" Ion 231.20 amu from m29559901099.d 95r2227: Run at 02: 12 AM COT on Wed Jun 28, 1995 ~ 1 1 ~~~~~~- I 160 I 150 Time (min.) 10 .e. ... Õ ::s .~-_. ,,~. '''- "." ...-, .. ..~ "... '''''' ,,_.." " GMC Data.Report No. 270 183/222 ~U__._ ___~ 0.002 -~~~- 0.004 0.006 ---- -.-.-.- .-- ---- 50 \ ~ . '.\~\¡M . ~i~ .\ Minutes , 1 ~ 0.010 r, 0.008 .0.012 0.014 ·10 }" ~ CÇ) )s \J\ .0.016 -... ...... -0...1 0.018 ------- ~·Page 2 of 3 ----- --- z:\gcwofk\arCl ., '< 'H)(}1 - Channel A 25 r .1. JJ ~...ßJ ,,¡)I 1 r---. Sample 10 :: . . . . Sgc Acquired: 995 11 :03:40 - 00 ~ - ct-002 tv N 0.004 0.006 0.008 0.010 0.012 tv O.~ C1 ~ (j t:J ~ ~ O·ØUì (tI "'Ö o ::t. ~ 0.018 --- C1 a:: () tj ~ Po' ~ (tI "'Ö o ::\. Z o ---" .'- :~-. , .. ..-; /'----:..... Ion 191.10 amu 95r222B; Run at 07: from m29556201062 d 11 PM COT on Fr i Jun '23, Abundance' ~ 160000- - 00 u. - N N N =~~~-...JvA-...J~~~.. '. ".1,1,1,.1 II ",¡J~Jwt.../.NfV""~ o I ' J.,J.I.,., ~.......I. ,."", 'I/#~' wJJM! JIt.J\ .I..,¡\J I II\,. I 1 1 I 1 I 1 ;' 50 t 60 140000- 120000- 100000- 80000- 60000- 40000- 20000- 1995 ~: I 70 I 80 I 90 Time (min.) ./----......... Q ~ n tJ Ø) - Ø) ~ ~ o :4- ~ tv ........¡ o Ion 191.10 amu 95r2228; Run at 07: i1 from m29556201062 d PM COT on Fr i 0un . 23, 1995 Abundance 160000- 140000- ", 120000- 100000- 80000- 60000- 40000- 20000- -= ~ '- --"- Lv ^'Jv-J ~ A J ~ )J,. '^^ ~ ~ "^ 1 J Nw ~ ~ ~..)\Mtv --- AVV'''N'''~ ~ 0- - I 00 70 I ~ I I - 75 tv I tv 80 tv I 85 Time (m in. ) 90 c.- ~> r t, Øo) .... ~ ~ (t) "0 o ::¡ Abundance 2 o t...: 2 40000- Ion 217.20 amu from m29556201062.d 95r2228; Run at 07: 11 PM COT on Fr i 0un 23, 1995 30000- 20000- J . I I = ~..JN-JV 'to' f\~ l>vJtJ l-W, ~.).~ ~w'-v\\1 \ ~ ~ ~ I \ \ 10000 - 0 I I I I I " I 50 55 60 65 70 - 00 -.....I (m in. ) - Time N N N ¡ ,/ ~~~~ I 75 ~-. Q ~ (") t:1 ~ ~ ~ ~ o :4- Z o tv ~ 40000- .-." Ion 217.20 amu from m29556201062.d 95r2228; Run at 07: 11 PM COT on Fr i 0un 23, 1995 Abundance 30000-- 20000- 10000 - = ~ w l1f\l\. J\P\ ìJv ~ - 00 00 - tv tv tv 0- 6.4 I 66 I 68 \ \ f . I ! ( l ,j J v\ I I 70 72 Time (min.) \/\ ~~ I 74 Q æ:: (") t:J ~ Ø) ~ ~ o ;:¡ Z o tv ........¡ o - 00 \0 - tv tv tv /----._-- ? . Ion 218.20 amu. from m29556201062.d 95r2228; Run at 07: 11 PM COT on Fr i 0un 23, 1995 Abundance 30000- 20000- 10000 - - .' ( =~J0/V\1)J\\f ~. (j 6.4 I 66 I . 68 f V\ 0J·¡ I I 70 72 Time (min.) ^ \)'v ~~1 I 74 ----'. Q &:: ("') tJ ~ Ø) ~ (t) "0 o ~ Z o N ........¡ o 25000- Ion 259.20 amu from m29556201062.d 95r2228; Run at 07: 11 PM COT on Fr i 0un 23, 1995 Ahunc-Jance 20000.- 15000- 10000- 5000 =rÀ.tv.À ~ ~) ~' ^' .~ ~ r vA'\',V, ~J WlJ,,~1 tJ'v~ o C4 I 66 I 68 I. I 70 Î 72 I 74 I 76 - \0 o - N N tv Time (min.) ,,~4~. Q ~ n t1 ~ - Ø) ~ ~ o ;:¡ ~ Abundance N ........¡ o 250000- 200000- 150000- 100000- 50000- o - \0 - - N N N ., ..-L. I 40 95r2228; TIC uf Run at m295600011 05- 30 00 d . AM . COT on Wed L1un 28, 1995 ,k~~,I~~A~~ ~_~~Ir.,w~~. ~k~ ~~ ~ ~~~" I I I 601 80 I 100 I 120 Time (m in. ) I 140 I 160 I 180 .,---- - Q ~ (") t1 ~ Ø) ~ ~ o ::¡ Z o tv ........¡ o Ion 231.20 amu from m29560001100.d 95r2228; Run at 05: 30 AM COT on Wed 0Ùn 28, 1995 Abundance 40000- 30000- 20000- 10000- - .~ . A. "",IL M. II ~ _ ~ JV\/'V'vJ ~V' v"\/ 1 '.JV\,JV ~~¡.J 4~~ o I 140 I 150 I 160 - \0 N - N N N Time (min.) ZZZ/E6r OLZ 'oN ¡Iod~~ mBQ :>WD " ::s =: CD tT iir Co CÞ ." o o ~ ... ~ ëñ GMC Data Report No. 270 193/222 I 'I I/ ~ 'Jo..w~.~J¡...,..t.wA.~ .kJJJ..11 I. 'II , , ~~JJv¡~'vw ~\.v\L..N\U.p)J..¡~~~JJJ1.1A.JM_J~__~ - o~ - N N ~2 0.006 0.008. 0.010. 0.012 0.014. 0.016. 0.018 0.020 0.022. 0.024. 0.026 0.028 0.030. 0.032 o l\.i 0.034 --0 \h :t ~ N Q OJ~ n 0.4!a ~ ~ o./)'Ø. ~ o o.~ Z 0.& N ........¡ O.Q ·-------··1:Ja, /~ z:\gcwork\arCC"· . ";''.001 - Channel A r-'-. . '. Sgc )95 08:21:29 Sample ID . . Acquired 0.048 ,-- "' ;,. o--~~~ ", ., ,L' 1'·..,1, '..,' I.," I I I J I / I I ~~'~,,~~ ..í~:~ ...JJMiLJ ,t'~' ,tM..,¡j~.....JA-,,,J(t.,IV~ 50 d I . I 60 :~'. G) ~ () t:1 ~ - ~ :::ø ~ o ::I. ~ tv ""'-1 o 250000- :'~~ Abundance Ion 191.10 amu 95r2230; Run at 08:; 59 from m29556301063 d PM COT on Fr i Jun '23, 200000- 150000-' 100000- 50000- -' - \C) tit N N tv f 70. . Time (min.) 1995 I 80 -, 90 Q ~ n tJ ~ ~ ~ ~ o ~ ~ - ! ~ . -, /----.... ,-,,-----,- Ion 191.10 amu from m29556301063 d 95r2230: Run at 08: 59 PM COT . on Fr i 0un 23. 1995 Abundance tv ð 250000- - \0 0'\ - tv tv tv 200000- 150000- 100000- 50000- =~LL"",,-,MJl ~ ~--- 'J~JiJJu.J~-~'-'~'-'"~ 0-- I I I I I I I . . 70 I I I I I I 75 I I I 80 Time (m in. ) I 85 I 90 o ~ () t:I Ø) ~ P' ~ ~ o ~ Z o tv ........¡ o - \0 -J - N N N -~-.'. Ion 217.20 amu from m29556301063.d 95r2230; Run at 08:59 PM COT on Fri 0un 23, 1995 Abundance 30000-- 20000- 10000- -~J>r1rN~\'\I\~ J.v'~ ~J'~\þ~\Å~~ 0- I 50 I 55 I I 60 65 Time (min.) \ \ t \ I 70 / , W~~~ I 75 r--'- Q ~ n tj ~ Ø) ~ ~ o ;:¡ Z o tv è3 30000- Ion 217.20 amu from m29556301063.d 95r2230; Run at 08: 59 PM COT on Fr i Jun 23. 1995 Abundance 20000- .>< 10000- =.AJM fv ~ ~ .¡J . 11 \ \ \if " I ~ \ vJ\ ' ~ ~ \v\)~ 0 I I I I I I I - 6.4 66 68 70 72 74 76 \D 00 (m in. ) - Time tv tv N Q &:: n ö Ø) - Ø) ~ ~ o ;:¡ Z o tv ........¡ o - \0 \0 - N N N Ion 218.20 amu from m29556301063.d 95r2230: Run at 08:: 59 PM COT on Fr i tJun 23, 1995 Abundance 40000- 30000- 20000- 10000- ~~'~)J, o 64 I 66 ~J'\J' ^v\/ WJI¡ I 68 I .. 70 Time (min.) "Âv I 72 ~~ I 74 --, ~v~ I 76 ~'. C) a:: n t1 ~ ...... Ø) ~ .g o ~ Z o !:j 14000- o . ...-----........ Ion 259.20 amu from m29556301063.d 95r2230: Run at 08: 59 PM COT on Fr i L1un 23, 1995 Abundance 12000- 10000- 8000 - 6000 - 4000 - = -, J/1ftv 2000 -=/\ Vi, l' v \fvv N 8 - N tv tv 0-' 6.4 I 66 1. . Á V~¡r!~tß' I 68 I ·1 70 72 Time (min.) , ,\ li,~'(I'Wy I ~ j! ~ I 74 I 76 C) ~ () ö ~ Ø) ~ ~ o ~ ~ N -J o tv o - N tv N .~-. Abundance 120000- 100000- 80000- 60000-' 40000- ~ - ~"¡ 95r2230' R . un TIC : ofm29560101001 at 08: 59 AM COT .d on Wed L1un 28, 1995 20000- '.' =,..,~~ h~. "À.~l~ N~ ~¡ i~~Jih ~ ~I~JJJ JMß¡I'I ~ ~ ~ ~~~ 0-" f f 40 I I - I 60 J -, - 80 100 I f 120 140 I Time (m in. ) 160 180 ~. Q ~ () t:J Ø) - ~ ~ (t) "0 o ~ Z o N ........¡ o Abundance 60000- 50000- 40000- 30000- 20000- 10000- N o tv - tv tv tv .~- .. Ion 231.20 amu from m29560101001.d 95r2230: Run at 08:59 AM COT on Wed 0un 28, 1995 0- r 140 ~~lf< t 150 Time (min.) ~.J~i,\J fv.Jv~ I 160 GMC Data Report No. 270 203/222 ,---- Sample 10 : :' ". . S Acquired' gc . 395 03:34:50 Z:\gCWO~\arC/""'--" .. . .001 - Channel A ·ùag - is .. .~ ( ~t Ft°·!a. t~··· Þ'C' C .... ~. ~ ~ ~ 0.616 :-'J ~. ~ C _f") \r--- N Í' \ I ~) o 0.014 --to 0.012 . 0.010 0.008 0.006 h,,~f ~NM .~~~~ ~ ~ ' ' )l J ~ PJ ,~~~JkJk~JJJt~~ ~ ~__JL,~~JlwJ )-..Jf V ~~ J'------....A._~ 0.004. 25 \)'.. , ~ ~. c ~ t ~~~: þ' ~.. t~~ c ... ...; ..., t ~ !:.. ~ c: . \'J ~ ('-J ~t-.., ~& 1'J t:: \"I t--: \0 t-..,. ,-i .~'. -~-, . . Ion 191 10 95z0004' . amu from 2 , Run at 08: 1.' 9 AM m 9555601056 d COT on F· - rl 0un 23, 1995 Abundance 200000- 150000- 100000- 50000- o c ~ .1, I I ~~-M.-~ 11l1lh' II' I 1. I I I I I ....-,'~."'-"I' """,,¡y.) """I J¡J ~i/'J1~..¡....J 1Iv.J\J .j.,¡..,.Jv.v-'~ I I . 50 I I I I 60 I I I 70 I 80 f Time (m in. ) . - - ~ . "-- . .",-.... /~-,- Q ~ ("') t:1 ~ Ø) ~ .g o ~ Z o tv ........¡ o 95Z000~~nR191,10 amu from m29555601056,d . un at 08:19 AM COT on Fr i L1un 23, 1995 Abundance 200000- 150000- 100000- 50000- =~_~~~'^"\I\J..JJ~JL 1-.#. w.~JJJJuw~","~~~ 0- I tv 70 I I I ~ 75 I - 80 tv 85 tv tv -Time (m in. ) _ 4~·..-l ,~' ,~-~'-.. -----........ Q ~ n tJ ~ - fU ~ ~ o ;:¡ Z o N -J o Ion 217.20 amu from m29555601056.d 95z0004: Run at 08: 19 AM COT on Fr i 0un 23. 1995 Abundance 60000- 50000- 40000- 30000- 20000- 10000- . ! \ .1.1 \ =~..\.r\fW/ cIv~J~~Jvn.\ft", \ \ ' 'vv'VI ~ \.""~ 0 I I I I I tv 50 55 60 65 0 -.1 - Time (m in. ) N tv N I 70 I 75 .~, o ~ () t1 ~ ~ ~ ~ o ::¡ Z o tv ........¡ o ------ Ion 217.20 a~u from m29555601056.d 95z0004; Run at 08: 19 AM COT on Fr i 0un 23, 1995 Abundance 30000- 20000- 10000 - I =~ ~~ V\~ o 64 I 66 N o 00 - N N tv I , r 1\ \ I 68 J I 70 J ¡.\ Time (min.) 1 i' \ \ V\ ¡ \ ~ \JI~~ 72 I 74 I 76 ~,,4_ ft ~ .' ~'. ~-~. o ~ (") t; ~ ~ ~ ~ o ;:¡. Z o N ........¡ o Ion 259.20 amu from m29555601056.d 95z0004; Run at 08": 19 AM COT on Fri 0un 23, 1995 Abundance 20000- 15000- 10000- ^:J II t A \ 5000 ~k J-A 'V\ ))AftJ ^ V ! IJtt 'ì/~ ~ \A(JI~ ~ M; V~ 0 I I I I I . I I N 64 66 68 70· 72 74 76 ~ em in. ) - Time N N N C) ~ () t:1 P' ~ P' ~ ~ o ~ Z o N ........¡ o N I--"' o - N N N ,~'. ..~. Ion 218.20 amu from m29555601056.d 95z0004; Run at 08: 19 AM COT on Fr i Jun 23, 1995 Abundance 30000- 20000- 10000~ -~~M\~) o 6.4 I 66 ( . r ~r I 68 ~ fA '11 ",j f ' \ pUV ',\) I I./' I I 70 72 Time (min.) 'M \ ~v~ I 74 I 76 Q ~ (") t1 CJ .-+ CJ ~ ("p "Cj o ;:¡. Z o N -J o N ..... ..... - N N N. .~"" Abundance -. 160000- --1 140000- --J 120000- 100000- 80000- 60000-- 40000- -J 20000 -, -----;' --...., ~ ~'-"\ v.. 'V." ^~ _, -r o /'~'. TIC 0 f ;m2955900 1090 . d 95z0004; Run at 08: 22 PM COT on Man Jun 26, 1995 r. ~ >. '~ J :.. ~ ,I J"f . ," . ,. , , ."~.. . J-, .l~.JLlj¡tJJ" ¡Jf·Wv· '~',,^,,'I'I'A.w &J.,,~¡,~ r 40 r 60 I' r I' I 80 I' f f 100 120 r f 140 Time (min.) r r 160 I - I I 180 ,r-- Q ~ () ö ~ Ø) ~ ~ o ~ Z o tv ........¡ o Abundance 7000 - 6000 - 5000 - 4000 - 3000 - 2000 - I J 1000 - I . f ~I tv ...... tv - tv tv tv o I 140 ------ Ton 231.20 amu from m29559001090.d 95z0004: Run at 08: 22 PM COT on Mon 0un 26, 1995 1 ~ , f I ~'~.M~"~~~'AM'~ \,.-M~~ ~ ,I . '150 I 160 Time (min.) . . ~. . '''I GMC Data Report No. 270 213/222 0002 -.---------, 0.004 .0.006 0.008 0.010 0.012 0014 .0.016 .0.018 0.020 .0022 o ~ 0024 Î\ .J Î\ ". ) 0.026 ~ 0.028 --.a \..'\ 0.030 0.032 0034 Page 2 ot 3 ...._--..-._~-----_._-- -.- J'Þ ith~\\~~~\, _ ~,~ ,I. ~Lk~__ . '. ...~~~J.k.~\J...vv ---- ,..--.... z:\gcwork\arc '>'9.001 - Channel A 25 ¡(~ ~'J ~ w~JdJ~,~ , ! '') Sgc 1995 05:00:54 ..---.J ~. ~ - to-) to-) ~002--.JlJ-' 0.006. 0.008. 0.010. 0.012. 0.014. 0.016 0.018. 0.020 0.022. 0.024. o~ 3:: () 0.612. Ø) - Ø) ~ c@O. o :4- Z 0~8. tv ........¡ o 0.026 . r Sample ID Acquired ."--'. G) ~ n tJ ~ ~ :;d (t) "0 o ;:¡ Z o N ........¡ o tv - Ut - tv N tv ~'.. ,-r......---.-.......... Ion 191.10 amu from m29555701057.d 95z0005: Run at 10:08 AM COT on Fr i Jun' 23. 1995 Abundance 180000- 160000- 140000- 120000- 100000- 80000- 60000- 40000- = . ,~ 20000 ~~kÀJJ.",~~wl~~~. ~.....~........~~WW,-^"k. o I 60 I 70 I 50 40 Time (min.) I 80 Q s: (") ö Ø) - Ø) ~ ~ o ;:¡ Z ? tv ........¡ o tv I-" ~ - N tv tv ,------ .~.... Ion 191 10 . 95z0005' . amu from 2 . Run at 100m 9555701057 d . ¡ 8 AM COT 0 n F· . ¡ r 1 0U n 23. Abundance 80000- 70000 -= 60000- 50000- 40000 -= 30000 -= 20000-= 1000 0 -= \". .) . =~,.~\"~~"..J~ ìj, J.f"'.hW~J JJIv.J.,.J~.,.t~ o I 70 I 75 I I 80 (m in. ) Time 1995 I 85 I 90 ·.--...., (;) ~ () tJ ~ ~ ~ (t) "0 o ~ Z o N ........¡ o Abundance 90000-=: 80000 -=: 70000 -= 60000-=: 50000-=: 40000-= 30000-=: - ",.. ~ . _ _.' ,~f ,- _£ 1995 \ ,^vJ' Jv~'~ .j~~\wJ..JVrJU4Þw'~f.~¡N\J,!f'N~~~Jv...~ 20000-= 10000 = ¡.J./\.I\...;N..J "'I o I 50 N I-' ........¡ - tv N tv -- Ion 217.20 amu from m29555701057.d R t 10'08 AM COT on Fr i 0un 23, 95z0005: . un a . I 55 I 60 I 65 Time (min.) I 70 . I I 75 Or, .",. - ...-.".! - ."\.".- .---- .~'" Q a: n t1 Ø) - ~ ~ (t) "0 o ;:¡ Z o N ........¡ o Ion 217.20 amu from m29555701057.d 95z0005; Run at 10: ;'08 AM COT on Fr i L1un 23, 1995 Abundance 40000- 30000- 20000- 10000 - I P t Â ~\ t I =A\JM Æ~ \¡lrl' \ 1\, ^' vAV ~ 0 I I I I I I tv 6.4 66 68 70 72 74 76 - 00 (m in. ) - Time tv N tv ·-.y - ~-_... . __.._n_____._·_ ¡--. .r---\ ~- Q ~ () d Ø) - Ø) ~ (t) t'd o ::¡ Z o !j 25000- o Ion 218.20 amO from m29555701057.d 95z0005; Run at' 10: 08 AM cor on Fr i 0un 23, 1995 Abundance 20000~ 15000- 10000- r ~. 5000 ~ r A \A \t)', \ ~ '^ ~I\.r'! ¡ '\ I' if ^ · \ N "WV\. vv· ~ ~ o - 6.4 I 66 I 68 I 70 . I I 72 I 74 I 76 t-.) - \0 - N N t..) Time (min.) Q ~ n tJ ~ - ~ ~ ~ o ::¡ Z o N ........¡ o N N o - tv tv t....) f~ AbundCince 25000- 20000- 15000- 10000 - 5000-= ^~ I ' _JVW, ^J'r ~ 0- 64 ,'. ~_.~, r i".: /'---"~'" ! ..- i Ion 259.20 a~u from m29555701057.d 95z0005; Run at 10: 08 AM COT on Fr i 0un 23, 1995 ~" V\v ))~ ^ ~ ~V\v N I 66 I 68 I· I I 70 72 Time (min.) I 74 ....---.........., I 76 a ~ () tJ þ.) ~ þ.) :::0 (D "0 o ::t. ~ -- Abundance N -1 o 120000- N N ...... - N tv. N 100000- 80000- 60000- 40000- 20000- ~*-'14 ...." o . ". .-....~- ,,;:.j} - ----....... ~I ." ...,.." \._.L~~~ J,~~iJ....J.",~ .j'~"'\~'JIW k"t~.~w I - I 40 "'-... ~ ...' "'\ TIC of m29559101091.d 95z0005; Run at 11: 1 PM COT on Man Jun 26, 1995 r 60 I 80 I I - .100 120 Time (min.) I 140 I .160 I I 180 r--.., Q ~ n t1 Ø) ~ Ø) ~ (t) "0 o ::+ z o tv ........¡ o Abundance 2000- 1500 - 1000 - . .......-.... ",. dl.. 1 '.' J W . 50?_ '~- N tv N - N tv tv . o ,_::. I -,-_. I 140 . . >: - -¿.~. :. ;__ ",~i- - -:---~,,-- ~- -- . ~\ --.... 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